Adhesive Bond Failure Research Articles

The bending of 3D-printed bio-inspired sandwich panels with wavy cylinder cores

Beetle Elytron Plates (BEPs) represent a new class of biomimetic sandwich cores with excellent mechanical properties inspired by the microstructure of the beetle elytra. The cores have a hexagonal centre-symmetric configuration with through-thickness cylinders in the unit cell. In this work, we describe the behaviour of sandwich panels with novel BEP core configurations possessing wavy cylinders under four-point bending tests. Full-scale simulations are also carried out to validate the experimental data. The results show that all the sandwich panels produced with face skins adhesively bonded have material failure earlier than the adhesive bond failure. BEPs with wavy cylinders have larger peak loads compared to those with straight cylinders, and all BEPs show higher peak loads than those of sandwich panels with classical hexagonal honeycombs. Additionally, all the BEPs exhibit an enhanced ductility compared to honeycomb sandwich panels.

Evaluating the Impact of Oxidation Heat Treatment and Dual Opaquing Techniques on Enhancing Metal-Ceramic Bond Strength.

This research aims to assess the impact of oxidation heat treatment (OHT) and dual opaquing techniques on enhancing the bond strength between metal and ceramic. Eighty rectangular patterns with dimensions of 0.5x3x25 mm (according to ISO 9693-2012) were fabricated in a custom-made silicon mold by using auto-polymerized pattern resin material. These rectangular patterns were cast using base metal alloys. The samples were split into two primary groups: group A, subjected to OHT, and group B, without oxidation treatment. Each primary group was then split up into subgroups according to the application of single layers (group A1, B1)or double layers (group A2, B2) of opaque porcelain.After pre-surface treatment and Ceramco 3 paste opaque application, dentin porcelain (Ceramco 3) wasapplied to the mid-region of the samples, followed by firing to achieve a standardized thickness. Flexural strength determination was conducted via a three-point bend test performed on the universal testing machine (UTM) (Instron Corp., Model 2519-107, USA), adhering to ISO standard 9693. Post-testing failure types were analyzed by morphological assessment of debonding surfaces via a scanning electron microscope (SEM). The statistical analysis was performed with SPSS version 16, incorporating ANOVA for intergroup analysis and independent t-tests for intragroup comparisons. Group A2 exhibited the highest mean flexural bond strength (P<0.05) at 41.85 MPawhen compared to group A1 at 37.60 MPa, group B2 at 35.47 MPa, and group B1 with the least mean flexural bond strength at 30.41 MPa. SEMobservations revealed cohesive bond failure for groups A1, A2, and B2and adhesive bond failure for groupsB1. It is evident that OHT and opaquing technique are important factors in determining the bond strength of ceramo-metal restorations. When combined, these techniques greatly increase the overall success and durability of metal-ceramic restorations, underscoring their significance in contemporary dental prostheses.

Promoting Adhesion of Natural Rubber/Styrene-Butadiene Rubber to Brass Using Vietnamese Natural Rubber-Based Adhesives

Abstract This study aimed to enhance the adhesion between brass and NR/SBR rubber sheets using solvent-based adhesives derived from Vietnamese natural rubber. The effects of silane coupling agents and iron nanoparticles on adhesion were investigated. (3-Aminopropyl) Triethoxysilane (APTES) and iron nanoparticles are incorporated into the adhesives at varying concentrations to enhance adhesion levels. The characteristics of the adhesive, such as viscosity, peel-off tensile strength, and the surface morphology of the adhesive bond failure, have been studied and evaluated. The research results demonstrated that as the APTES content added to the adhesives increases gradually, the peel strength between the NR/SBR and brass significantly improves. The highest peel strength value achieved was 5.27 N/mm at 25 phr APTES, representing a 974% increase compared to the sample without silane. The continued addition of iron nanoparticles to the adhesive further improves the peel tensile strength, reaching a maximum value of 5.93 N/mm at a nanoparticle content of 5 phr. This information will be crucial for developing practical applications for this type of adhesive.

A Novel Bio-Adhesive Based on Chitosan-Polydopamine-Xanthan Gum for Glass, Cardboard and Textile Commodities.

