Dynamic Compression Experiments Research Articles

A failure model for bulk metallic glass based on strain rate-correlated softening mechanism

Due to the amorphous nature of the bulk metallic glasses (BMGs), catastrophic fractures occur once the nucleation and propagation of shear bands occur, which is quite different from crystal materials. So far, the underlying mechanism of BMG failure behavior and its strain rate effect are still controversial. In this work, the quasi-static and dynamic compression experiments of Vit-1 BMG were carried out in a wide range of strain rates from 0.001 s−1 to 5000 s−1. The results show that the variation tendency of failure stress with strain rate can be divided into three stages. The quasi-static failure stress is insensitive to the change of strain rate with only almost constant free volume softening effect inside the material during the failure process. When entering dynamic loading stage, the failure stress decreases significantly, which is caused by a combination of increasing thermal softening and free volume softening effects. When the strain rate increases to the third stage, that is, over 2000 s−1, the failure stress and the softening effects basically remain unchanged. The transformation of failure mechanism is well confirmed by the micromorphology of fracture surfaces. Based on the experimental results, a concise empirical failure model is established, in which the failure stress is decomposed into softening and non-softening parts. The verification experiments show that the model can effectively predict the compression failure stress of BMG under different strain rates.

Potentially overlooked high post-shock temperatures in dynamic compression experiments

An unexpectedly high amount of energy in shock experiments is converted to thermal energy, challenging the common understanding of shock release as an isentropic process

Automated pipeline processing X-ray diffraction data from dynamic compression experiments on the Extreme Conditions Beamline of PETRAIII.

Presented and discussed here is the implementation of a software solution that provides prompt X-ray diffraction data analysis during fast dynamic compression experiments conducted within the dynamic diamond anvil cell technique. It includes efficient data collection, streaming of data and metadata to a high-performance cluster (HPC), fast azimuthal data integration on the cluster, and tools for controlling the data processing steps and visualizing the data using the DIOPTAS software package. This data processing pipeline is invaluable for a great number of studies. The potential of the pipeline is illustrated with two examples of data collected on ammonia-water mixtures and multiphase mineral assemblies under high pressure. The pipeline is designed to be generic in nature and could be readily adapted to provide rapid feedback for many other X-ray diffraction techniques, e.g. large-volume press studies, in situ stress/strain studies, phase transformation studies, chemical reactions studied with high-resolution diffraction etc.

Strain rate effects on fragment morphology of ceramic alumina: A synchrotron-based study

Dynamic (600–1000 s−1) and quasi-static (0.001–0.01 s−1) compression experiments are conducted on a high-purity alumina ceramic using a split Hopkinson pressure bar and a material test system, respectively. The postmortem fragments of ceramic samples at different strain rates are then characterized via synchrotron micro computed tomography (CT). The three-dimensional (3D) morphologies of fragments are quantified using the gyration tensor analysis after proper segmentation of CT images. The mean fragment size decreases in a power-law form while the mean shape indices (sphericity, elongation index and flatness index) increase in a logarithmic-linear form, with increasing strain rates. In addition, the fragment size and shape distributions are all found to follow the Weibull probability distribution. To reveal the underlying mechanisms of such strain rate effects, high-speed optical and X-ray imaging are implemented to capture the fracture process of ceramic samples under quasi-static and dynamic compression. Primary and secondary wing cracks (PWCs/SWCs) control the fracture and fragmentation of the ceramic under both loading conditions. Compared to quasi-static loading, a considerably larger number of SWCs are produced under dynamic loading, and pronounced branching and bridging occur among the PWCs, which prevent the PWCs from coalescing into axial splitting cracks. Consequently, crack networks composed of high-density wing cracks break the sample into finer and more isotropic fragments, consistent with CT characterizations. Scanning electron microscopy is utilized to analyze the micro damage modes of ceramic samples. Transgranular fracture dominates the grain-scale damage and contributes to the higher dynamic fracture resistance of the alumina under dynamic loading, as a result of more homogeneous nucleation and growth of micro cracks.

