Erbium-doped Fluoride Research Articles

10 W, 2 mJ-level ns all-fiber amplifier at 2.8 µm.

In this Letter, we demonstrate a single-stage erbium-doped fluoride fiber amplifier composed of two spliced large core fibers with respective diameters of 85 and 130 µm. An optical parametric generator (OPG) operating at a 5 kHz repetition rate, and providing ∼2 ns pulse duration, and an average output power of 500 mW at a wavelength of 2.8 µm was used as a seed source. This nanosecond amplifier configuration achieved an average output power of 10 W with a record pulse energy of 2 mJ, corresponding to 1 MW of output peak power. The maximum slope efficiency of this hybrid amplifier is 21% with respect to the total incident pump power at 940 nm. The presented master-oscillator power-amplifier (MOPA) configuration shows its potential for further power and energy scaling.

2 W monolithic fiber laser at 3.8 µm

We report a dual-wavelength-pumped all-fiber continuous-wave laser operating at the extended wavelength of 3.79 µm that reaches a record output power of 2.0 W. This represents, to the best of our knowledge, the highest output power reported at the longest spectral range for a fiber laser. The laser cavity, made of a heavily erbium-doped fluoride fiber and bounded by two photo-inscribed fiber Bragg gratings, reaches a slope efficiency of 46.5% with respect to the absorbed 1976 nm pump power. The system exhibits an absorption dependency of the 1976 nm pump on the launched 976 nm pump and a quenching behavior dependency on the output coupler reflectivity. The all-fiber design of the cavity allows significant power scaling of the laser and ensures its long-term stability.

Histological analysis of laser-enabled tissue coring with a novel 2910 nm erbium-doped fluoride glass fiber laser.

There remains an unmet need for a laser-enabled tissue coring device that can effectively improve face and neck skin laxity and rhytides. We investigate a novel 2910 nm erbium-doped fluoride glass fiber laser (2910 nm fiber laser) (UltraClear; Acclaro Medical) for laser-coring of submental tissue. Five subjects, Glogau scale III-IV, were treated with a single pulse of the laser-coring mode of the 2910 nm fiber laser in the submentum. A 4 mm punch biopsy was immediately performed. Biopsy specimens were sectioned and stained with hematoxylin and eosin and placed on glass slides. All sections were reviewed, and sections containing the center of the transected core were analyzed for depth and diameter of the ablative microchannel and width of the surrounding zone of coagulation. A total of 15 intact micro-cores were analyzed. Histological analysis revealed an average ± standard deviation microchannel diameter of 242.5 ± 65.2 µm, an average ablative depth of 980 ± 318.8 µm, and an average zone of coagulation of 104 ± 32 µm. Laser-enabled tissue coring with a novel 2910 nm fiber laser can safely achieve a wider microchannel diameter with ablative depth extending to the mid and deep dermis, which has the potential for collagen contraction and tissue tightening. Laser-coring to this ablation diameter and depth and with the surrounding zone of coagulation was found to be safe without adverse effects of post-inflammatory erythema or scarring in our study.

Full-face and neck resurfacing with a novel ablative fractional 2910 nm erbium-doped fluoride glass fiber laser for advanced photoaging.

Ablative fractional lasers have long been considered the gold standard for facial resurfacing for advanced photoaging. These lasers offer an improved safety profile compared to traditional ablative lasers but typically require more treatment sessions given their fractional approach. In this study, we evaluate a new novel 2910 nm erbium-doped fluoride glass fiber laser (2910 nm fiber laser) (UltraClear; Acclaro Medical) for full-face and neck resurfacing for the treatment of advanced photoaging. Twenty-two healthy subjects aged 44-80 years presenting for advanced facial photoaging and rhytides were enrolled in the study. All subjects received three full-face and neck, multipass treatments utilizing the 2910 nm fiber laser spaced 6-8 weeks apart. Subjects were asked to rate the average level of pain during the treatment. At 90 days following subjects' third treatment subjects evaluated their improvement using a Global Aesthetic Improvement Scale (GAIS) and rated their satisfaction with the treatment. Evaluation of pretreatment and posttreatment photos was completed by two blinded physician reviewers. Reviewers were asked to identify the pretreatment and posttreatment photographs and to rate the degree of improvement utilizing a GAIS. Fifteen participants completed the study; six were exited from the study (withdrew or lost to follow-up). The average subject GAIS score for overall appearance was 3.8. The average subject satisfaction level at follow-up was 4.8. The average subject pain score was 4.9. One blinded physician reviewer correctly identified 100% of subjects' posttreatment photographs, while the second blinded reviewer correctly identified 93%. Blinded evaluation of digital photographs revealed an average GAIS score of 3.2. Posttreatment skin responses included pin-point hemorrhage, erythema, edema, and soft tissue crusting lasting 5-7 days. There were no instances of infection, scarring or hypopigmentation. There were two instances of temporary hyperpigmentation. Treatment with the novel 2910 nm fiber laser is safe and effective in treating advanced photoaging and rhytides. Three treatments produced moderate to marked improvement with high patient satisfaction and treatment was associated with less discomfort and downtime compared to conventional fractional ablative lasers.