The escalating environmental concerns associated with petroleum-based adhesives have spurred an urgent need for sustainable alternatives. Chitosan, a natural polysaccharide, is a promising candidate; however, its limited water resistance hinders broader application. The aim of this study is to develop a new chitosan-based adhesive with improved properties. The polydopamine association with chitosan presents a significant increase in adhesiveness compared to pure chitosan. Polydopamine is synthesized by the enzymatic action of laccase from Trametes versicolor at pH = 4.5, in the absence or presence of chitosan. This pH facilitates chitosan's solubility and the occurrence of catechol in its reduced form (pH < 5.5), thereby increasing the final adhesive properties. To further enhance the adhesive properties, various crosslinking agents were tested. A multi-technique approach was used for the characterization of formulations. The formulation based on 3% chitosan, 50% polydopamine, and 3% xanthan gum showed a spectacular increase in adhesive properties when tested on glass, cardboard and textile. This formulation increased water resistance, maintaining the adhesion of a sample soaked in water for up to 10 h. For cardboard and textile, material rapture occurred, in mechanical tests, prior to adhesive bond failure. Furthermore, all the samples showed antiflame properties, expanding the benefits of their use. Comparison with commercial glues confirms the remarkable adhesive properties of the new formulation.

Digital image processing in the determination of glued wood joints behavior

The determination of the efficiency of adhesives applied in glued joints, through the analysis of the percentage of wood failure, is one of the main validation parameters for the quality of gluing techniques and adhesive. However, the subjectivity of the interpretation, performance, and visual acuity of the evaluators makes the methodology subjective. This research aimed to establish a method for evaluating the behavior of the glue line in glued joints, using freely available software and digital camera images. Shear samples of glued joints with polyvinyl acetate - PVAc, resorcinol formaldehyde - RF, and melamine formaldehyde - MF were evaluated using digital images obtained by a 16.1-megapixel camera. The images were pre-processed to enable vectorization in Inkscape software, version 1.1.2. Each image was vectorized and subjected to the measurement of the areas of the generated vector layers (glue line and wood). The validation process was performed by evaluating the accuracy of vectorization. Thus, the photograph of each sample and the vectorized image were imported into ImageJ software, version 1.53. To ensure the reliability of the proposed methodology, statistical analyses of the Kappa coefficient, global accuracy, user, and producer were applied. To evaluate the efficiency of the proposed method in relation to the conventional method provided in ASTM D5266-13, five evaluators analyzed the proportion of bond line and wood failure of the 10 samples submitted to the proposed methodology. Subsequently, a descriptive analysis of the data was carried out to evaluate the variability and subjectivity of the conventional analyses among the evaluators. It is noted that the proposed methodology achieved high efficiency in the analysis of the proportion of glue line and wood, and it can be assured by the accuracy tests performed. The research also showed that there was no agreement among the five evaluators using the conventional method. It is concluded that the proposed methodology meets the research objective, with high levels of accuracy, and confirms the subjectivity of the analyses performed with the conventional methodology. The results underscore the need for objective methodologies, employing computational techniques to reduce subjectivity in adhesive bond failure assessments, enhancing critical decisions in the selection of adhesives for industrial structural applications.

Caries affected disinfection using Phycocyanin activated by PDT, Holy Basil, and Ti-sapphire laser on adhesive bond strength, microleakage, and bond failure

AIMTo investigate the effect of different cavity disinfectants, Phycocyanin (PC), Ocimum Sanctum (OS), and Ti Sapphire Laser, on the bond integrity and microleakage of resin restorations. Material and method60 human mandibular molars were extracted and prepared based on ICDAS scores of 4 and 5. To obtain the CAD surface, a visual examination was supported by tactile sensation and a dye for caries detection. Samples were randomly allocated into 4 groups based on cavity disinfectants applied (n = 15). Group 1: Specimens disinfected with CHX, Group 2: Specimens disinfected with Ti sapphire laser, Group 3: Specimens disinfected with Phycocyanin activated by Photodynamic therapy, and Group 4: Specimens disinfected with OS. Following the disinfection of the CAD surfaces, composite bulk-fill restorative material was bonded to each specimen and all samples were subjected to thermocycling. Ten samples from each group underwent SBS testing performed on a universal testing machine. Five samples were subjected to a microleakage analysis. ResultThe maximum microleakage scores were displayed by Group 3: PC (0.521 nm) treated specimens. Whereas, and minimum microleakage was exhibited by Group 4: OS (0.471 nm). Group 4: OS (23.06±0.21 MPa) treated group displayed the maximum bond scores of resin adhesive to the CAD surface. However, Group 3: PC (21.67±0.24 MPa) treated specimens exhibited the lowest bond scores. Failure mode analysis revealed that among all the investigated groups the predominant type of failure was cohesive failure i.e., Group 1 (80%), Group 2 (80%), Group 3 (70%), and Group 4 (90%). ConclusionOcimum Sanctum, Phycocyanin activated by Photodynamic therapy, and Ti-sapphire laser for disinfection of caries-affected dentin have shown promise in terms of improved bond strength and reduced microleakage

