Glass Funnel Research Articles

Assessing residual fragrances on skin after body washing: Optimization of an analytical method using solid-phase microextraction coupled with gas chromatography-mass spectrometry.

The aim of this study is to develop and optimize a method for evaluating the persistence of residual fragrance after body washing, addressing a significant requirement in the development of personal care products. The main objective is to establish a reliable, sensitive and reproducible analytical technique to assess fragrance longevity on skin post-use of body wash products. Headspace solid-phase microextraction (HS-SPME) coupled with gas chromatography-mass spectrometry (GC-MS) is used to analyse residual fragrances. We investigate the extraction efficiencies of various SPME fibres and compare different methods for sampling skin-emitted fragrances, including tape stripping and sealed glass funnels. A controlled body-washing procedure is implemented to standardize the cleansing process. Our findings indicate that the relative standard deviation for measuring five distinct fragrances is within the range of 3%-14%, highlighting the precision of the method. A notable variance exists in the extraction efficiency of fragrances using different types of SPME fibres, with some exhibiting over a threefold difference. Furthermore, the glass funnel method for fragrance collection demonstrates an 11.7 times greater sensitivity to galaxolide than that of the tape-stripping method. Residual fragrances with base notes as the main components can be detected on the skin up to 24 h after body washing. The optimized method for residual fragrance evaluation developed in this study offers a robust tool for analysing fragrance components persisting on the skin for up to 24 h post-wash. This advancement facilitates a deeper understanding of fragrance longevity in personal care products, enabling comparative analyses between different products.

A new filtration system for extraction and accurate quantification of microplastics.

The analysis of microplastics is crucial due to their widespread occurrence and significant impact as environmental pollutants. Appropriate extraction and analytical techniques are necessary to evaluate the abundance, dispersal, and effects of microplastics. In this context, the filtration step to extract microplastics from solution media is indispensable for quantifying microplastics accurately. Usually, a pretreatment procedure such as density separation or solvent extraction is employed before filtration. Nevertheless, the adsorption of microplastic particles onto the glassware surface is known to occur and careful rinsing is inevitable for a suitable recovery rate. The study presents a novel filtration device developed for easy use to increase microplastic recovery from liquid samples. Fluorescent polyethylene (PE) particles were used to examine recovery by optical microscopy and pyrolysis-gas chromatography/mass spectrometry (Py-GC/MS). The conventional filtration system (CFS) exhibited lower microplastic recovery (45.1 ± 7.9%, n = 10) due to the adsorption of microplastics onto the inner surface and the bottom edge of the upper glass funnel. In contrast, the newly developed modified filtration system (MFS) enables fast suction of liquid samples by removing the glass frit with the upper glass funnel and filter being spatially separated. The significantly improved recovery rates using MFS for PE particles were 100% (n = 5) and 93.4 ± 3.4% (n = 10), respectively, confirming the feasibility of the newly developed filtration system to analyze microplastics using Py-GC/MS. The study highlights the importance of filtration processing in establishing analytical standards for assessing and managing microplastics by suggesting MFS as an advanced filtration system.

Studying the effect of the argon flow introduced into the arc discharge in the atomic-emission spectrometry of powdered samples using the spillage-injection method

Atomic emission spectral analysis of a powder sample by the method of spillage-injection into the plasma of an arc discharge burning in air is accompanied by the formation of cyanide, nitride and oxide compounds which form molecular bands in the spectrum thus impeding measuring the intensity of the analytical lines of the elements to be determined. Feeding an argon flow into the arc discharge can reduce the amount of spectral interference and increase the plasma temperature, which promotes more a complete evaporation of the analyzed sample injected into the arc discharge and, accordingly, increases the degree of ionization of the elements and the intensity of ion spectral lines. The aim of the study was to develop a device for argon introduction into the arc discharge zone and simultaneous sample delivery by a spillage-injection method, as well as to study the effect of argon consumption on arc discharge parameters and emission spectra of powder samples. The argon input device (up to 2.25 L/min) is developed on the basis on glass funnels, the geometric dimensions of which are selected with the goal of gaining the maximum intensity of spectral lines and reduced intensity of molecular bands at the minimal argon consumption. The study carried out on a «Grand Potok» spectrometer demonstrated that with an increase in argon consumption, the intensity of SiO molecular bands decreases, the plasma temperature increases by 350 – 540 K, and the intensity of ion and atomic lines with the ionization energy above 8 eV increases by more than 4.7 and 2.9 times, respectively. The developed device can be used in analysis of geological materials to improve the metrological characteristics of the results of atomic emission spectral analysis.