Single treatment scar resurfacing with a novel ablative fractional 2910 nm erbium-doped fluoride glass fiber laser.

Single treatment scar resurfacing with a novel ablative fractional 2910 nm erbium-doped fluoride glass fiber laser.

Numerical Investigation of Polarization-Dependent Ultrashort Pulse Amplification in Erbium-Doped Fluoride Fibers

We have theoretically investigated the polarization-dependent ultrashort pulse amplification in erbium-doped fluoride fibers. The numerical model is based on the coupled generalized nonlinear Schrödinger equations and the rate equations. It is found that the Raman effect can be weakened by converting the seed polarization from linear to circular. Compared with the linearly polarized seed pulses, amplification of the circularly polarized seed pulses can generate Raman solitons with a larger pulse energy of the same central wavelength, although more pump power is needed. Furthermore, the amplification dynamics when no pulse splitting occurs have also been investigated. We demonstrate that amplification of the circularly polarized seed pulses allows the main pulse to accumulate more energy while maintaining a single-pulse profile. It is predicted that sub-two-cycle laser pulses at 2.8 μm with megawatt peak power and hundreds of nanojoules pulse energy can be directly generated from the erbium-doped fluoride fiber amplifiers. The investigations conducted in this paper can provide guidelines for the design of Raman-soliton-based tunable fiber laser systems and high-power few-cycle fiber laser systems.

Numerical modeling of multi-point side-pumped mid-infrared erbium-doped fluoride fiber lasers.

We investigate the power scaling and thermal management of multi-point side-pumped 2.825 µm heavily-erbium-doped fluoride fiber lasers by numerical simulation. The 4-point (or 6-point) erbium-doped fluoride fiber laser with polished erbium-doped fluoride fiber-based side-pump couplers delivers an output laser power of over 100 W at each launched 981 nm pump power of 100 W (or 75 W). Meanwhile, the core temperature increases of the gain fiber tips are below 1 K, making it possible for a highly reflective fiber Bragg grating to work stably in high-power operation. Once the preparation processes of these erbium-doped fluoride fiber-based side-pump couplers and endcaps with effective coatings are mature, the proposed multi-point side-pumped erbium-doped fluoride fiber lasers with some feasibility may theoretically pave the way for the development of hundred-watt mid-infrared fiber lasers with effective thermal management.

Gain-switched 2.8 μm fluoride fiber laser pumped at 1550 nm

We demonstrated a gain-switched heavily erbium-doped fluoride fiber laser pumped at 1550 nm. A 2.8 μm short-pulsed laser with a maximum average output power of 350 mW and a practical optical-optical efficiency of ∼11.3% was obtained at a repetition rate of 50 kHz with a single pulse energy of 7 μJ, a pulse width of 938 ns, and a peak power of 7.5 W. Gain-switched temporal states with 1/n (n = 4,3,2) (ratio of signal pulses per pump pulses) pump repetition rates were first observed in the 2.8 μm erbium-doped fluoride fiber laser. These results indicate that the 1550 nm pulsed pumping scheme is an efficient and potential way for power scaling of 2.8 μm short-pulsed erbium-doped fluoride fiber lasers.

All-fiber 2–6 [formula omitted] coherent supercontinuum source based on chalcogenide fibers pumped by an amplified mid-IR soliton laser

We numerically and experimentally investigate an all-fiber configuration of coherent mid-infrared supercontinuum generation in the femtosecond pumping regime. In particular, we demonstrate the advantageous combination of various dispersion-engineered chalcogenide (Ge-Se-Te glass) fibers with a turn-key amplified femtosecond fiber laser delivering 175-fs soliton pulses around 3.4 μm and developed from the erbium-doped fluoride fiber technology. Our results show that compact and coherent octave-spanning fiber supercontinuum sources centered on the 2–5 μm infrared atmospheric window can be obtained with a maximum average power of 50 mW at 25 MHz repetition rate.