Improving adhesive behavior of fiber reinforced composites by incorporating electrospun Polyamide-6,6 nanofibers in joining region

Adhesive joining of fiber reinforced polymer (CFRP) composite components is demanded in various industrial applications. However, the joining locations frequently suffer from adhesive bond failure between adhesive and adherent. The aim of the present study is improving bonding behavior of adhesive joints by electrospun nanofiber coatings on the prepreg surfaces that have been used for composite manufacturing. Secondary bonding of woven and unidirectional CFRP parts was selected since this configuration is preferred commonly in aerospace practices. The optimum nanofiber coating with a low average fiber diameter and areal weight density is succeed by studying various solution concentrations and spinning durations of the polyamide-6.6 (PA 66) electrospinning. We obtained homogeneous and beadles nanofiber productions. As a result, an average diameter of 36.50 ± 12 nm electrospun nanofibers were obtained and coated onto the prepreg surfaces. Prepreg systems with/without PA 66 nanofibers were hot pressed to fabricate the CFRP composite laminates. The single-lap shear test coupons were prepared from the fabricated laminates to examine the effects of PA 66 nanofibers on the mechanical properties of the joint region of the composites. The single-lap shear test results showed that the bonding strength is improved by about 40% with minimal adhesive use due to the presence of the electrospun nanofibers within the joint region. The optical and SEM images of fractured surfaces showed that nanofiber-coated joints exhibited a coherent failure while the bare surfaces underwent adhesive failure. The PA66 nanofibers created better coupling between the adhesive and the composite surface by increasing the surface area and roughness. As a result, electrospun nanofibers turned adhesive failure into cohesive and enhanced the adhesion performance composite joints substantially.

Investigation on the structural failure behaviour of pultruded circular tubular GFRP multiplanar truss bridges with non-metallic connections through finite element modelling

The finite element (FE) method was used to investigate the failure of member connections of five glass fibre-reinforced polymer (GFRP) multiplanar truss bridges (MTB) with non-metallic connections. Three-dimensional FE models for the MTBs were developed and validated against previous experimental results and were accompanied by multiple parametric studies. Adhesive failure of the brace occurs progressively around the perimeter of the brace and GFRP laminate wrapping failure was not observed before adhesive bond failure of the brace. Furthermore, the failure sequence of the GFRP laminate layer and the adhesive bonding between the brace and chord was found to be dependent on the brace wall thickness. Extent of the predicted fibre tensile rupture of the GFRP laminate was greater for cement mortar grouted GFRP rods than its non-GFRP grouted counterpart.

Simulation of buckling-driven progressive damage in composite wind turbine blade under extreme wind loads

Wind turbine blades are continuously upscaled in size to meet the increasing demand of low cost renewable energy. The larger and slender blades with reduced mass are susceptible to large-deflection bending and instability during extreme wind gusts. The loading can induce interactive damage modes such as adhesive bond failure and composite skin damage progressively degrading the blade structural performance. The structural deformation and instability as well as progressive damage in composite blade is analyzed by developing finite element (FE) models using ANSYS software. First, a geometric nonlinear FE analysis of the 3D blade is performed to predict its deflection and regions of high stresses. The results demonstrated that high compressive stresses in the blade suction side trigger local skin buckling; thus initiating debonding of weak adhesive interface joint between skin and spar combined with skin damage. Subsequently, the interactive buckling-driven skin-spar debonding and composite skin damage in the identified region are analyzed through a submodel using cohesive zone model (CZM) as well as continuum damage mechanics (CDM) based progressive failure analysis, respectively, through a user-defined material subroutine. The results indicated that buckling-driven debonding of adhesive interface between skin and spar was primary damage mode leading to progressive failure of the blade composite skin. Consequently, the blade ultimate load carrying-ability was governed by coupled adhesive debonding and progressive skin damage phenomena, which is in good agreement with published experimental results. The developed simulation approach is capable to efficiently analyze the interactive buckling-induced interface damage as well as progressive failure of composite blade structure. In this work, modelling of interaction between interface debonding and skin damage, based on the CZM and CDM scheme, is a novel methodology for progressive damage analysis of blade under extreme loading.