Start Up And Operation Of A UASB Rector With Molasses As A Preferred Substrate – A Case Study

Anaerobic digestion followed by aerobic treatment has gained wide acceptability for many of the wastewater treatment. Several novel bio-reactors have been developed. All these reactors pose a problem of shock loading, when the high COD organic industrial waste is fed in to the reactor. Further, the normal substrates like glucose, sewage, citric acid may result in addition of a large volume of the substrate solution for a given organic loading. Both these problems are solved by adopting molasses, a typical by-product from the sugar industry. Among the bio-reactors to treat high strength waste waters, the Up-flow Anaerobic Sludge Blanket Reactor (UASBR), has received wide popularity for the treatment of domestic waste waters as well as for a variety of industrial wastewaters. This paper is to present a cogent and a clear picture of the startup and steady state operation of an UASB Reactor with molasses as the initial startup substrate for the development of well settleable sludge granules, the major feature of an UASB Reactor. The UASB reactor was fabricated in transparent Plexiglas. The reactor had a working volume of 9.75 liters with provision of ports for input, output, collection of samples, and collection of gas. Inside the settler, a gas-liquid-solid separation system using a glass funnel and a gas pressurizing plexiglass tube was provided. The aim was to granulate the sludge and acclimatizing it completely to take high organic loading. The feed was supplemented with a fixed COD: N: P ratio by adding urea for nitrogen and KH2PO4 for phosphorous. The HRT was fixed to be 8 hours. The reactor temperature was maintained at 35 ± 20oC. In about 55 days, the buttery seed sludge got granulated at an OLR of 8 g COD/l.day. The SEM of the granules exhibited a mixed morphology on the surface of the granules while filamentous Methanothrix proliferation could be clearly seen in the interior of the granule. Methanoceata and Methanothrix are the two dominant species found in the granules.

Girls’ school-to-work transitions into male dominated workplaces

ABSTRACT The article addresses school-to-work transitions among young women in a strongly male dominated professional sphere – the transport industry. Drawing on interviews with two girls over the time span 2015–2022 and visits to their upper secondary school 2016–2019, the study focuses on how power structures related to gender play out in the positioning that takes place in school and workplaces: How the girls were positioned socially and in relation to professional qualification, and how they positioned themselves in these respects. The findings indicate significant changes in discourse and practice when the girls transitioned from students to employees, changes which in the article are discussed in the framework of ‘inequality regimes’ and through the lens of the ‘glass funnel’ metaphor. Linking the funnel metaphor to the framework of inequality regimes broadens the picture to consider how young people are exposed to generally increasing inequalities in labour markets where institutions and organisations are affected by neoliberal economic policies, weakened collective protection of workers and wider wage gaps. With individualisation and insecurity, young people like the two girls in focus in this article, are increasingly left to fend for themselves in a harsh labour market.

Using a Cone-Shaped Glass Funnel Adapter Reduces Endothelial Cell Loss Caused by Preloading Descemet Membrane Endothelial Keratoplasty Tissue.