Impact Toughness Analysis and Numerical Simulation of Coral Aggregate Concrete at Various Strength Grades: Experimental and Data Investigations

This paper comprehensively investigates the dynamic mechanical properties of concrete by employing a 75 mm diameter Split Hopkinson Pressure Bar (SHPB). To be detailed further, dynamic compression experiments are conducted on coral aggregate seawater concrete (CASC) to unveil the relationship between the toughness ratio, strain rate, and different strength grades. A three-dimensional random convex polyhedral aggregate mesoscopic model is also utilized to simulate the damage modes of concrete and its components under varying strain rates. Additionally, the impact of different aggregate volume rates on the damage modes of CASC is also studied. The results show that strain rate has a significant effect on CASC, and the strength grade influences both the damage mode and toughness index of the concrete. The growth rate of the toughness index exhibits a distinct change when the 28-day compressive strength of CASC ranges between 60 and 80 MPa, with three times an increment in the toughness index of high-strength CASC comparing to low-strength CASC undergoing high strain. The introduction of pre-peak and post-peak toughness highlights the lowest pre-to-post-peak toughness ratio at a strain rate of approximately 80 s−1, which indicates a shift in the concrete’s damage mode. Various damage modes of CASC are under dynamic impact and are consequently defined based on these findings. The LS-DYNA finite element software is employed to analyze the damage morphology of CASC at different strain rates, and the numerical simulation results align with the experimental observations. By comparing the numerical simulation results of different models with varying aggregate volume rates, it is reported that CASC’s failure mode is minimized at an aggregate volume rate of 20%.

The high power laser facility at beamline ID24-ED at the ESRF

ABSTRACT This paper describes technical details and new scientific opportunities offered by the new High Power Laser Facility at the ESRF, opened to users since 2022. This facility enables laser-induced dynamic compression experiments probed by ultra-fast X-ray Absorption Spectroscopy at beamline ID24-ED. This capability allows to reach and probe more extreme pressure and temperature states and higher strain rates with respect to static compression, addressing open questions in fundamental, planetary and material science.

Release dynamics of nanodiamonds created by laser-driven shock-compression of polyethylene terephthalate

Laser-driven dynamic compression experiments of plastic materials have found surprisingly fast formation of nanodiamonds (ND) via X-ray probing. This mechanism is relevant for planetary models, but could also open efficient synthesis routes for tailored NDs. We investigate the release mechanics of compressed NDs by molecular dynamics simulation of the isotropic expansion of finite size diamond from different P-T states. Analysing the structural integrity along different release paths via molecular dynamic simulations, we found substantial disintegration rates upon shock release, increasing with the on-Hugnoiot shock temperature. We also find that recrystallization can occur after the expansion and hence during the release, depending on subsequent cooling mechanisms. Our study suggests higher ND recovery rates from off-Hugoniot states, e.g., via double-shocks, due to faster cooling. Laser-driven shock compression experiments of polyethylene terephthalate (PET) samples with in situ X-ray probing at the simulated conditions found diamond signal that persists up to 11 ns after breakout. In the diffraction pattern, we observed peak shifts, which we attribute to thermal expansion of the NDs and thus a total release of pressure, which indicates the stability of the released NDs.