Service Life of Adhesive Bonds under Cyclic Loading with a Filler Based on Natural Waste from Coconut Oil Production.

The research is focused on the evaluation of mechanical properties of adhesive bonds with a composite layer of adhesive to increase their service life (safety) under cyclic loading of different intensities. Cyclic loading represents a frequent cause of adhesive bond failure and, thus, a reduction in their service life. Waste from the production of coconut oil, that is, coconut shells in the form of particles, was used as a filler. Coconut shells are in most cases incinerated or otherwise uselessly incinerated, but they can also be used as a natural filler. Cyclic loading (quasi-static tests) was performed for 1000 cycles in two intensities, that is, 5–30% (157–940 N) of maximum force and 5–50% (157–1567 N) of maximum force. The results of the experiment showed a positive effect of the added filler, especially at an intensity of 5–50%, when the service life of adhesive bonds with a composite adhesive layer (AB10, AB20, AB30) increased compared to adhesive bonds without added AB0 filler, which did not withstand the given intensity. A more pronounced viscoelastic behavior of adhesive bonds was demonstrated at an intensity of 5–50% between the 1st and 1000th cycle. SEM analysis showed reduced wetting of the filler and matrix and delamination due to cyclic loading.

A constant-frequency ultrasonic phase method for monitoring imperfect adherent/adhesive interfaces

A primary mechanism of adhesive bond failure is a degradation of the adherent/adhesive interfacial stiffness from unwanted contamination or exposure to those environmental factors, which reduce adhesion quality. Substantial research has been conducted on the assessment of adhesively bonded structures and the detection of “kissing” bonds. Advanced ultrasonic assessment methods to interrogate bonded joints and measure interfacial stiffness using a distributed spring interface model have been developed. Amplitude-based ultrasonic methods have traditionally been used in adhesive bond quality assessment, but recent advancements in ultrasonic phase measurements allow for high measurement resolution with low-uncertainty. In this work, an ultrasonic phase technique for the monitoring of adhesively-bonded interfaces is demonstrated. Constant frequency measurements are obtained from the ultrasonic phase of the reflection coefficient from the adhesive bond with a glass adherent, where the degree of cure is controlled by exposure to ultraviolet light. A peak in the phase of the reflection coefficient, as predicted by the interfacial spring model, is measured experimentally. It is shown that the peak phase predicts the interfacial stiffness when some frequency dependent threshold value is crossed. With knowledge of the acoustic impedances of both materials at the interface, the interfacial stiffness is determined by an inverse algorithm involving measurements of ultrasonic phase shifts of bonded joint reflections. By monitoring the interface of bonded structures and coatings, this method permits a nondestructive inspection of bond strength from structural construction through its service life.

Analysis of model and data uncertainties for the failure of adhesive bonds in composite materials

AbstractThis study has been performed within the research project MuScaBlaDes “Multi‐scale failure analysis with polymorphic uncertainties for optimal design of rotor blades" as part of the DFG Priority Programme (SPP 1886) “Polymorphic Uncertainty Modelling for the Numerical Design of Structures" started in 2016. Stress concentrations in adhesive bonds of a composite structure influence the structural integrity and can initiate the overall failure. Their numerical prediction always depends on present model and data uncertainties. For that, the development of an efficient numerical model and the role of the quality of data is presented. The assessment of the numerical models is shown by comparing predicted strains to measured ones.

Damage Mechanism Based Approach to the Structural Health Monitoring of Wind Turbine Blades

A damage mechanism based approach to the structural health monitoring of wind turbine blades is formulated. Typical physical mechanisms of wind turbine blade degradation, including surface erosion, adhesive fatigue, laminate cracking and in some cases compressive kinking and failure are reviewed. Examples of a local, damage mechanism based approach to the structural health monitoring of wind turbine blades are demonstrated, including the monitoring of leading edge erosion of wind turbine blades, adhesive bond failure, plydrop delamination, static and dynamic plydrop tests, and bolt and laminate fatigue. The examples demonstrate the possibilities of monitoring specific damage mechanisms, and specific localizations of wind turbine blades.