Amplification of GaSb-Based Diode Lasers in an Erbium-Doped Fluoride Fibre Amplifier

Building upon recent advances in GaSb-based diode lasers and Er-doped fluoride fibre technologies, this article demonstrates for the first time the fibre-based amplification of mid-infrared diode lasers in the wavelength range around 2.78 <inline-formula xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink"><tex-math notation="LaTeX">$\mu$</tex-math></inline-formula> m. The laser setup consists of a GaSb-based diode laser and a single-stage Er-doped fibre amplifier. Amplification is investigated for continuous wave (CW) and ns-pulsed input signals, generated by gain-modulation of the GaSb-based seed lasers. The experimental results include the demonstration of output powers up to 0.9 W, pulse durations as short as 20 ns, and pulse repetition rates up to 1 MHz. Additionally, the amplification of commercial and custom-made GaSb-based seed lasers is compared and the impact of different fibre end-cap materials on laser performance is analysed.

Amplification of Nanosecond Pulses in a Single- Mode Erbium-Doped Fluoride Fibre Amplifier

We investigate the amplification of nanosecond pulses in a single-mode Er-fluoride fibre amplifier. A PPLN-based optical parametric oscillator (OPO) with a Q-switched Nd:YAG pump laser was used to generate seed pulses at a wavelength of 2790 nm. The OPO system produced seed pulses with sub-10 ns pulse durations and pulse energies of <inline-formula xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink"> <tex-math notation="LaTeX">$0.5~\mu \text{J}$ </tex-math></inline-formula> at a repetition rate of 10 kHz. These seed pulses were amplified in a single-mode Erbium-fluoride fibre amplifier, consisting of 2.2 m of double-clad fibre with a doping concentration of 7 mol%. Using this setup, we demonstrate gain values of up to 20 dB, output pulse energies of <inline-formula xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink"> <tex-math notation="LaTeX">$52.7~\mu \text{J}$ </tex-math></inline-formula> , and peak powers of more than 8 kW.

Broadband saturable absorption of indium tin oxide nanocrystals toward mid-infrared regime.

We experimentally demonstrate the ultrabroadband optical nonlinearity of indium tin oxide nanocrystals (ITO NCs) in the mid-infrared regime. Especially, the ITO NCs show considerable saturation absorption behavior with large modulation depth covering the spectral range from 2-µm to 10-µm wavelength. We also demonstrate the application of the optical nonlinearity to successfully modulate the erbium-doped fluoride fiber laser to deliver a nanosecond pulse with a signal-to-noise ratio over 43 dB at 2.8-µm wavelength. The results provide a promising platform for the development of ITO-based broadband and robust optoelectronic devices toward the deep mid-infrared spectral range.

Wavelength-Tuning of Nanosecond Pulses in Er-Doped Fluoride Fibre Amplifier

We investigate the gain bandwidth and wavelength-tuning range of an erbium-doped fluoride fibre amplifier. The presented experimental setup consisted of a widely wavelength-tunable optical parametric oscillator (OPO), which was amplified in a single-stage Er-doped fluoride fibre amplifier. The OPO laser provided seed pulses with a pulse width of 5.2 ns and a repetition rate of 10 kHz. The fibre section consisted of 2.2 m of double-clad, single-mode fibre with a doping concentration of 7 mol%. Wavelength-tuning was analysed at gain values of up to 26 dB and amplified pulse energies of up to 37.4 <inline-formula xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink"><tex-math notation="LaTeX">$\mu \mathrm{J}$</tex-math></inline-formula> . Using this setup, we demonstrate continuous wavelength tuning of more than 100 nm, covering the wavelength range from 2712 nm to 2818 nm.

Numerical Analysis of a Dual-Wavelength-Clad-Pumped 3.5 μm Erbium-Doped Fluoride Fiber Laser

The stability and efficiency of a 3.5 μm erbium-doped fluoride fiber is strongly limited by the core pumping setup of a 1976 nm pump. A dual-wavelength-clad-pumped scheme was put forward for a more robust and higher electro-optical efficiency in this paper, and a numerical model was built up to stimulate the fiber. Parameter optimizations were given for both the traditional dual-wavelength pump setup and our new scheme. The results show the possibility of using a laser diode as pump source for the generation of a 3.5 μm laser, and the characteristics were analyzed.

