Fatigue Resistance Research Articles

Evaluation of mechanical properties of an original and a replica-like reciprocating instruments.

This study assessed the mechanical properties of the Only One File Blue and the Reciproc Blue instruments. A total of 80 new 25 mm reciprocating NiTi instruments (25/.08v) were evaluated for their mechanical performance (n = 40 per group). Cyclic fatigue resistance, torsional fatigue, flexural resistance and buckling resistance tests were conducted. Statistical analysis was employed with a significance level set at 5%. The results indicated no statistically significant differences in resistance to cyclic fatigue neither in the fragment length between the instruments (p > 0.05). However, the Reciproc Blue instrument exhibited greater torque to fracture and a larger rotation angle than the Only One File Blue instrument (p < 0.05). The Only One File Blue instrument demonstrated higher flexibility but lower resistance to buckling compared to the Reciproc Blue instrument (p < 0.05). In conclusion, the tested instruments exhibit differences in mechanical properties, with the Reciproc Blue instrument generally presenting greater advantages than the Only One File Blue.

Lysine-Triggered Polymeric Hydrogels with Self-Adhesion, Stretchability, and Supportive Properties

Hydrogels, recognized for their flexibility and diverse characteristics, are extensively used in medical fields such as wearable sensors and soft robotics. However, many hydrogel sensors derived from biomaterials lack mechanical strength and fatigue resistance, emphasizing the necessity for enhanced formulations. In this work, we utilized acrylamide and polyacrylamide as the primary polymer network, incorporated chemically modified poly(ethylene glycol) (DF-PEG) as a physical crosslinker, and introduced varying amounts of methacrylated lysine (LysMA) to prepare a series of hydrogels. This formulation was labeled as poly(acrylamide)-DF-PEG-LysMA, abbreviated as pADLx, with x denoting the weight/volume percentage of LysMA. We observed that when the hydrogel contained 2.5% w/v LysMA (pADL2.5), compared to hydrogels without LysMA (pADL0), its stress increased by 642 ± 76%, strain increased by 1790 ± 95%, and toughness increased by 2037 ± 320%. Our speculation regarding the enhanced mechanical performance of the pADL2.5 hydrogel revolves around the synergistic effects arising from the co-polymerization of LysMA with acrylamide and the formation of multiple intermolecular hydrogen bonds within the network structures. Moreover, the acid, amine, and amide groups present in the LysMA molecules have proven to be instrumental contributors to the self-adhesion capability of the hydrogel. The validation of the pADL2.5 hydrogel’s exceptional mechanical properties through rigorous tensile tests further underscores its suitability for use in strain sensors. The outstanding stretchability, adhesive strength, and fatigue resistance demonstrated by this hydrogel affirm its potential as a key component in the development of robust and reliable strain sensors that fulfill practical requirements.

Implantable Wet‐Adhesive Flexible Electronics with Ultrathin Gelatin Film

AbstractImplantable flexible electronic has attracted significant research interest in various fields. However, it still faces the challenge of simultaneously achieving tight adhesion to tissues in a mildly wet environment and possessing excellent biocompatibility to reduce immune rejection reactions after implantation. Here, a degradable wet‐adhesive flexible electronic device based on liquid metal and ultrathin gelatin film is developed. The ultrathin gelatin film forms numerous hydrogen bonds with tissue in a slightly humid environment, rapidly constructing a wet‐adhesive interface without damaging tissue structure. Inkjet printing is utilized to pattern the mixture of liquid metal and PVP on the surface of the ultrathin gelatin to create flexible patch. With the excellent conductivity of liquid metal, low toxicity, and similarity to natural tissue components of gelatin, flexible patch exhibits outstanding biocompatibility and fatigue resistance. It can be implanted in the body for up to 6 weeks, retaining monitoring capabilities and resisting 1 000 000 cycles of bending fatigue. This study provides a novel strategy for the future development of implantable flexible electronics.

Cartilage-Inspired, High-Strength, and Heat-Tolerant Lubricating Hydrogels by Macrophase Separation.

