Flow Experiments Research Articles

Flow Experiment with Conductive Liquid Metal Using Lorenz Force for Developing High-Performance Electric Casting System

Flow Experiment with Conductive Liquid Metal Using Lorenz Force for Developing High-Performance Electric Casting System

Insight into interactive synergy of MoS2@CoNC for peroxymonosulfate activation: From bath experiments to continuous flow experiments

Insight into interactive synergy of MoS2@CoNC for peroxymonosulfate activation: From bath experiments to continuous flow experiments

Enhanced Cu-EDTA degradation with trace Cu(II) in limestone via activating PMS

Effective removal of heavy metal complexes from contaminated water remains a challenging task. In this work, a limestone/PMS system was constructed for the efficient degradation of Cu-EDTA. Under the conditions of 3.0 g/L limestone and 1.0 mM PMS, the degradation efficiency of 10.0 mg/L Cu-EDTA reached 99.0 % in 60 min, and the removal efficiency of Cu ions approached 50.0 %. The main active specie revealed by quenching and EPR experiments was the singlet oxygen (1O2). Interestingly, Trace amounts of Cu(II) in limestone react with PMS enhancing the degradation of Cu-EDTA. The results of the HPLC-MS analysis showed that the reactive species attacked the Cu–O and Cu–N bonds, as well as triggered a decarboxylation process, resulting in the decomposition of Cu-EDTA into six intermediates. Meanwhile, SEM and XPS analyses revealed that Cu ions released during the degradation of Cu-EDTA are deposited on the limestone surface as Cu(OH)2 and Cu2(OH)2CO3. In addition, the initial pH and co-existing ions have a weak effect on the system. Finally, a one-month continuous flow experiment showed that the degradation efficiency of Cu-EDTA was about 95.0 % and the removal efficiency of Cu ions was 40.0 %. In conclusion, this study provides a new approach for the destruction of metal complexes and the removal of heavy metals.

Numerical simulation of the temporal and spatial evolution of sandstone pore type reservoir damage types and severity

During the oilfield development process, various factors can cause different types of reservoir damage, leading to reduced oil well production or even shutdown, and decreased water injection capacity in water wells, resulting in significant economic losses for the oilfield. However, formation damage control measures must be based on the quantitative diagnosis of the types and degrees of reservoir damage. This paper establishes a spatiotemporal evolution numerical model for 12 common types of damage during the oil and gas exploration and development process, based on the material balance theory and Fick’s diffusion law in reservoir damage processes. This model achieves numerical simulation of the degree of various reservoir damage types in different spatiotemporal domains. The overall damage degree of a specific well’s evolution with time and space is further simulated in simple superposition way. The sequential core flow experiment was carried out in the laboratory, and then compared with the calculation results. The accuracy is above 90%. Finally, using field test data, the simulation results show a 95% or higher degree of agreement with the actual field measurements, proving that the reservoir damage spatiotemporal evolution quantitative simulation technology established in this paper has high accuracy and practicality.

Lateral Shear Stress Calculation Model Based on Flow Velocity Field Distribution from Experimental Debris Flows

AbstractDebris flows continuously erode the channel downward and sideways during formation and development, which changes channel topography, enlarges debris flow extent, and increases the potential for downstream damage. Previous studies have focused on debris flow channel bed erosion, with relatively little research on lateral erosion, which greatly limits understanding of flow generation mechanisms and compromises calibration of engineering parameters for prevention and control. Sidewall resistance and sidewall shear stress are key to the study of lateral erosion, and the distribution of the flow field directly reflects sidewall resistance characteristics. Therefore, this study has focused on three aspects: flow field distribution, sidewall resistance, and sidewall shear stress. First, the flow velocity distribution and sidewall resistance were characterized using laboratory debris flow experiments, then a debris flow velocity distribution model was established, and a method for calculating sidewall resistance was developed based on models of flow velocity distribution and rheology. A calculation method for the sidewall shear stress of debris flow was then developed using the quantitative relationship between sidewall shear stress and sidewall resistance. Finally, the experiment was validated and supplemented through numerical simulations, enhancing the reliability and scientific validity of the research results. The study provides a theoretical basis for the calculation of the lateral erosion rate of debris flows.

