The study of shock/boundary-layer interactions on a non-canonical hypersonic geometry involves physical complexities not found on the canonical investigations that dominate the literature. The present case examines a cone-slice-ramp, which combines an upstream asymmetric flow expansion with a downstream three-dimensional compression ramp. Optical diagnostics of the off-body flowfield are a necessary complement to surface instrumentation including high-frequency pressure sensors and Temperature Sensitive Paint (TSP). Focused Laser Differential Interferometry (FLDI) measured the flowfield distribution of second-mode instability waves responsible for transition. Filtered Rayleigh Scattering (FRS) was used for flow visualization of the separation region and unsteady shear layer. Velocimetry through the separation shear layer was provided by Femtosecond Laser Electronic Excitation Tagging (FLEET) whereas Coherent Anti-Stokes Raman Scattering (CARS) measured the thermal profiles through multiple flow features generated by the interaction. These flowfield diagnostics detail the alterations in the shock/boundary-layer interaction as the flow state moves from laminar to transitional to turbulent conditions, revealing behaviors absent from canonical flows.
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