The aims of this study were (1) to compare "front" and "rear" methods for loading Descemet membrane endothelial keratoplasty (DMEK) tissue into both micro-Jones and standard-Jones tubes and (2) to evaluate the efficacy of a cone-shaped glass funnel adapter designed to make loading DMEK tissue safer for corneal endothelial cells. The corneal endothelium was stained with 0.06% trypan blue to confirm equivalence between mate corneas. The tissues were then processed using the Iowa Lions Eye Bank standard DMEK protocol. In comparison 1, one mate was loaded into the rear of a micro-Jones or standard-Jones tube and the other was loaded into the front of the same tube. In comparison 2, one mate was loaded into the front of the micro-Jones tube and the other was loaded through the cone-shaped funnel adapter into the rear. All tissues were ejected through the front of the modified Jones tubes and assessed for endothelial cell loss (ECL) with calcein AM staining, FIJI, and Trainable Weka Segmentation; scroll widths were measured digitally. There were no statistically significant differences in ECL between front and rear loading [micro (N = 6 pairs): front 15.74% vs. rear 17.95%; standard (N = 6 pairs): front 19.58% vs. rear 19.17%; all P > 0.05]. DMEK scrolls loaded with the funnel adapter exhibited lower ECL compared with scrolls loaded through the front [micro (N = 8 pairs): front 13.53% vs. loading funnel 2.40%; P < 0.001]. Loading with the adapter was not faster (front 6.66 seconds vs. loading funnel 5.52 seconds; P = 0.24). Using a cone-shaped DMEK loading funnel may reduce ECL sustained during preloading.

Microplastics and anthropogenic debris in rainwater from Bahia Blanca, Argentina

Concern about atmospheric microplastic (MP) contamination has increased in recent years. This study assessed the abundance of airborne anthropogenic particles, including MPs, deposited in rainfall in Bahia Blanca, southwest Buenos Aires, Argentina. Rainwater samples were collected monthly from March to December 2021 using an active wet-only collector consisting of a glass funnel and a PVC pipe that is only open during rain events. Results obtained show that all rain samples contained anthropogenic debris. The term “anthropogenic debris” is used to refer to the total number of particles as not all the particles found could be determined as plastic. Among all the samples, an average deposition of 77 ± 29 items (anthropogenic debris) m−2d−1 was found. The highest deposition was observed in November (148 items m−2d−1) while the lowest was found in March (46 items m−2d−1). Anthropogenic debris ranged in size from 0.1 mm to 3.87 mm with the most abundant particles being smaller than 1 mm (77.8%). The dominant form of particles found were fibers (95%), followed by fragments (3.1%). Blue color predominated (37.2%) in the total number of samples, followed by light blue (23.3%) and black (21.7%). Further, small particles (<2 mm), apparently composed of mineral material and plastic fibers, were recognized. The chemical composition of suspected MPs was examined by Raman microscopy. The analysis of μ-Raman spectra confirmed the presence of polystyrene, polyethylene terephthalate, and polyethylene vinyl acetate fibers and provided evidence of fibers containing industrial additives such as indigo dye. This is the first assessment of MP pollution in rain in Argentina.

Effects of Olfactory Stimulation with Aroma Oils on Psychophysiological Responses of Female Adults.

This study investigated the effects of olfactory stimulation with aroma oils on the psychophysiological responses in women. Ten aromatic oils (lavender, rosemary, rose, eucalyptus, jasmine, geranium, chamomile, clary sage, thyme, and peppermint) were used on 23 women aged between 20 and 60 years. They inhaled the scent for 90 s through a glass funnel attached to their lab apron, 10 cm below their nose, while the pump was activated. Electroencephalography, blood pressure, and pulse rate were measured before and during inhalation of the aroma oils. The relative alpha (RA) power spectrums indicating relaxation and resting state of the brain significantly increased when lavender, rosemary, eucalyptus, jasmine, chamomile, clary sage, and thyme oils were inhaled compared to those of before olfactory stimulation. The ratio of alpha to high beta (RAHB), an indicator of brain stability and relaxation, significantly increased when rosemary, jasmine, clary sage, and peppermint oils were inhaled. The relative low beta (RLB) power spectrum, an indicator of brain activity in the absence of stress, significantly increased when stimulated with lavender, rosemary, rose, and geranium scents. Further, systolic blood pressure significantly decreased after introduction of all 10 types of aromatic oils, which indicates stress reduction. Thus, olfactory stimulation with aroma oil had a stabilizing effect on the prefrontal cortex and brain activity and decreased systolic blood pressure.

