Effect Of Dentin Surface Treatments Research Articles

Monolitik Zirkonya Materyalinin Dentine Bağlanma Dayanımı Üzerine Farklı Tür Asit Yüzey Uygulamalarının Etkilerinin Araştırılması

Objective: The aim of this study is to evaluate the effect of dentin surface treatments with citric, tartaric, phosphoric, and boric acids on the bonding strength of monolithic zirconia. Material and Methods: A hundred human molar teeth were randomly divided into subsets (n = 10) based on acid treatment modalities and thermocycling procedure. Monolithic zirconia superstructures were fabricated using CAD/CAM system in the final dimensions of 7 mm in diameter and 3 mm in thickness. After application of acid treatments to dentin surface, shear bond strength test was performed to assess the effectiveness of surface modifications that were also examined using a scanning electron microscope. Results: The study groups were ranked respectively as (citric acid>tartaric acid>phosphoric acid>boric acid>control) for the set of groups without thermocycling and (citric acid>tartaric acid) and (phosphoric acid>boric acid>control) for the set of thermocycling groups (p<0.05) based on highest value. The bonding strength of tartaric acid group was not significantly different from the bonding strength of phosphoric acid group (p>0.05). Conclusion: In both procedures with and without thermal cycling; based on order of efficacy, citric, tartaric, phosphoric, and boric acids were more effective in improving the shear bond strength between monolithic zirconia and dentin surface. The thermal cycling procedure decreased the bonding strength in all the groups.

Effects of Dentin Surface Treatments on Hypersensitivity to Bond Strength of Restorations: An In Vitro Study

This study evaluated the effects of desensitizing treatments on the shear bond strength (SBS) of adhesive resin cement (Rely X U100) applied to dentin. Human molars (n = 120) with exposed dentin were divided into 12 groups. In the experimental groups, dentin surfaces were treated with (1) an erbium:yttrium- aluminium-garnet (Er:YAG) laser, (2) a neodymium:yttrium-aluminium-garnet (Nd:YAG) laser, (3) glutaraldehyde (Gluma)-, (4) fluoride (Aqua Prep-F)-, and (5) oxalate (BisBlock)-containing desensitizing agents, (6) Gluma preceding the Er:YAG laser, (7) Aqua Prep-F preceding the Er:YAG laser, (8) BisBlock preceding the Er:YAG laser, (9) Gluma preceding the Nd:YAG laser, (10) Aqua Prep-F preceding the Nd:YAG laser, (11) and BisBlock preceding the Nd:YAG laser, in groups EL, NL, G, F, O, EL-G, EL-F, EL-O, NL-G , NL-F, and NL-O, respectively. Then, lithium disilicate ceramics were cemented to the treated surfaces. Subsequently, an SBS test was performed and the data were statistically analyzed (α = .001). The results suggested that the combined treatment of Gluma preceding Er:YAG laser increased the bond strength of ceramic to the dentin surface using a self-adhesive resin cement.

Effects of dentin surface treatments including Er,Cr:YSGG laser irradiation with different intensities on the push-out bond strength of the glass fiber posts to root dentin

Objective. Intra-canal post systems are commonly used to restore root-filled teeth. Bond strengths of the posts can be affected by various surface treatments of the post or the dentin. The aim of this study was to evaluate the effects of dentin surface treatments including erbium-chromium; yttrium-scandium-gallium-garnet (Er,Cr:YSGG) laser irradiation with different intensities on the push-out bond strength of the glass fiber posts to root dentin. Materials and methods. Forty single-rooted human maxillary incisors were filled and post spaces were prepared. After these procedures, the specimens were divided randomly into four groups according to the dentin surface treatments, as follows: (i) untreated surface (control), (ii) 1W Er,Cr:YSGG laser application, (iii) 2W Er,Cr:YSGG laser application and (iv) 3W Er,Cr:YSGG laser application. Then the posts were cemented into the root canals using dual-cured resin cement. Bonded specimens were cut into 1-mm-thick slices and push-out tests were performed using a universal testing device. All specimens were loaded until fracture and the failure modes were evaluated with a stereomicroscope at 32× magnification. Representative specimens were analyzed by scanning electron microscopy. Data were analyzed using a one-way ANOVA, Tukey and Wilcoxon tests. Results. The bond strength values ranged from 3.22–4.68 MPa. There were no statistically significant differences among the groups, regardless of the different levels. The coronal and middle levels of the post space had significantly higher bond strength values compared with the apical level (p < 0.05). Conclusion. Er,Cr:YSGG laser irradiation with different intensities did not increase the bond strength of the fiber posts to the root canal dentin walls.

Effects of dentin surface treatments on shear bond strength of glass-ionomer cements

The aim of this in vitro study was to evaluate the effect of different surface treatments on shear bond strength of a conventional glass-ionomer cement (GIC) and a resin-modified glass-ionomer cement (RMGIC) to dentin. 80 bovine permanent incisors were used. 40 cylindrical specimens of a GIC (Fuji IX GP Extra) and 40 cylindrical specimens of a RMGIC (Fuji II LC) were attached to the dentin. The teeth were then randomly assigned to 8 groups of equal size (n=10), 4 for every type of glass-ionomer cement, corresponding to type of dentin surface treatments. Group 1: GC Cavity Conditioner; Group 2: 37% phosphoric acid gel; Group 3: Clearfil SE Bond; Group 4: no dentin conditioning (control). The specimens were placed in a universal testing machine (Model 3343, Instron Corp., Canton, Mass., USA) and subsequently tested for shear bond strength (MPa). ANOVA showed the presence of significant differences among the various groups. Post hoc Tukey test showed different values of shear bond strength for Fuji IX GP Extra and for Fuji II LC. The different conditioners variably influence the adhesion of the glass-ionomer cements tested. Conclusions. RMGIC shear bond to dentin was higher than GIC. The use of a Self-etch adhesive system improved the shear bond strength values of RMGIC and lowered the shear bond strength values of GIC significantly.