Erbium-doped ZBLAN fiber laser pumped at 1.7 µm for emission at 2.8 µm.

In this paper, a novel, to the best of our knowledge, efficient pump scheme for an erbium-doped fluoride fiber laser with emission at 2.8 µm in the mid-infrared region is proposed and demonstrated. A singular pump source at 1.7 µm is used to excite Er3+ ions from ground state 4I15/2 to lower laser level 4I13/2, and then further boost the ions to 4I9/2, where a non-radiation transition occurs for the Er3+ ions to reach upper laser level 4I11/2. This scheme can efficiently recycle ions on the lower laser level 4I13/2 by excited-state absorption, therefore realizing population inversion and enhancing laser efficiency. In our demonstration, a 660-mW laser output at 2.8 µm is achieved from a 1.7-µm core-pumped erbium-doped fluoride fiber laser, where the slope efficiency versus launched pump power is 23.7%. The proposed innovative pump scheme shows great potential to realize high-power, high-efficiency erbium-doped fiber lasers at 2.8 µm.

Numerical modeling and optimization of hundred-watt-level 2.8 μm and 1.6 μm cascaded heavily-erbium-doped fluoride fiber amplifiers

We propose a continuous-wave dual-seed cascaded heavily erbium-doped fluoride fiber amplifier scheme with a 981 nm bi-directional pump configuration for hundred-watt-level power scaling for the first time. When the powers of the 2.8 μm and 1.6 μm seed lasers and the total pump light are 5 W, 20 W, and 300 W, respectively, the 2.8 μm laser theoretically achieves an output power of ∼100 W. The amplifier scheme can also reduce the fiber temperature. Additionally, the results show that there is no excited state absorption at ∼1.675 μm, and thus injecting a 1.675 μm laser to the amplifier is not conducive to the power scaling.

Spectral beam combining of 2.8 μm fiber laser based on telescope system

We reported a spectral beam combining (SBC) of 2.8 μm erbium-doped fluoride glass fiber laser based on a telescope system. The application of the telescope system compressed the spectra of SBC significantly and allowed more fiber lasers to be combined. The SBC of three fiber lasers with a beam combining the efficiency of 68% was demonstrated. This work shows the ability of SBC in fluoride fiber power scaling.

15 W monolithic fiber laser at 3.55 µm

We report a dual-wavelength-pumped all-fiber continuous-wave (CW) laser operating at 3.55 µm that reached an output power of 14.9 W, which is, to the best of our knowledge, a record. The laser cavity, made of an erbium-doped fluoride fiber and bounded by two fiber Bragg gratings (FBGs), operates at an overall optical efficiency of 17.2% and a slope efficiency of 51.3% with respect to the 1976 nm launched pump power. The all-fiber design of the cavity not only allows for significant power scaling of the laser output, but also improves its long-term stability at high output power. The cavity design was set according to a numerical optimization that showed very good agreement with the experimental results.

Mode-locked fiber laser of 3.5 µm using a single-walled carbon nanotube saturable absorber mirror

We report on a mid-infrared fiber laser that uses a single-walled carbon nanotube saturable absorber mirror to realize the mode-locking operation. The laser generates 3.5 µm ultra-short pulses from an erbium-doped fluoride fiber by utilizing a dual-wavelength pumping scheme. Stable mode-locking is achieved at the 3.5 µm band with a repetition rate of 25.2 MHz. The maximum average power acquired from the laser in the mode-locking regime is 25 mW. The experimental results indicate that the carbon nanotube is an effective saturable absorber for mode-locking in the mid-infrared spectral region.

Numerical study of a hybrid mode-locked erbium-doped fluoride fiber laser at 2.8 μm

We numerically investigate a hybrid mode-locked erbium-doped fluoride fiber laser in the mid-infrared region. Based on the coaction of nonlinear polarization rotation (NPR) and semiconductor saturable absorber mirror (SESAM), uniform mode-locked soliton pulse with 155 fs pulse duration, 14.78 kW peak power, and 2.29 nJ pulse energy can be achieved. For comparison, the single SESAM mode-locking and NPR mode-locking of the erbium-doped fluoride fiber laser are simulated, respectively. The effect of all kinds of parameters including gain fiber length, saturable energy of the gain fiber, linear cavity phase delay bias, and small-signal gain on the hybrid mode-locking laser are also investigated.