Mechanical response and phase transformation characteristics of R-phase NiTi shape memory alloy under high strain rate compression

R-phase NiTi shape memory alloy (R-NiTi SMA) has many excellent properties, but there are application problems such as simple structure and high price. High velocity impact welding can effectively solve these problems, but the research on the mechanical response and phase transformation (PT) characteristics of R-NiTi SMA under dynamic deformation is lacking. Therefore, the quasi-static (0.001 s-1) and dynamic (500 s-1, 1000 s-1, 1500 s-1, 2000 s-1) compression experiments were conducted on R-NiTi SMA in this research. The results showed that the true stress-strain curves of R-NiTi SMA during deformation were characterized by three stages, including the superelastic, elastic, and plastic segments. The critical stress of austenite to R (A-R) and R to martensite (R-M) phase transformation increased with the increase of strain rate, and the phase transformation process gradually disappeared when the strain rate exceeded 1000 s-1, which was related to the velocities of A-R and R-M phase transformation. With the increase of strain rate, defects such as dislocations increased and hindered the phase transformation process during unloading, resulting in the increase of A-phase content. In addition, the enthalpy of the deformed samples decreased significantly and the temperature ranges of phase transformation increased slightly. This work deepens the understanding of the dynamic response of R-NiTi SMA and helps to expand the application of high strain rate processing technology in R-NiTi SMA.

Shock compression experiments using the DiPOLE 100-X laser on the high energy density instrument at the European x-ray free electron laser: Quantitative structural analysis of liquid Sn

X-ray free electron laser (XFEL) sources coupled to high-power laser systems offer an avenue to study the structural dynamics of materials at extreme pressures and temperatures. The recent commissioning of the DiPOLE 100-X laser on the high energy density (HED) instrument at the European XFEL represents the state-of-the-art in combining x-ray diffraction with laser compression, allowing for compressed materials to be probed in unprecedented detail. Here, we report quantitative structural measurements of molten Sn compressed to 85(5) GPa and ∼3500 K. The capabilities of the HED instrument enable liquid density measurements with an uncertainty of ∼1% at conditions which are extremely challenging to reach via static compression methods. We discuss best practices for conducting liquid diffraction dynamic compression experiments and the necessary intensity corrections which allow for accurate quantitative analysis. We also provide a polyimide ablation pressure vs input laser energy for the DiPOLE 100-X drive laser which will serve future users of the HED instrument.

Influence of Interface Type on Dynamic Deformation Behavior of 3D-Printed Heterogeneous Titanium Alloy Materials.

Using the Split Hopkinson Pressure Bar technique, strain-limited dynamic compressive loading experiments were performed on TA1/TA15 heterostructure (HS) materials. The plastic deformation mechanisms, fracture forms, and energy absorption properties of an HS material with a metallurgical bonding interface (MB) and an HS material without a metallurgical bonding interface (NMB) are compared and analyzed. The results show that there is no significant difference between the two deformation mechanisms. The fracture forms are all "V-shaped" fractures within the TA1 part. The NMB was carried for 57 μs before failure and absorbed 441 J/cm3 of energy. The MB was carried for 72 μs before failure and absorbed 495 J/cm3 of energy. Microstructure observations show that there is a coordinated deformation effect near the MB interface compared to the NMB, with both TA1 and TA15 near the interface carrying stresses. This causes an enhancement of the MB load-bearing time and a 12% increase in energy absorption.

Hybrid Fabrication of Cold Metal Transfer Additive Manufacturing and Laser Metal Deposition for Ti6Al4V: The Microstructure and Dynamic/Static Mechanical Properties.

The titanium alloy components utilized in the aviation field are typically large in size and possess complex structures. By utilizing multiple additive manufacturing processes, the precision and efficiency requirements of production can be met. We investigated the hybrid additive manufacturing of Ti-6Al-4V using a combination of cold metal transfer additive manufacturing (CMTAM) and laser metal deposition (LMD), as well as the feasibility of using the CMT-LMD hybrid additive manufacturing process for fabricating Ti-6Al-4V components. Microstructural examinations, tensile testing coupled with digital image correlation and dynamic compressive experiments (by the split Hopkinson pressure bar (SHPB) system) were employed to assess the parts. The results indicate that the interface of the LMD and CMTAM zone formed a compact metallurgical bonding. In the CMTAM and LMD zone, the prior-β grains exhibit epitaxial growth, forming columnar prior-β grains. Due to laser remelting, the CMT-LMD hybrid additive zone experiences grain refinement, resulting in equiaxed prior-β grains at the interface with an average grain size smaller than that of the CMTAM and LMD regions. The microstructures reveal significant differences in grain orientation and morphology among the zones, with distinct textures forming in each zone. In the CMT-LMD hybrid zone, due to interfacial strengthening, strain concentration occurs in the arc additive zone during tensile testing, leading to fracture on the CMTAM zone. Under high-strain-rate dynamic impact conditions, the LMD region exhibits ductile fracture, while the CMTAM zone demonstrates brittle fracture. The hybrid zone combines ductile and brittle fracture modes, and the CMT-LMD hybrid material exhibits superior dynamic impact performance compared to the single deposition zone.