Hydrogels are considered as a potential cartilage replacement material based on their structure being similar to natural cartilage, which are of great significance in repairing cartilage defects. However, it is difficult for the existing hydrogels to combine the high load bearing and low friction properties (37 °C) of cartilage through sample methods. Herein, we report a facile and new fabrication strategy to construct the PNIPAm/EYL hydrogel by using the macrophase separation of supersaturated N-isopropylacrylamide (NIPAm) monomer solution to promote the formation of liposomes from egg yolk lecithin (EYL) and asymmetric template method. The PNIPAm/EYL hydrogels possess a relatively high compressive strength (more than 12 MPa), fracture energy (9820 J/m2), good fatigue resistance, lubricating properties, and excellent biocompatibility. Compared with the PNIPAm hydrogel, the friction coefficient (COF 0.046) of PNIPAm/EYL hydrogel is reduced by 50%. More importantly, the COF (0.056) of PNIPAm/EYL hydrogel above lower critical solution temperature (LCST) does not increase significantly, exhibiting heat-tolerant lubricity. The finite element analysis further proves that PNIPAm/EYL hydrogel can effectively disperse the applied stress and dissipate energy under load conditions. This work not only provides new insights for the design of high-strength lubricating hydrogels but also lays a foundation for the treatment of cartilage injury as a substitute material.

Study on the influencing factors of mechanical properties of anti-icing modified asphalt mortar

Accumulated snow and ice on road surface affect traffic operation. Anti-icing asphalt pavement is widely implemented as an active snow melting technology. However, there are few studies on anti-icing modified asphalt mortar mechanical properties and the effect of mortar materials on the interaction between modified asphalt and anti-icing filler. For this reason, this study investigated the mechanical properties of asphalt including rheological, high-temperature, fatigue and low-temperature properties through frequency and temperature scan, multiple stress creep recovery, linear amplitude scan, and single edge notched beam test. Based on this, the significant factors affecting asphalt mechanical properties were identified by analysis of variance. Subsequently, the Palierne-C-G* parameter was used to quantify the interaction between modified asphalt and anti-icing filler, and the effect of asphalt chemical structure on the interaction was revealed by Fourier Transform Infrared Spectroscopy (FTIR) test. The results indicated that the anti-icing filler significantly improved the high temperature and fatigue resistance of asphalt. Compared with SBS modified asphalt mortar, the mechanical properties of composite modified asphalt mortar were superior. The most significant factor affecting the mechanical properties of SBS modified asphalt mortar was modifier dosage, while the most significant factor affecting the composite modified asphalt mortar was crushed rubber dosage. The interaction showed a decreasing trend with the increase of frequency, while it appeared to increase and then decrease with the increase of temperature. The carbonyl functional group of asphalt correlated best with the interaction between asphalt and filler.

Performance evaluation of SBS-modified asphalt mixtures incorporating waste tire rubber and HDPE

Based on the functional complementarity of waste tire rubber (WTR) and waste high-density polyethylene (HDPE) in asphalt, this study presents a novel approach that simultaneously utilizes WTR and HDPE for modification and substitution of styrene-butadiene-styrene (SBS) modified asphalt. Through experiments on three major indicators, the dosage ratios of the three polymers are scientifically designed using the response surface methodology, and four different ratios of SBS-HDPE-WTR are selected to prepare modified asphalt mixtures. Performance evaluations are conducted on various pavement properties, including high-temperature stability, low-temperature crack resistance, water stability, fatigue resistance, and aging resistance, by comparing them to the reference 4% SBS-modified asphalt mixture. The results demonstrate that the addition of WTR significantly improves the elastic properties and fatigue resistance of the mixture, while the addition of HDPE enhances its high-temperature stability and aging resistance. The SBS-HDPE-WTR asphalt mixtures, designed with appropriate ratios, exhibit superior high-temperature stability, low-temperature crack resistance, and fatigue resistance. Therefore, the use of these waste materials in asphalt mixtures offers a sustainable and environmentally friendly solution for the construction industry.