Emergence of aortic aneurysms due to failure of adhesive bonds between proteoglycans

AbstractAortic aneurysms are a common disease among older patients. Aneurysm ruptures cause more than 150 000 deaths annually [2]. One of the main risk factors which lead to the abnormal enlargements of vessels (&gt;150% of original size) is arterial hypertension.This contribution presents a modeling approach, where the cyclic loading of the artery caused by the blood pressure leads to fatigue inside the arterial wall. The arterial wall is considered as a composite material, where a matrix (ground substance) is reinforced by collagen fibers consisting of fibrils connected by proteoglycan (PG) bridges. These PG bridges support interfibrillar sliding leading to lower fibril stretch [6]. Molecular adhesive bonds rupture under any pulling force if the force is held sufficiently long enough [1]. This rupturing over time leads to a decrease in the density of PG bridges, higher stretches in the fibrils, more damage inside the fibrils and finally to fatigue of the soft tissue which causes the abnormal enlargement.Finally the model is compared against experimental data of uniaxial tension tests and used in a FEM simulation to study the emergence of aortic aneurysms under arterial hypertension. (© 2017 Wiley‐VCH Verlag GmbH &amp; Co. KGaA, Weinheim)

Comparison of porcelain bond strength of different metal frameworks prepared by using conventional and recently introduced fabrication methods

Statement of problemMost studies evaluating dental laser sintering systems have focused on the marginal accuracy of the restorations. However, the bond strength at the metal-ceramic interface is another important factor that affects the survival of restorations, and currently, few studies focus on this aspect. PurposeThe purpose of this in vitro study was to compare the porcelain bond strength of cobalt-chromium (Co-Cr) metal frameworks prepared by using the conventional lost-wax technique, milling, direct metal laser sintering (DMLS), and laser cusing, a direct process powder-bed system. Material and methodsA total of 96 metal frameworks (n=24 in each group) were prepared by using conventional lost-wax (group C), milling (group M), DMLS (group LS), and direct process powder-bed (group LC) methods according to International Organization for Standardization standard ISO 9693-1. After porcelain application, a 3-point bend test was applied to each specimen by using a universal testing machine. Data were statistically analyzed using 1-way ANOVA and Tukey honest significant difference tests (α=.05). Failure types at the metal-ceramic interfaces were examined using stereomicroscopy. Additionally, 1 specimen from each group was prepared for scanning electron microscopy analysis to evaluate the surface topography of metal frameworks. ResultsThe mean bond strength was 38.08 ±3.82 MPa for group C, 39.29 ±3.51 MPa for group M, 40.73 ±3.58 MPa for group LS, and 41.24 ±3.75 MPa for group LC. Statistically significant differences were observed among the 4 groups (P=.016). All groups, except for LS, exhibited adhesive and mixed type bond failure. ConclusionsBoth of the laser sintering methods were found to be successful in terms of metal-ceramic bond strength.

Comparison of two different debonding techniques in orthodontic treatment.

The purpose of this research is to investigate whether and how the adhesive bond failure site varied in relation to the material used for the orthodontic bonding and debonding technique applied. Two different methods of orthodontic debonding were included in our survey; cutters for orthodontics and debonding plier. Three different materials for the adhesion of the bracket: composite light curing, self-curing composite and glass ionomer cement. The remaining amount of adhesive on the tooth surface is an important parameter that gives information on how the location of the posting site varied during the debonding. 60 dental elements, maxillary and mandibular, previously extracted for orthodontic reasons, as well as periodontal, were included in our research. We investigated a possible significant correlation between different variables (debonding technique and materials for membership) and the ARI index. The use of orthodontic cutters or debonding pliers does not affect the adhesive bond failure site and both techniques have a tendency to leave a significant amount of adhesive on the surface enamel. In the resin-reinforced glass ionomer cements, detachment occurs at the interface enamel-adhesive and this pattern of detachment increases the risk of the enamel damage during debonding. In both types of composite resins (photopolymerizable or self-curing), the detachment occurs at the interface bracketing adhesive. In this case the amount of remaining adhesive material on the tooth must be removed with further methods, which in addition, increase the risk of iatrogenic injury as well as the working hours.

Failure of adhesive bonds between proteoglycans causes viscoelasticity of soft tissues

AbstractSoft tissues can be considered as a composite material where a matrix (ground substance) is reinforced by collagen fibers. These fibers consist of fibrils, which are connected by proteoglycan (PG) bridges. The time‐dependent properties of soft tissues appear to be mainly caused by proteoglycans [3]. This contribution presents a modeling approach where damage in the PG bridges arises due to the failure of the covalent bonds between two proteoglycans. The breakage of covalent bonds is reversible over time and incorporated using a healing formulation. A high PG density supports interfibrillar sliding and hence leads to a lower fibril stretch [8]. Accordingly, the damage propagation in PG bridges leads to a higher stretch in the fibrils and therefore to a stiffer material response. The strain energy of the fibrils is based on the response of single tropocollagen molecules and takes both, an entropic and an energetic regime into account [5]. Finally, the model is compared against experimental data available in the literature. (© 2016 Wiley‐VCH Verlag GmbH &amp; Co. KGaA, Weinheim)