Effect of Ce on microstructure and dynamic compression properties of ZK60 alloy

The Mg–6Zn– xCe–0.6Zr ( x = 1, 2) alloys were subjected to a dynamic compression experiment, and the change in microstructure was noticed and studied. The primary components of two alloys are α-Mg matrix, Mg7Zn3 phase, and (Mg1− xZn x)11Ce phase. The two alloys have grain diameters of 2.8 and 3.2 μm, respectively. The dynamic compressive mechanical characteristics of the two alloys show a positive strain-strengthening effect, with Mg–6Zn–1Ce–0.6Zr alloy having somewhat higher values than Mg–6Zn–2Ce–0.6Zr alloy. At a strain rate of 500 s−1, {10[Formula: see text]2} tensile twin is the dominant deformation mechanism for two alloys, but the Mg–6Zn–2Ce–0.6Zr alloy is more prone to produce {10[Formula: see text]2} tensile twin. With the increase of the strain rate, the dominant deformation mechanism changes from {10[Formula: see text]2} tensile twin to pyramidal slip.

Influences of Graphene Oxide on Mechanical Properties and Mesoscopic Deformation and Failure Process of Concrete

In this research, graphene oxide (GO) was integrated into concrete to assess its effectiveness as an additive. Triaxial compression permeability experiments, variable‐angle (30°, 45°, and 60°) shear experiments, and dynamic compression experiments were conducted on graphene oxide concrete (GOC) and normal concrete (NC). The Holmquist–Johnson–Cook model and LS‐DYNA software were utilized to simulate the mesoscopic failure of NC and GOC under impact loading. The mechanism of GO was examined through scanning electron microscope (SEM) microscopic scanning and energy dispersive spectroscopy (EDS) energy spectrum testing. The findings demonstrate that the contain of GO significantly enhances the destruction resistance of concrete under triaxial compression. The permeability of both NC and GOC exhibits a negative exponential decrease with increasing confining pressure, and carbon fiber reduces concrete permeability by 17.79%–60.9%. Compared to NC, the cohesion and internal friction angle of GOC increased by 7.80% and 8.55%, respectively. GO also improves energy conversion and storage capacity during the elastic stage of concrete, reducing inelastic energy loss during shear processes. Although, both NC and GOC exhibit strain rate sensitivity, the DIF value of GOC surpasses that of NC and the disparity between the two intensifies with increasing impact pressure. Simulation results indicate that the number of crushing units in GOC is significantly lower than in NC, maintaining integrity. Analysis of SEM microscopic test results reveals that the distribution of cement hydration products in NC is uniform, whereas in GOC, it displays regional characteristics, a phenomenon corroborated by EDS energy spectrum test results.

Time-resolved X-ray diffraction diagnostic development for the National Ignition Facility.

We present the development of an experimental platform that can collect four frames of x-ray diffraction data along a single line of sight during laser-driven, dynamic-compression experiments at the National Ignition Facility. The platform is comprised of a diagnostic imager built around ultrafast sensors with a 2-ns integration time, a custom target assembly that serves also to shield the imager, and a 10-ns duration, quasi-monochromatic x-ray source produced by laser-generated plasma. We demonstrate the performance with diffraction data for Pb ramp compressed to 150GPa and illuminated by a Ge x-ray source that produces ∼7 × 1011, 10.25-keV photons/ns at the 400μm diameter sample.