Nanofiber derived MXene composite paper for electromagnetic shielding and thermal management

Despite the urgent demands in protecting wearable electronics from electromagnetic interference (EMI) in various conditions, it remains challenging to attain mechanically robust and flexible materials with both excellent EMI shielding and thermal managing performance. Herein, we report MXene composite paper that can provide multifunction with superior mechanical properties. To construct a hierarchical composite with 2D/0D reinforcements, the MXene paper is fabricated by hot pressing of electrospun Poly (vinylidene fluoride-co-hexafluoropropylene) (PVDF-HFP) nanofibers incorporated with MXene nanosheets and carbon black nanoparticles. Due to the laminated structure connected by nanoparticles, the flexible composite paper shows remarkable mechanical strength and fatigue resistance that can provide stable EMI shielding effectiveness of 500 dB/mm even after 10000th cyclic rolling. Moreover, the high in-plane electrical conductivity and out-of-plane thermal conductivity allow a fast electrothermal heating and cooling behavior, which qualifies the MXene paper as multifunctional surface for wearable electronics.

Effect of surface rolling process on rolling contact fatigue behavior and failure mechanism of powder metallurgy steel

The effect of surface rolling process on the surface microstructure and rolling contact fatigue of the Fe-2Cu-0.6 C powder metallurgy steel was investigated in the present investigation. Results indicated that a densified and hardened layer with a densification depth of 330 μm and a surface hardness of 330 HV0.1 was generated in the surface layer after rolling process. Ferrite grain and pearlite lamellae became typical fibrous structures on the top surface. The microstructure of pearlite was presented by two typical features. One was that the discrete cementite plates were severely curled and wavy. The other one was that the cementite plates remained parallel to each other, but were a reticular structure at a macroscopic level. The rolling contact fatigue (RCF) test showed that the RCF life of the rolled sample was superior. The L10, L50, L63.2 life increased by 182%, 105%, 92%, respectively. Surface initiated spalling was the main fatigue failure mode. Subsurface equivalent contact stress and local equivalent stress were calculated. The results showed that surface cracks were due to the repetitive tensile stress, which caused pits. Subsurface cracks nucleated and propagated in the region where the local equivalent stress was higher than the matrix yield strength, which caused spalling as connecting with surface cracks. The surface densified layer plays an important role in improving the rolling fatigue resistance of the material.

Design, simulation and energy dissipation evaluating of a new lead shear damper

This study presents a novel design for a lead shear damper (LSD) that features lead blocks encased in laminated steel and rubber plates, intersected by X-shaped steel sticks. It combines the excellent energy dissipation and fatigue resistance of lead with the uniform yielding capabilities of X-shaped steel sticks along their height. Cyclic loading testing and fatigue tests are conducted in order to determine the mechanical properties of the LSD. The test results reveal that the LSD has a variable yielding force, and exhibits stiffness hardening when the damper's deformation direction deviates from the origin. However, when the deformation direction returns to the origin, there is no stiffness hardening observed, and the resistant force remains constant. Furthermore, this LSD can work effectively despite the failure of energy dissipation parts, which improves hysteretic energy dissipation under large deformation. In order to replicate the hysteretic behaviour, a uniaxial constitutive model is formulated and its parameters are determined by the utilization of the differential evolution approach, based on test data. The observed strong concurrence between the experimental and simulated hysteresis curves serves as compelling evidence for the efficacy of the differential evolution method. Meanwhile, a three-story building from the third-generation benchmark problem is employed as the testbed structure to examine the energy dissipation capacity of the developed dampers. Nonlinear seismic analysis on the benchmark model equipped with the proposed dampers is also conducted, and the results are compared to those fitted with conventional dampers, such as mild dampers and friction dampers. The findings of this study indicate that the performance of the LSD in reducing structural displacements is superior to that of mild dampers and friction dampers.

Design, fabrication and experiment of soft fingers with double-chamber based on layer jamming

Purpose The purpose of this paper is to propose a casting process for the production of double-chamber soft fingers, which avoids the problems of air leakage and fracture caused by multistep casting. This proposed method facilitates the simultaneous casting of the inflation chamber and the jamming chamber. Design/methodology/approach An integrated molding technology based on the lost wax casting method is proposed for the manufacture of double-chamber soft fingers. The solid wax core is assembled with the mold, and then liquid silicone rubber is injected into it. After cooling and solidification, the mold is stripped off and heated in boiling water, so that the solid wax core melts and precipitates, and the integrated soft finger is obtained. Findings The performance and fatigue tests of the soft fingers produced by the proposed method have been carried out. The results show that the manufacturing method can significantly improve the fatigue resistance and stability of the soft fingers, while also avoiding the problems such as air leakage and cracking. Originality/value The improvement of the previous multistep casting method of soft fingers is proposed, and the integrated molding manufacturing method is proposed to avoid the problems caused by secondary bonding.