Direct Measurement of Mercury Deposition at Rural and Suburban Sites in Washington State, USA

Because of mercury’s (Hg) capacity for long-range transport in the atmosphere, and its tendency to bioaccumulate in aquatic biota, there is a critical need to measure spatial and temporal patterns of Hg atmospheric deposition. Dry deposition of Hg is commonly calculated as the product of a measured atmospheric concentration and an assumed deposition velocity. An alternative is to directly assess Hg deposition via accumulation on surrogate surfaces. Using a direct measurement approach, this study quantified Hg deposition at a rural site (Pullman) and suburban site (Puyallup) in Washington State using simple, low-cost equipment. Dry deposition was measured using an aerodynamic “wet sampler” consisting of a Teflon plate, 35 cm in diameter, holding a thin layer (2.5 mm) of recirculating acidic aqueous receiving solution. In addition, wet Hg deposition was measured using a borosilicate glass funnel with a 20-cm-diameter opening and a 1 L Teflon sampling bottle. Hg deposition was estimated based on changes in total Hg in the aqueous phase of the samplers. Dry Hg deposition was 2.4 ± 1.4 ng/m2·h (average plus/minus standard deviation; n = 4) in Pullman and 1.3 ± 0.3 ng/m2·h (n = 6) in Puyallup. Wet Hg deposition was 7.0 ± 4.8 ng/m2·h (n = 4) in Pullman and 1.1 ± 0.2 ng/m2·h (n = 3) in Puyallup. Relatively high rates of Hg deposition in Pullman were attributed to regional agricultural activities that enhance mercury re-emission and deposition including agricultural harvesting and field burning. Hg concentration in precipitation negatively correlated with precipitation depth, indicating that Hg was scavenged from the atmosphere during the beginning of storm events. Because of their relative simplicity and robustness, direct measurement approaches such as those described in this study are useful in assessing Hg deposition, and for comparing results to less direct estimates and model estimates of Hg deposition.

The Glass Funnel: A Tool to Analyse the Gender Regime of Healthcare Education and Work

ABSTRACT The concepts glass escalator and glass ceiling have been widely used in studies of gender and organisations. In this paper we propose a novel metaphor to describe and analyse gender segregation and discrimination, that of a glass funnel. This concept does not relate to men and women as groups in the sense of fixed collective entities, but rather shows how taken-for-granted distinctions between men and women are reiterated and promote men in a way that downgrades women. However, as gender intersects with other power structures, both men and women can be propelled downwards through the funnelling motion made up of a market-oriented devaluation of the healthcare profession. Through an empirical investigation of the community of practice and gender regime of an upper secondary healthcare education programme in Sweden, we develop the glass funnel concept, an analytical tool aiming to open up for intersectional analyses of healthcare education and work.

Developing of a 3D Printer to Produce Parts Using Powder Metal

The additive manufacturing (AM) process or three-dimensional printing (3DP) process is making stereoscopic shapes using a layered system. There are several materials used for printing such as plastic, wood, metal as powder, filament, liquid, or others, and there are also different ways for printing. Recently, the focus has been on metal printing, but the problem is that the high energy used such as laser, electron beam, or high heat to melt the metal to print it as required. For this reason, the price of 3D printers for metal is very expensive. In this paper, the design and implementation of a 3D printer for metal parts production are worked. The work also includes making an experimental test for the new 3D printer and printing 3D metal parts without using heat. In this work, Tevo-Tarantula 3D printer has been modified in terms of software and hardware. Two new extruders are designed to inject the metal powder and adhesive, where the heat was removed from the extruder head and the printer bed. The metal powder extruder contains a powder reservoir, glass funnel, and access valve where controlled through the solenoid valve. The adhesive extruder is controlled using a simple hydraulics. The printing process was done by printing two layers of metal powder and a layer of adhesive depending on the desired shape to create 3D objects using the SolidWorks software. Different metal models were printed and these models were compared with the original design which was drawing by SolidWorks software. The difference between the actual model drawing and the printed parts is differences between (0.004 mm) for some parts to (2.3 mm) for other parts or the percentage of error is between (0.1% - 4%) for the printed parts. However, the material can be used in high temperatures, where rubber materials cannot be used, and in applications requiring porosity.