Unveiling synergistic enhancement mechanism of nitrogen removal in surface flow constructed wetlands: Utilizing iron scraps and elemental sulfur as integrated electron donors

Lacking electron donors generally causes poor denitrification performance in constructed wetlands (CWs). In this study, iron scraps (ISs) and elemental sulfur (S0) were employed as electron donors in different surface flow constructed wetlands (SFCWs): control (C-SF), ISs added (Fe-SF), S0 added (S-SF), and ISs and S0 combined (Fe + S-SF) to investigate the performance and mechanism of nitrogen (N) removal through continuous flow and batch experiments. The impact of hydraulic retention times (HRTs) and temperatures on N removal was explored. The combined use of ISs and S0 significantly improved nitrate (NO3− -N) removal in Fe + S-SF compared to the other SFCWs. During the 3-d HRT at 25 °C, the average NO3− -N removal efficiency in Fe + S-SF reached the highest value of 71.66 ± 12.54%, reducing NO3− -N concentrations from 12.03 mg/L to 3.47 mg/L. The results of the batch experiments revealed an N removal pattern that aligned with the findings of the continuous flow experiment. The microbial community analysis revealed a selective enrichment of key functional genera (e.g., Ferritrophicum and Dechloromonas), contributing to enhanced N removal in Fe + S-SF. These findings suggest that the synergistic use of ISs and S0 can achieve better denitrification efficiency and potentially be utilized for enhanced N removal from low C/N wastewater.

A critical state μ(I)-rheology model for cohesive granular flows

The dynamic behaviour of granular media can be observed widely in nature and in many industrial processes. Yet, the modelling of such media remains challenging as they may act with solid-like and fluid-like properties depending on the rate of the flow and can display a varying apparent friction, cohesion and compressibility. Over the last two decades, the $\mu (I)$ -rheology has become well established for modelling granular liquids in a fluid mechanics framework where the apparent friction $\mu$ depends on the inertial number $I$ . In the geo-mechanics community, modelling the deformation of granular solids typically relies on concepts from critical state soil mechanics. Along the lines of recent attempts to combine critical state and the $\mu (I)$ -rheology, we develop a continuum model based on modified cam-clay in an elastoplastic framework which recovers the $\mu (I)$ -rheology under flow. This model permits a treatment of plastic compressibility in systems with or without cohesion, where the cohesion is assumed to be the result of persistent inter-granular attractive forces. Implemented in a two- and three-dimensional material point method, it allows for the trivial treatment of the free surface. The proposed model approximately reproduces analytical solutions of steady-state cohesionless flow and is further compared with previous cohesive and cohesionless experiments. In particular, satisfactory agreements with several experiments of granular collapse are demonstrated, albeit with shear bands which can affect the smoothness of the surface. Finally, the model is able to qualitatively reproduce the multiple steady-state solutions of granular flow recently observed in experiments of flow over obstacles.

Acceleration is the key to drag reduction in turbulent flow

A turbulent pipe flow experiment was conducted where the surface of the pipe was oscillated azimuthally over a wide range of frequencies, amplitudes, and Reynolds numbers. The drag was reduced by as much as 35%. Past work has suggested that the drag reduction scales with the velocity amplitude of the motion, its period, and/or the Reynolds number. Here, we find that the key parameter is the acceleration, which greatly simplifies the complexity of the phenomenon. This result is shown to apply to channel flows with spanwise surface oscillation as well. This insight opens potential avenues for reducing fuel consumption by large vehicles and for reducing energy costs in large piping systems.

Efficacy for aspiration prevention through thickening of liquid foods evaluated using a swallowing model apparatus

Abstract An apparatus simulating the swallowing process of liquid foods was constructed using a flow channel. In the channel, a circular cylindrical obstruction was fixed to serve as an epiglottis in the mesopharynx. The apparatus was designed with an adjustable gate for flow control to represent the processes of healthy swallowing and dysphagia. The parameters considered were the holding time and flow resistance controlled by the gate, which were assumed to indicate the swallowing reflex and power, respectively. When a Newtonian liquid with relatively low viscosity was used, the flow experiment performed using the apparatus under conditions of shorter holding time and larger flow resistance successfully reproduced a phenomenon similar to aspiration in a patient with dysphagia. In addition to a Newtonian liquid with high viscosity, non-Newtonian liquids thickened to various concentrations using commercially available thickeners were used. In flow experiments with these test liquids, the efficacy for aspiration prevention was inferred based not only on the viscosity of the liquid but also its elasticity, depending on its viscosity.