Mixture of hydrogen and methane under planetary interior conditions.

We employ first-principles molecular dynamics simulations to provide equation-of-state data, pair distribution functions (PDFs), diffusion coefficients, and band gaps of a mixture of hydrogen and methane under planetary interior conditions as relevant for Uranus, Neptune, and similar icy exoplanets. We test the linear mixing approximation, which is fulfilled within a few percent for the chosen P-T conditions. Evaluation of the PDFs reveals that methane molecules dissociate into carbon clusters and free hydrogen atoms at temperatures greater than 3000 K. At high temperatures, the clusters are found to be short-lived. Furthermore, we calculate the electrical conductivity from which we derive the non-metal-to-metal transition region of the mixture. We also calculate the electrical conductivity along the P-T profile of Uranus [N. Nettelmann et al., Planet. Space Sci., 2013, 77, 143-151] and observe the transition of the mixture from a molecular to an atomic fluid as a function of the radius of the planet. The density and temperature ranges chosen in our study can be achieved using dynamic shock compression experiments and seek to aid such future experiments. Our work also provides a relevant data set for a better understanding of the interior, evolution, luminosity, and magnetic field of the ice giants in our solar system and beyond.

Dynamic compression responses of heterogeneous-structured CrMnFeCoNi high-entropy alloy at cryogenic temperatures

Dynamic compression experiments are conducted on a heterogeneous-structured CrMnFeCoNi high-entropy alloy (HEA) at different strain rates (1000–5000 s−1) and temperatures (123–293 K) with a split Hopkinson pressure bar system. Yield strength and strain hardening rate increase considerably with decreasing temperature at 5000 s−1 (low-temperature strengthening), but are insensitive to strain rate at 173 K, which can be well described by the Zerilli–Armstrong model. Compared to typical aluminum alloys and homogeneous-structured CrMnFeCoNi HEA, the heterogeneous-structured HEA exhibits higher thermal sensitivity and strain hardening rate. Microstructural characterizations show that dislocation density in the fine-grained domains increases more drastically than in the coarse-grained domains, inducing high deformation gradient between the coarse- and fine-grained domains. At 123 K, nano-scale primary and secondary deformation twins form in grain interior, along with a great number of stacking faults on twin boundaries; the twin width and spacing in coarse grains are considerably higher than in fine grains. In addition, the twin density at 123 K is significantly higher than that at 293 K. Overall, the increased deformation twinning and deformation gradient contribute to pronounced strengthening and strain hardening with decreasing temperatures in the heterogeneous-structured HEA under dynamic compression.

Constitutive modeling and simulation of polyethylene foam under quasi-static and impact loading

In this paper, quasi-static and dynamic compression experiments were carried out on polyethylene foam by a universal material testing machine and a drop tower impact device. The mechanical response characteristics and energy absorption capacity of polyethylene foam under quasi-static and moderate strain rate (4 × 10−3–102s−1) loading conditions were obtained. An improved constitutive model of strain-rate term coupling strain and strain rate was established based on the Sherwood–Frost phenomenological constitutive model and Johnson–Cook constitutive model. Low Density Foam model combined in the finite element software ABAQUS with the improved constitutive model was used as the parameter definition of polyethylene foam material in the simulation. The drop-tower impact tests at different heights were simulated, and the simulation results were compared with the actual drop tower impact test results. The results showed that the peak acceleration errors between simulation and experiment were less than 7.1%, verifying the accuracy of the constitutive model. This study provides a method of constitutive models and finite element simulation to the performance of polymer foams.