Experimental investigations on the fatigue behavior of hybrid basalt/glass fiber epoxy composites

AbstractTo expand the applications of hybrid fiber composites in structural engineering applications, it is essential to study their fatigue behavior. The tensile and fatigue performance of unidirectional hybrid basalt/glass epoxy composites made with vacuum‐assisted resin infusion molding are investigated in this research. The sequencing influence on tensile properties was assessed using the two configurations of basalt/glass fiber epoxy hybrid fiber composites, namely GBBBG and BGBGB, having nearly equal volume fractions. According to the test results, hybrid fiber composites showed a positive hybrid effect on their tensile strength. Both hybrid layups showed higher tensile strengths (3.5% to 10.5%) than GFRPs and BFRPs. The GBBBG laminate has slightly higher fatigue resistance than BGBGB laminate under tension–tension (T–T) fatigue. Scanning electron microscopy (SEM) images verify the fatigue failure modes, which include fiber, matrix cracking, delamination, and debonding. The DMA analysis showed the lower adhesion efficiency of hybrid fiber composites, signifying lower damping properties.

Flaw sensitivity of bacterial cellulose hydrogel under monotonic and cyclic loadings

The presence of flaw in solid materials can lead to stress concentration, resulting in the reduction of rupture stress and stretchability of material. When the flaw is sufficiently smaller than a material-specific length, referred to as flaw sensitivity length, the material exhibits flaw insensitivity. The flaw sensitivity length is a critical material property that reflects how the material is sensitive or insensitive to crack. However, the impact of crack length on the load-bearing process of material remains an open problem. In this work, we characterize the flaw sensitivity of a stretchable material, bacterial cellulose hydrogel, under monotonic and cyclic loadings. Through fracture and fatigue tests, we first determine that the hydrogel exhibits high fracture toughness and fatigue resistance. We next characterize the flaw sensitivity of the hydrogel through two visualized experimental methods. Photoelasticity observation on the stress distribution in samples during loading shows that the samples with cracks below 2 mm exhibit uniform stress distribution during the deformation process, while those with cracks above 2 mm experience stress concentration at crack tip. Scanning electron microscope observation on the microstructure morphology of samples under fixed stretch shows that the samples with cracks below 2 mm exhibit uniform alignment of nanofibers, while those with cracks above 2 mm exhibit more intense alignment and even bundling of nanofibers at crack tip. Similar trends are observed in the samples under cyclic loading, where the transition length is also about 2 mm. Notably, the flaw sensitivity lengths obtained by the visualized methods agree well with that obtained by direct measurement of rupture stress and theoretical estimations under monotonic and cyclic loadings. The methods offer novel way to study the flaw sensitivity of materials, thereby contributing to the exploration of failure mechanisms.

Analysis of The Feasibility of Hydrogen Injection in Pipeline Gas Distribution Networks

Analysis of The Feasibility of Hydrogen Injection in Pipeline Gas Distribution Networks

Cyclic Fatigue Resistance of Edge File X7 and 2Shape Endodontic Systems: in vitro study.

Objectives: In order to test the resistance of rotary instruments to cyclic fatigue fracture and its importance in root canal preparationthe purpose of this study was to see how different tapers (4% and 6%) affected the cyclic fatigue resistance of the Edge File X7 and 2Shape endodontic systems at 45° and 60°canal curvature.Methods: Eighty NiTi files from two different systems (N= 40 each) were used; Group 1: Edge File X7, Group 2: 2Shape. each group was subdivided into four subgroups (N= 10 for each subgroup). The files were evaluated for cyclic fatigue resistance using a modified custom-made static model with 45°and 60° angles having a radius of 3mm and a diameter of 1.5 mm. Each file was rotated in a continuous rotation motion at 300 rpm with 1.2 N.cm torque for TS1, 300 rpm with 2.5 N.cm torque for TS2, and Edge file X7 was used at 300 rpm and 3 N.cm. Until it fractured. The time it took to separate the files was noted. Each file's number of cycles to failure was computed. A Kolmogorov-Smirnova normality test was done for all groups, and a two-way ANOVA was used to statistically examine the data.Results: The ranking of the groups from the highest to the lowest NCF was as follows: EdgeFile 4% 45 degrees (6594.00), EdgeFile 6% 45 degrees (6317.90), EdgeFile 4% 60 degrees (5682.00), EdgeFile 6% 60 degrees (2142.00), 2Shape 4% 45 degrees (2517.00), 2Shape 4% 60 degrees (535.90), 2Shape 6% 45 degrees (474.50), and 2Shape 6% 60 degrees (213.00). Conclusions: Edge File X7 showed better results than the 2Shape system. EdgeFile X7 4% at 45 degrees showed the highest NCF. The 2Shape system 6% at 60 degree that showed lowest NCF. As the canal curvature increased the NCF decreased. Taper 4% is better than taper 6%.