Study on increasing polymer gel strength with Janus nanoparticles and its feasibility in profile control and water plugging

In formations subjected to prolonged flooding, dominant channels are formed in high permeability layers, thereby reducing the displacement efficiency in medium- and low-permeability layers. In this study, the Janus synthesis method was employed to produce Janus Nano-TiO2 with a particle size range of 60–120 nm and superior dispersion properties. These nanoparticles were subsequently combined with polyacrylamide to formulate a high-strength polymer nano-gel for water plugging applications. The successful synthesis of the material was confirmed through FTIR and TGA. Gelation experiments indicated that the gelation strength and time augmented significantly with the increased addition of Janus-T6. Conversely, an increase in temperature or salinity resulted in a reduction of both gelation strength and time. Rheological experiments demonstrated a decrease in polymer viscosity with rising shear rates or temperatures, revealing significant shear thinning behavior in the water-plugging agent solution. System viscosity increased with more Janus-T6. Flow experiments revealed decreasing resistance coefficients at higher permeabilities, while all cores exhibited plugging rates above 85%. Additionally, the breakthrough pressure continuously rose with the increased addition of Janus-T6. Ultimately, displacement experiments indicated a 22.83% increase in the recovery rate after employing PNG plugging followed by secondary water flooding, compared to primary water flooding alone.

Development and Experimental Study of Supercritical Flow Payload for Extravehicular Mounting on TZ-6.

This paper provides a detailed description of the development and experimental results of the supercritical flow experiment payload carried on the TZ-6 cargo spacecraft, as well as a systematic verification of the out-of-cabin deployment experiment. The technical and engineering indicators of the payload deployment experiment are analyzed, and the functional modules of the payload are shown. The paper provides a detailed description of the design, installation location, size, weight, temperature, illumination, pressure, radiation, control, command reception, telemetry data, downlink data, and experimental procedures for the out-of-cabin payload in the extreme conditions of space. The paper presents the annular liquid surface state and temperature oscillation signals obtained from the space experiment and conducts ground matching experiments to verify the results, providing scientific references for the design and condition setting of space experiments and comparisons for the experimental results to obtain the flow field structure under supercritical conditions. The paper provides a specific summary and discussion of the space fluid science experiment project, providing useful references for future long-term in-orbit scientific research using cargo spacecraft.

Numerical Simulation of Gas Atomization and Powder Flowability for Metallic Additive Manufacturing

The quality of metal powder is essential in additive manufacturing (AM). The defects and mechanical properties of alloy parts manufactured through AM are significantly influenced by the particle size, sphericity, and flowability of the metal powder. Gas atomization (GA) technology is a widely used method for producing metal powders due to its high efficiency and cost-effectiveness. In this work, a multi-phase numerical model is developed to compute the alloy liquid breaking in the GA process by capturing the gas–liquid interface using the Coupled Level Set and Volume-of-Fluid (CLSVOF) method and the realizable k-ε turbulence model. A GA experiment is carried out, and a statistical comparison between the particle-size distributions obtained from the simulation and GA experiment shows that the relative errors of the cumulative frequency for the particle sizes sampled in two regions of the GA chamber are 5.28% and 5.39%, respectively. The mechanism of powder formation is discussed based on the numerical results. In addition, a discrete element model (DEM) is developed to compute the powder flowability by simulating a Hall flow experiment using the particle-size distribution obtained from the GA experiment. The relative error of the time that finishes the Hall flow in the simulation and experiment is obtained to be 1.9%.

Micro-scale flow simulation study of low-yield wells in tight gas reservoirs

Abstract The mechanism of gas-water flow in reservoirs has traditionally been characterized macroscopically based on flow experiments, but the microscopic mechanisms of gas-water flow in porous media cannot be precisely described experimentally. This paper categorizes low-yield gas wells into Types I, II, and III. With microscopic visualization principles, three different types of core thin-section photos were selected to construct a pore structure model, allowing for micro-scale flow simulation to examine micro-scale percolation patterns in various types of low-yield gas well reservoirs. The results show that there is a shorter displacement time in Type I reservoirs compared to Type II and III reservoirs which exhibit more pronounced fingering phenomena.