Antimicrobial and Antioxidant Activities of Novel Marine Bacteria (Bacillus 2011SOCCUF3) Isolated from Marine Sponge (Spongia officinalis)

Background : Bacillus species represent a rich source of new bioactive metabolites that can combat diseases. Methods: Bacillus strain was isolated from the marine sponge Spongia officinalis and routinely maintained on marine broth. The bacteria strain was identified as Bacillus 2011SOCCUF3 using 16S rDNA sequencing. The strain was cultured on Tryptone Casein Oat Soluble Starch (TCOATSS) media with continuous agitation for 4 days. The fermented broth was centrifuged, and the supernatant was mixed with 10% (w/v) of adsorbent resin (XAD-7HP and XAD-16N, 1:1) and shaken continuously at a reduced speed for 7 h; and the resin was collected by filtration through sintered glass funnel and washed with MilliQ water, and then eluted with methanol to obtain the extract. The extract was evaporated in vacuo at reduced temperature and pressure to obtain the dry extract. The dry extract was purified by vacuum liquid chromatography, eluting with methanol in acetone gradient. The in vitro antimicrobial and antioxidant activities were investigated using the agar-well diffusion, DPPH scavenging and the phosphomolybdate methods respectively. Results: The extract and fractions showed good antimicrobial activities with minimum inhibitory concentration range of &lt;1.0 mg/mL. The extract and fractions also exhibited good antioxidant activities with their IC50 values been comparable to the standard. Conclusion: Thus, a novel Bacillus strain isolated from the marine sponge (Spongia officinalis) obtained from Cortiou and Riou, France, exhibited promising antimicrobial and antioxidant activities.

Investigation of the microplastics profile in sludge from China’s largest Water reclamation plant using a feasible isolation device

Sewage sludge, which is widely applied to land as a fertilizer, is a key source of microplastics in the environment. We sought to develop a feasible device for isolation of microplastic from sewage sludge for further understanding their fates in the environment. In the present study, an effective isolation device, consisting of a fritted glass funnel and a glass filtration apparatus, was constructed to extract microplastics from sludge with nearly 100% recovery efficiency. Then, a high abundance of microplastics was detected in sludge sampled from China’s largest sewage treatment plant. Among the 25 types of microplastic polymers confirmed by Fourier transform infrared spectroscopy, poly(11-bromoundecyl acrylate) (PBA) and poly(11-bromoundecyl methacrylate) (PBMA) accounted for 23.63% of total microplastics detected. Rayon, polyethylene (PE), polyethylene terephthalate (PET), polypropylene (PP), and copolymers, such as PP/PE and poly(styrene:acrylonitrile:butadiene) (ABS), were also detected. The shapes of these microplastics consisted of pellets, fragments, films, and microfibers. Characterization of the isolated microplastics revealed that domestic applications and vehicle products were the major sources of microplastic in sewage treatment sludge. Some priority recommendations were issued based on these results. In conclusion, the present study demonstrate that the device is effective for the isolation of microplastics from sludge.

Developing of a 3D Printer to Produce Parts Using Powder Metal

The additive manufacturing (AM) process or three-dimensional printing (3DP) process is making stereoscopic shapes using a layered system. There are several materials used for printing such as plastic, wood, metal as powder, filament, liquid, or others and there are also different ways for printing. Recently, the focus has been on metal printing, but the problem is that the high energy used such as laser, electron beam, or high heat to melt the metal to print it as required. For this reason, the price of 3D printers for metal is very expensive. In this paper, design and implementation of a 3D printer for metal parts production are worked. The work also includes making an experimental test for the new 3D printer and printing 3D metal parts without using heat. In this work, Tevo-Tarantula 3D printer has been modified in terms of software and hardware. Two new extruders are designed to inject the metal powder and adhesive, where the heat was removed from the extruder head and the printer bed. The metal powder extruder contains a powder reservoir, glass funnel, and access valve where controlled through the solenoid valve. The adhesive extruder is controlled using a simple hydraulics. The printing process was done by printing two layers of metal powder and a layer of adhesive depending on the desired shape to create 3D objects using the SolidWorks software.Different metal models were printed and these models were compared with the original design which was drawing by SolidWorks software. The difference between the actual model drawing and the printed parts is differences between (0.004 mm) for some parts to (2.3 mm) for other parts or the percentage of error is between (0.1% - 4%) for the printed parts. However, the material can be used in high temperatures, where rubber materials cannot be used, and in applications requiring porosity. Keywords: 3D printer, powder metal, adhesive, layered system, FDM. DOI : 10.7176/ISDE/10-5-02 Publication date :June 30 th 2019