Modeling Bauschinger effect through the reversibility of dislocation slip in an Al–Cu–Li alloy

Al–Cu–Li alloys are promising lightweight materials for extensive applications in aerospace. As aerospace components often experience strain path changes during service, understanding the resulting Bauschinger effect is crucial for optimizing the fatigue resistance and performance of these alloys. This study investigates the role of T1 precipitates in the Bauschinger effect in AA2099. The presence of shearable T1 precipitates has been found to significantly influence the Bauschinger effect by reducing the strengthening effect of T1 precipitates during reverse straining. An analytical expression for slip reversibility has been derived to quantify this phenomenon, and a microstructure-based constitutive model has been developed to accurately predict the Bauschinger effect in AA2099.

Abrasive waterjet cutting of r‐GO infused magnesium fiber metal laminates: Experimental investigations and optimization through gorilla troops algorithm

AbstractLaminated metal‐composite structures, known as fiber metal laminates (FMLs), are modern lightweight materials extensively utilized in diverse industries such as aerospace and automotive manufacturing. These materials offer enhanced impact and fatigue resistance, making them invaluable for various applications. However, machining FMLs poses a challenge due to the occurrence of delamination and heterogenous in nature during conventional methods. Therefore, this study aims to investigate the quality characteristics such as kerf width, surface roughness and kerf taper of Magnesium based FMLs processed with an unconventional machining process namely abrasive water jet cutting (AWJC). These FMLs comprise alternately stacked kevlar/carbon fibers adhesively bonded with epoxy resin matrix filled with varying wt% of reduced graphene oxide (r‐GO), combined with AZ31B alloy sheet as the skin material. AWJC experiments were performed by varying the process parameters including waterjet pressure (275–325 MPa), stand‐off distance (2.5–3.5 mm), and cutting speed (600–800 mm/min) based on the box–behnken experimental design. The findings from the statistical analysis underscore the significant influences of stand‐off distance and waterjet pressure on kerf characteristics, while the inclusion of r‐GO is observed to notably affect the surface quality. In pursuit of enhancing cut quality, a multi‐response optimization was conducted employing the Gorilla Troops Optimization (GTO) algorithm. Comparative analysis with established metaheuristics like the gray wolf algorithm, dragonfly algorithm, and harmony search algorithm reveals GTO's superior performance across various metrics, including rapid convergence, diversity, and spacing values. Further, the cutting‐induced damages such as matrix plowing, fiber‐metal debonding and composite delamination were observed through microstructure analysis.Highlights Magnesium (AZ31B) fiber metal laminate comprising with various wt% of reduced graphene oxide was fabricated. Abrasive waterjet cutting of FMLs were performed based on box–behnken design experimental approach. Statistical analysis and influence of process parameters on the kerf width, surface roughness and kerf taper were investigated. Multi‐response optimization was carried out using metaheuristic‐based gorilla troops algorithm.

Surface roughness and cyclic fatigue resistance of a novel shaping system: An in-vitro study.