Fast Spatiotemporal Sequence Graph Convolutional Network-based transient flow prediction around different airfoils

A novel Spatiotemporal Sequence Graph Convolutional Network (ST-SGCN) data-driven model is proposed to predict transient fluid dynamics around airfoils using complex and unstructured flow field data, with the aim of reducing dimensions and expediting predictions. Graph Neural Networks directly interact with the flow field grid, capturing spatiotemporal physical features of grid nodes and their interconnections, while eliminating the need for complex preprocessing steps. The ST-SGCN model integrates a Graph Convolutional Network and a Graph Attention Network with a Deep Recurrent Neural Network that uses a Gate Recurrent Unit as the kernel, adeptly extracting spatial and temporal physical features of the flow field to accurately predict transient flow states. Preliminary airfoil flow experiments demonstrated the model's ability to continuously predict transient flow fields, achieving an average accuracy of 97% for both velocity and pressure field predictions, with a maximum error of approximately 10% in the testing dataset. Further experiments, varying angles of attack, airfoils, and Reynolds numbers, demonstrated the model's generalizability, extensibility, and adaptability, with prediction errors below 5% and a speedup of over 20 times.

Efficient one-pot tandem C-C formation reaction catalyzed by a multi-functionalized polyacrylonitrile fiber catalyst

A simple and straightforward method has been proposed in this work to construct a multi-functionalized polyacrylonitrile fiber catalyst containing carboxylic acid, tertiary amine, and quaternary ammonium salt to enable series one-pot C-C bond formation in water. The fiber catalyst was prepared from polyacrylonitrile fiber using a two-step method and characterized using various detection techniques. Furthermore, the activity of multi-functional synergistic catalysts can be controlled by adjusting the ratio of acid and base. It is noteworthy that the polyacrylonitrile fiber catalyst with an acid-base ratio of 3:1 (PANF-ABNCl3/1) exhibited superior catalytic activity and high yield in a variety of C-C generation reactions. Additionally, the PANF-ABNCl3/1 catalyst demonstrated exceptional recyclability (at least 10 times) and performed well in scale-up (7.4g, 96%) and continuous flow experiments (can be used continuously for 7 × 24h) using kettle and tubular fixed bed reactor respectively. These findings suggest that the PANF-ABNCl3/1 catalyst holds promise for industrialization.

Capsule polymer flooding for enhanced oil recovery

To solve the problems of shear degradation and injection difficulties in conventional polymer flooding, the capsule polymer flooding for enhanced oil recovery (EOR) was proposed. The flow and oil displacement mechanisms of this technique were analyzed using multi-scale flow experiments and simulation technology. It is found that the capsule polymer flooding has the advantages of easy injection, shear resistance, controllable release in reservoir, and low adsorption retention, and it is highly capable of long-distance migration to enable viscosity increase in deep reservoirs. The higher degree of viscosity increase by capsule polymer, the stronger the ability to suppress viscous fingering, resulting in a more uniform polymer front and a larger swept range. The release performance of capsule polymer is mainly sensitive to temperature. Higher temperatures result in faster viscosity increase by capsule polymer solution. The salinity has little impact on the rate of viscosity increase. The capsule polymer flooding is suitable for high-water-cut reservoirs for which conventional polymer flooding techniques are less effective, offshore reservoirs by polymer flooding in largely spaced wells, and medium to low permeability reservoirs where conventional polymers cannot be injected efficiently. Capsule polymer flooding should be customized specifically, with the capsule particle size and release time to be determined depending on target reservoir conditions to achieve the best displacement effect.