Dentin treatment effects on the bonding performance of self‐adhesive resin cements

The effects of dentin surface treatments on the microtensile bond strengths and on the interfacial characteristics of self-adhesive resin cements were investigated. Flat dentin surfaces were obtained from human molars and were treated as follows: (i) no treatment of dentin; (ii) 0.1 M EDTA scrubbed for 60 s; or (iii) 10% polyacrylic acid applied for 30 s. Three self-adhesive cements were used to lute composite overlays on deep-coronal dentin surfaces in the presence of simulated pulpal pressure (15 cm of H(2)O). Bonded specimens were cut into beams 1 mm thick and stressed in tension until failure. Fractured sticks were examined under a scanning electron microscope. Additional specimens were stained with Masson's trichrome and observed under light microscopy for interfacial evaluations. The bond strength to dentin of the hydrophobic and solvent-free cement (RelyX Unicem) was unaffected by the tested dentin treatments. The bond strength of the 2-hydroxyethyl methacrylate (HEMA)-based cement (Bis-Cem) decreased after treatment of dentin with EDTA and/or polyacrylic acid. The hydrophilic and water-containing cement (G-Cem) attained a higher bond strength when luted on polyacrylic acid-conditioned dentin. In conclusion, smear layer removal, opening of dentinal tubules, and the water content of dentin differently influence the bond strengths and the interfacial characteristics of self-adhesive cement-dentin interfaces.

Effect of dentinal surface preparation on bond strength of self-etching adhesive systems

The aim of this study was to evaluate the effects of dentin surface treatments on the tensile bond strength (TBS) of the self-etching primer Clearfil SE Bond (CSE) and the one-step self-etching One-Up Bond F (OUB). The exposed flat dentin surfaces of twenty-four sound third molars were prepared with diamond bur at high-speed, carbide bur at low-speed or wet ground with #600 grit SiC paper. The adhesive systems were applied to the dentin surfaces and light-cured according to the manufacturers' instructions. A 6-mm high composite crown was incrementally built-up and each increment was light-cured for 40 seconds. After being stored in water (37 degrees C/24 h), the samples were serially sectioned parallel to the long axis, forming beams (n = 20) with a cross-sectional area of approximately 0.8 mm(2). The specimens were tested in a Universal Testing Machine at 0.5 mm/min. The cross-sectional area was measured and the results (MPa) were analyzed by two-way ANOVA and Tukey Test (p < 0.05). Overall, the groups treated with CSE exhibited the highest TBS for all surface treatments. Dentin surfaces prepared with carbide bur at low speed reduced TBS in the CSE group; however, OUB was not affected by surface treatments. The effect of surface abrasive methods on TBS was material-dependent.

Dynamic contact angle and spreading rate measurements for the characterization of the effect of dentin surface treatments

A new methodology capable of providing reliable and reproducible contact angle ( θ) data has been employed to study the effect of clinical treatments grinding, acid etching, and deproteinization on medial dentin tissue. It is based on the application of the ADSA-CD algorithm to the determination of low-rate dynamic contact angles, obtained from slowly growing drops, and on contact angle measurement, as well as spreading behavior analysis, during the relaxation of the system (water on treated dentin) after initial drop growth. The θ data obtained were substantially more reproducible than those obtained with classical methods. A net effect of the treatment on θ was found, increasing dentin wettability: θ (polished) > θ (etched) > θ (deproteinized). The spreading rates correlate with the angles and are adequate for the dentin surface characterization. ANOVA and SNK tests show that for advancing contact angles the means corresponding to all treatments are significantly different. In the relaxing phase, mean angle and spreading rates on polished dentin differ significantly from those on etched and deproteinized dentin, but the latter do not differ significantly from each other.

Effects of dentin surface treatments on the shear bond strength of vitrabond

The influences of nine dentin surface treatments were evaluated on the shear bond strength of a new light-cured glass-ionomer cement (GIC) and on the SEM morphology of the treated dentin surfaces. The following treatments were performed: saline solution (control), NaOCl, acidic glycine, EDTA, malic acid, malic acid plus glycine, polyacrylic acid, tannic acid, and neutral + acidic oxalate solutions. Buccal dentin surfaces were polished with #320-grit abrasive paper, treated with one of the chemicals, washed, and air-dried. Cylindrical GIC samples were then applied to the dentin surface, stored in 100% humidity, and tested after 24 h. SEM observations demonstrated no effect of saline or NaOCl treatment on the smear layer but its complete removal with exposure of collagen fibrils after malic or malic acid plus glycine treatment. Partial removal of the smear layer occurred following glycine treatment and with tannic or polyacrylic acids. Complete removal of the smear layer was seen after EDTA or pyruvic acid treatment. Oxalate treatment produced a layer of crystals, which completely covered the dentin surface. Shear bond strength of GIC was significantly increased only by treatment with the oxalate solutions.