Recently developed Nickel-Titanium (NiTi) instruments with practical changes have resulted in safer instrumentation. In addition, topographical features on the file surface are a contributing factor to clinical durability. Therefore, this study aimed to investigate both the cyclic fatigue resistance and the roughness change of MTwo and Rotate instruments (VDW, Munich, Germany). Each instrument (n = 6/each group) was scanned with an atomic force microscopy prior to and after instrumentation. In addition, cyclic fatigue testing was conducted for each instrument (n = 11/each group) with stainless-steel blocks, including 45°-60°-90° degrees of curvature milled to the instruments' size. The roughness parameters increased for both systems after instrumentation (p<0.05). Both systems presented an increased roughness following instrumentation (p<0.05). The cyclic fatigue resistance was lowest at 90° for both systems (p<0.05), whereas the Rotate files presented a higher resistance than that of the Mtwo files (p<0.05). Compared to the Mtwo files, Rotate files presented better resistance, while the resistance decreased as the curvature increased.

Model reduction for fatigue life estimation of a welded joint driven by machine learning

In structural mechanics, the design of component assemblies is fundamental for ensuring structural integrity and durability. Fatigue, a common failure mode, particularly challenges the validation of welded joints' fatigue resistance. Various analytical and numerical methods estimate fatigue life but often involve costly processes requiring extensive parameter adjustments and software integration. This study applies machine learning (ML) for metamodeling of a complete finite element analysis and fatigue analysis workflow for estimating the fatigue life of welded joints, considering geometric characteristics, loading conditions, and weld classes. The comparison of the effect of learning database configuration for several regression estimators has led to a reduced model that provides design rules. Our findings demonstrate the significant potential of ML to streamline complex frameworks and accurately estimate the fatigue life of welded joints, advancing AI's application in mechanical engineering.

Wireless wearable system based on multifunctional conductive PEG-HEMA hydrogel with anti-freeze, anti-UV, self-healing, and self-adhesive performance for health monitoring

Polymer gels, such as hydrogels, have been widely applied in biomedicine, flexible electronics, and soft robotics. However, due to the complexity of application environments, preparing hydrogels that can maintain comprehensive performance under harsh conditions remains a challenge. Herein, based on polyethylene glycol (PEG) and water as a mixed solvent and using hydroxyethyl methacrylate (HEMA) as a monomer, a conductive dual-network PEG-HEMA hydrogel with anti-freezing, anti-ultraviolet, self-healing, and self-adhesive functions was prepared. The results show that PEG-HEMA hydrogel remained unfrozen even at -20°C, with tensile strength and elongation at break of 49.946 KPa and 529.7%, high resolution (able to measure strains as low as 0.2%), good sensitivity and linearity (GF=1.076, R2=0.999), fatigue resistance (over 1000 cycles), and long-term storage capability (over one week). Furthermore, a small wireless wearable strain sensor system was developed by integrating the hydrogel with a microcontroller, which is capable of monitoring various human motion and physiological signals in real time and exhibiting excellent sensing performance. This work provides a straightforward approach for multifunctional hydrogels, and it is expected to attract widespread attention and applications in fields such as electronic skin, human-machine interaction, and human health monitoring.

A short linear glucan nanocomposite hydrogel formed by in situ self-assembly with highly elastic, fatigue-resistant and self-recovery

Polyacrylamide (PAM) hydrogels are widely used in wide-ranging applications in biology, medicine, pharmaceuticals, and environmental sectors. However, achieving the requisite mechanical properties, fatigue resistance, self-recovery, biocompatibility, and biodegradability remains a challenge. Herein, we present a facile method to construct a nanocomposite hydrogel by integrating short linear glucan (SLG), obtained by waxy cornstarch debranching, into the PAM network through self-assembly. The resulting composite hydrogels with 10 % SLG content exhibited satisfactory stretchability (withstanding over 1200 % strain), along with maximum compressive and shear strengths of about 490 kPa and 39 kPa at 90 % deformation, respectively. This hydrogels demonstrated remarkable resilience and could endure repeated compression and stretching. Notably, the nanocomposite hydrogels with 10 % SLG content exhibited full stress recovery at 90 % deformation after 20 s, without requiring specific environmental conditions, achieving an energy dissipation recovery rate of 98 %. Meanwhile, these hydrogels exhibited strong adhesion to various soft and hard substrates, including skin, glasses, and metals. Furthermore, they maintain solid integrity at both 37 °C and 50 °C swelling equilibrium, unlike traditional PAM hydrogels, which exhibited softening under similar conditions. We hope that this PAM-SLG hydrogels will open up new avenues for the development of multifunctional electronic devices, offering enhanced performance and versatility.