Metabolic Cage for Urine Collection from Small Animals with High Level of Performance and Low Cost

The results of designing the original metabolic cage for urine collection from small laboratory animals consisting of a case, a cylindrical animal chamber with the floor, a funnel, a urine collection vessel and two graded drinking bottles that can be placed at a different height depending on animal age are presented. The case was made of laminated particle board; a cylindrical animal chamber was made of polyethylene terephthalate; a circular floor of the animal chamber was made of stainless steel wire cloth mesh. As a funnel for urine collection, a ribbed glass funnel SIMAX (Czech Republic) was used. To prevent rat feces from entering the urine collection vessel, there were installed two stainless steel wire mesh filter discs, namely a larger disc located on the internal ribbed surface of the funnel and a smaller disc located close to the hole of the funnel tube. To support the urine collection vessel, a metal vessel stand with a deepening was made. Between the vessel and the funnel, there was placed a fine stainless steel metal cylinder preventing urine evaporation.&#x0D; In addition to low cost, the proposed design of the metabolic cage provides high levels of performance as confirmed by its high ability to allow urine to flow freely, as well as to collect urine, significantly smaller volume of urine evaporated, improved housing conditions for animals and allows us to collect the amount of urine more fully reflecting animal diuresis.

SUBSTÂNCIAS TÂNICAS PRESENTES EM PARTES DA ÁRVORE SABIÁ (Mimosa caesalpiniifolia Benth.) EM PLANTIO COMERCIAL DE 5 ANOS

RESUMO: O sabiá (Mimosa caesalpiniifolia Benth.) é uma espécie arbórea, nativa do bioma Caatinga, de grande abrangência e de relevante interesse econômico, pelo seu potencial madeireiro e forrageiro. Estudos vem sendo desenvolvidos, buscando espécies da região Nordeste do Brasil com potencial tanífero em função da exploração desordenada sobre o Angico vermelho (Anadenanthera colubrina (Vell.) Brenan) para a exploração da casca e seu uso no curtimento de peles. Baseado nisto, este estudo teve como objetivo, analisar folhas, galhos finos e casca da espécie sabiá, quanto a suas características como produtora de taninos vegetais. Os materiais foram secos ao ar, moídos e classificados, tendo sido utilizada a porção que passou por uma peneira de 16 “mesh” (1,00 mm) e ficou retida numa de 60 “mesh” (0,25 mm). Para as extrações foram utilizados 25 gramas de cada material. O extrato obtido foi passado em peneira de 150 “mesh” (0,105 mm), em tecido de flanela, filtrado em funil de vidro sinterizado de porosidade 2 e concentrado. Em seguida, foram determinados o teor de sólidos totais (TST) e o teor de taninos condensados (TTC). Todas as partes da planta analisadas apresentaram taninos, porém, a casca da planta apresentou maior concentração de taninos condensados (8,38%) e menor quantidade de não taninos (1,22%), indicando que dentro do extrativo, há uma quantidade de tanino considerável. Conclui-se que a casca do sabiá apresenta potencial como produtora de taninos vegetais, sendo necessário a realização de estudos para identificar seu potencial no curtimento de peles dentre outras formas de utilizações.PALAVRAS-CHAVE: Floresta seca, Produto Florestal não Madeireiro, Taninos vegetais.