Study on flow regime characteristics in 3×3 rod bundle channels based on wire mesh sensor

Abstract The characteristics and evolution of two-phase flow are of critical importance to the safety of pressurized water reactors. Based on the double-layer wire mesh sensors in this paper, the air-water two-phase flow experiment of the 3×3 rod bundle channels is carried out at room temperature and pressure. The results show that the critical bubble diameter range for the reversal of lateral lift direction is 4 to 5.8 mm. In addition, the time-averaged void fraction for bubbly flow reveals a wall peak distribution at lower superficial gas velocities and shifts to a core peak as these velocities increase. For cap flow, the cross-distribution of cap bubbles within adjacent subchannels triggers large-scale mixing of the liquid phase between adjacent subchannels. For slug flow, large-sized bubbles develop along the axis and cross subchannel gaps to aggregate into slug-shaped bubbles, with a more pronounced distribution of the central peak of void fraction. The drift-flux models are evaluated against the experimental data, and the Ozaki model demonstrates higher precision in estimating void fraction, exhibiting a deviation of 9.8% on average.

Comprehensive analysis of the effect of braiding angle on the wettability and mechanical properties of 3D braided carbon fiber fabric-reinforced composites

Fiber-reinforced composites are designed to enhance strength, stiffness, and lightweight properties. However, while the use of continuous fibers offer substantial performance benefits it presents challenges in achieving complex configurations. This study focused on evaluating the effects of different braiding angles on the mechanical properties of braided fabric-reinforced composites (B-CFRP). Continuous fiber tows were braided around a mandrel, with meticulous control over the key process parameters to ensure consistency. The composites were then processed using the Vacuum Assisted Resin Transfer Molding (VARTM) technique to achieve optimal impregnation of the resin. Mechanical properties, including tensile, flexural, compressive strength, interlaminar shear strength (ILSS), and impact strength, were performed to establish the relationship between resin impregnation and mechanical properties with different braid angles. Additionally, resin flow experiments and scanning electron microscopy (SEM) analysis were conducted to investigate how variations in braiding angle influence fiber arrangement, resin distribution, and fracture behavior. These insights aim to guide the design and manufacturing of high-performance composites.

Synergistic catalysis of dual-sites promoted cycloaddition of CO2 with epoxides

This study explores the catalytic efficacy of fluorine-modified 1 wt% copper oxide on MCM-41 (F-1Cu/MCM-41) in carbon dioxide cycloaddition reactions. It delves into reaction mechanisms, active sites, and the practical applicability of the catalyst. Comprehensive examination through in situ diffuse reflectance infrared Fourier transform spectroscopy and other analytical methods substantiated the role of halogen-modified mono-dispersed copper species in carbon dioxide activation and silicon hydroxide sites in epoxide activation, while underscoring the role of Lewis bases and Brønsted acids. Kinetic studies and density functional theory calculations pinpointed carbon dioxide activation as the pivotal step. Furthermore, the catalyst exhibited robust stability and efficiency in continuous flow experiments, sustaining a 99% selectivity towards cyclic carbonate over 150 h. An eco-friendly evaluation confirmed the sustainability of the process, emphasizing its minimal environmental footprint and high efficiency. These results establish fluorine-modified 1 wt% copper oxide on MCM-41 as a formidable candidate for industrial-scale cyclic carbonate production, due to its promising performance and sustainability.

Parametric Study on Venturi Pressure Drop for Two Phase Oil (D130)-Water Flow for Different Operating Conditions – An Experimental Investigation

The governing parameters which affect pressure drop of two-phase oil-water flow across the venturi meter are water cut and angle of inclination. The study investigates experimentally the effect of inclination and water cut on pressure drop measurements across different venturi meters with beta ratios (β) = 0.4, and 0.6 for oil–water two-phase flow experiments in a 3-inch pipe for different operating conditions. Two-phase inclinable flow loop has been employed for conducting the experiments for different fluid mixture flow rates and water cuts. The working fluids utilized are Exxsol mineral oil (D130) and potable water. The experiments were conducted for water cuts varying from 0 to 100% in steps of 20%, flow rates ranging from 2000 to 12000 barrels per day (BPD), and for horizontal and vertical flow loop inclinations (0◦ and 90◦). Liquid flow rates considered in the study match flow rates of real oil wells. The results indicate that the venturi pressure drop varies linearly with water cuts for both β ratios (0.4 and 0.6). The study indicates that the effect of inclination on venturi pressure drop is not appreciable for all water cuts and flow rates. Also, from the experimental results it can be concluded that venturi with β = 0.6 is favourable for multiphase flow metering (with flow rates ranging from 8000 to 12000 BPD). The tangible findings of the study will be helpful in combating multi-phase flow challenges in oil and petroleum industries.