A contact problem for viscoelastic bodies with inertial effects and unilateral boundary constraints

We consider a viscoelastic body occupying a smooth bounded domain $\Omega\subset \mathbb{R}^3$ under the effect of a volumic traction force g. The macroscopic displacement vector from the equilibrium configuration is denoted by u. Inertial effects are considered; hence, the equation for u contains the second-order term utt. On a part ΓD of the boundary of Ω, the body is fixed and no displacement may occur; on a second part ΓN ⊂ ∂Ω, the body can move freely; on a third portion ΓC ⊂ ∂Ω, the body is in adhesive contact with a solid support. The boundary forces acting on ΓC due to the action of elastic stresses are responsible for delamination, i.e., progressive failure of adhesive bonds. This phenomenon is mathematically represented by a non-linear ordinary differential equation settled on ΓC and describing the evolution of the delamination order parameter z. Following the lines of a new approach outlined in Bonetti et al. (2015, arXiv:1503.01911) and based on duality methods in Sobolev–Bochner spaces, we define a suitable concept of weak solution to the resulting system of partial differential equations. Correspondingly, we prove an existence result on finite-time intervals of arbitrary length.

Behavior and failure of adhesive bonds in pin fin heat sinks using cohesive zone model

Adhesive bonding is a versatile material joining method that tends to distribute the load over the bonded area and provide more flexibility in selecting the base material without worrying about the joining process and its effects. To improve the performance of heat sinks, polymer composite pin fin are used to improve the thermal conductivity. Adhesives are usually used in bonding composite fins to their metal base plate. In this work we provide a methodology for estimating the fatigue life of the adhesive joint. A thermo-mechanical cohesive zone model (CZM) is used at the interfaces to measure the softening of the bond under thermal cyclic loading which in turn decreases the critical stress for failure. A summary of the fatigue crack initiation (FCI) life prediction model is presented before a qualitative study is performed to estimate the effect of convection environment on the life and behavior of the adhesive bond.

Push-out bond strength of root fillings made with C-Point and BC sealer versus gutta-percha and AH Plus after the instrumentation of oval canals with the Self-Adjusting File versus WaveOne.

To compare the push-out bond strength exhibited by root fillings performed with either C-Point and Endosequence® BC sealer™ (BC Sealer) or gutta-percha and AH Plus® after the instrumentation of oval canals with either the Self-Adjusting File (SAF) System or WaveOne (WO) reciprocating file. Eighty extracted premolars were selected and divided randomly into the following four groups (n = 20): group 1, SAF instrumentation and filling using gutta-percha and AH Plus sealer; group 2, SAF instrumentation and C-Point and BC sealer filling; group 3, WO instrumentation and filling using gutta-percha and AH Plus sealer; and group 4, WO instrumentation and filling with C-Point and BC sealer. Sodium hypochlorite (5.25%) and EDTA (17%) were used as irrigants for all groups. After the sealer was set completely, the teeth were prepared for micro push-out assessment using 1.0-mm-thick root slices. Loading was performed with a universal testing machine at a speed of 0.5 mm min(-1) . Two-way anova and Student's t-test for pairwise comparisons were used to compare groups. All specimens filled with C-Point and BC sealer were associated with significantly higher push-out bond strength compared with gutta-percha and AH Plus sealer (P < 0.001). The bond strength was higher for the coronal and apical samples of the C-Point/BC sealer/SAF group (6.6 ± 0.3 and 3.2 ± 0.3 MPa) versus those of the gutta-percha/AH Plus/WO group (4.8 ± 0.3 and 1.8 ± 0.3 MPa), by 38% and by 80% in the coronal and apical parts, respectively (P < 0.001, P < 0.0001). Adhesive bond failure was more common in the WaveOne-instrumented group in general and in the buccal and lingual recesses in this group in particular. In oval canals, the instrument used and the root filling material significantly affected the push-out values of root fillings. The highest value was recorded in oval root canals instrumented with the SAF System and filled with C-Point and BC sealer, whereas the lowest strength was noted in oval canals instrumented with WaveOne and filled with gutta-percha and AH Plus sealer.