An efficient microwave assisted synthesis of N′-aryl/(alkyl)-substituted N-(4-hydroxy-6-phenylpyrimidin-2-yl)guanidines: Scope and limitations

Abstract Treatment of N-[(4-hydroxy-6-phenyl)pyrimidin-2-yl]cyanamide with 1° alkyl or arylamines in isopropyl alcohol for only 10 min at 110–120 °C under microwave conditions gave the corresponding N′-alkyl(aryl)guanidine derivatives in excellent yields (65–84%). Isolated yields were greatest when >1.0 equiv. of amines were employed, but excellent results were also obtained when aryl and alkylamines were reacted with a more atom-economical loading (1.0 equiv.; 70% and 72% ave. yields, respectively). Arylamines with either highly electron withdrawing substituents (e.g. CO 2 H) or pi-deficient heterocycles (e.g. variously substituted aminopyridines) did not work well under these conditions, and reaction with ureas and/or amino acids did not give detectable products. Work-up was exceedingly simple, and involved simple collection and washing of product on a sintered glass funnel. Products were obtained in analytically pure form and required approximately 1 h to prepare, start to finish.

A Modified Cooling Method and its Application in Drosophila Experiments

Chilling is a cost-effective and safe method of immobilising flies in Drosophila experiments. However, should condensation form on the plate, it would be fatal to the flies. Here we describe a modified cooling method using reusable commercial ice pack(s) (ca. 400 ml, 2–3 cm tall) rather than crushed ice. The ice pack is covered with a piece of filter paper which absorbs the condensed water formed on the cold surface, and the moistened filter paper does not wet the wings of flies inverted onto it. An ice pack (ca. 400 ml) takes effect in at least 1 h, and its height is shorter than the maximum specimen height of a dissecting microscope, so that flies can be checked while they remain on the cold surface. This method overcomes the disadvantages of the indigenous cooling anaesthetising approach and makes it practically feasible. We also describe an easy-to-make fly-transferring toolkit which will greatly facilitate fly transferral when it is combined with our chilling method. In our design, the flies were directed out of a vial by a blue pipette tip, which is inserted in a foam stopper and channelled down into another vial by a glass funnel inserted in another foam stopper which is escape-proof.

Novi infundibulum na nekropoli antičkog Jadera

Na nedavnim zaštitnim arheološkim istraživanjima u Ulici fra Ivana Zadranina u Zadru potvrđena je zona nastavka antičke nekropole. Tom je prigodom ustanovljeno 35 antičkih ukopa. Velika većina otkrivenih grobova su paljevinski grobovi s veoma bogatim nalazima i prilozima. Jedan od njih je i incinerirani ukop – grob 34, u kojem je pronađen i stakleni lijevak – infundibulum. Na zadarskom području s novim je nalazom lijevka do sada otkriveno čak sedam u cijelosti očuvanih staklenih infundibula. Uz dva lijevka bez konteksta nalaza, svi su ostali otkriveni u grobnom kontekstu incineriranih ukopa pri arheološkim istraživanjima antičke nekropole Jadera. Stakleni lijevci posve su specifičan i rijedak oblik slobodno puhanog staklenog posuđa koje služi za pretakanje a ne za pohranu različitih tekućina. Možda su upravo nalazi brojnih staklenih lijevaka na ovom prostoru, a za koje se pretpostavlja da su istočnomediteranske produkcije, rezultat aktivnosti prerade aromatičnog i ljekovitog bilja. Toj pretpostavci ide u prilog i brojnost nalaza ostalih staklenih oblika, ali i postojanje lokalne staklarske radionice (ili više njih). Stoga potrebaza staklenim proizvodima općenito, pa tako i za lijevcima, s obzirom da je staklo veoma neutralno na sadržaje koji se u njemu pohranjuju, ima svoje uporište u aktivnostima proizvodnje različitih farmaceutskih pripravaka. Ako je suditi po staklenim lijevcima, takva se aktivnost odvijala u drugoj polovini 1. st. po. Kr.

A study on PbO in CRT funnel glass at high-temperature condition

Glasses from the end-of-life Cathode Ray Tubes (CRTs) represent a pressing environmental problem, especially the funnel glass containing high lead concentration. To avoid lead contamination and re-utilise it, it is of great importance to study the separation process of lead contained in the funnel glass. In this study, the microstructure of scrap funnel glass and molten funnel glass were analysed by SEM and XRF. The results indicated that the PbO content in the top was more than that in the bottom. PbO would be released from scrap funnel glass at high-temperature condition when Na 2 O was added into the glass specimens.