Quantifying uncertainty in analysis of shockless dynamic compression experiments on platinum. II. Bayesian model calibration

Dynamic shockless compression experiments provide the ability to explore material behavior at extreme pressures but relatively low temperatures. Typically, the data from these types of experiments are interpreted through an analytic method called Lagrangian analysis. In this work, alternative analysis methods are explored using modern statistical methods. Specifically, Bayesian model calibration is applied to a new set of platinum data shocklessly compressed to 570 GPa. Several platinum equation-of-state models are evaluated, including traditional parametric forms as well as a novel non-parametric model concept. The results are compared to those in Paper I obtained by inverse Lagrangian analysis. The comparisons suggest that Bayesian calibration is not only a viable framework for precise quantification of the compression path, but also reveals insights pertaining to trade-offs surrounding model form selection, sensitivities of the relevant experimental uncertainties, and assumptions and limitations within Lagrangian analysis. The non-parametric model method, in particular, is found to give precise unbiased results and is expected to be useful over a wide range of applications. The calibration results in estimates of the platinum principal isentrope over the full range of experimental pressures to a standard error of 1.6%, which extends the results from Paper I while maintaining the high precision required for the platinum pressure standard.

Quantifying uncertainty in analysis of shockless dynamic compression experiments on platinum. I. Inverse Lagrangian analysis

Absolute measurements of solid-material compressibility by magnetically driven shockless dynamic compression experiments to multi-megabar pressures have the potential to greatly improve the accuracy and precision of pressure calibration standards for use in diamond anvil cell experiments. To this end, we apply characteristics-based inverse Lagrangian analysis (ILA) to 11 sets of ramp-compression data on pure platinum (Pt) metal and then reduce the resulting weighted-mean stress–strain curve to the principal isentrope and room-temperature isotherm using simple models for yield stress and Grüneisen parameter. We introduce several improvements to methods for ILA and quasi-isentrope reduction, the latter including calculation of corrections in wave speed instead of stress and pressure to render results largely independent of initial yield stress while enforcing thermodynamic consistency near zero pressure. More importantly, we quantify in detail the propagation of experimental uncertainty through ILA and model uncertainty through quasi-isentrope reduction, considering all potential sources of error except the electrode and window material models used in ILA. Compared to previous approaches, we find larger uncertainty in longitudinal stress. Monte Carlo analysis demonstrates that uncertainty in the yield-stress model constitutes by far the largest contribution to uncertainty in quasi-isentrope reduction corrections. We present a new room-temperature isotherm for Pt up to 444 GPa, with 1-sigma uncertainty at that pressure of just under ±1.2%; the latter is about a factor of three smaller than uncertainty previously reported for multi-megabar ramp-compression experiments on Pt. The result is well represented by a Vinet-form compression curve with (isothermal) bulk modulus K0=270.3±3.8 GPa, pressure derivative K0′=5.66±0.10, and correlation coefficient RK0,K0′=−0.843.

A modified HJC model for geological materials subjected to blasting loadings

In this paper, a modified HJC model is proposed to address the problem that the HJC model cannot simulate tensile damage cracks. The modified HJC model modifies the strength surface, strain rate effect and damage model of the original HJC model, respectively. The modified model is embedded in LS-DYNA software for single and multiple finite element validation. The effects of different parameters on the modified HJC model stress–strain curves are analyzed in the single finite element validation. In multiple finite element verification, uniaxial and triaxial compression experiments, Brazilian disc splitting experiments, SHPB dynamic compression experiments, and SHPB dynamic splitting experiments are performed. The results of single and multiple finite element numerical validation illustrate that the modified HJC model can well simulate the pre-peak and post-peak nonlinear mechanical behaviors of geological materials such as rocks and concrete. Compared with the HJC model, the damage pattern of the modified HJC model is closer to the real damage pattern. For the strain rate effect, the modified HJC model can reflect the real compressive strain rate effect and improve the sensitivity of tensile strength to strain rate. The results of the numerical simulation of the blasting funnel illustrate that: the modified HJC model can simulate explosive tensile cracking well and can explain the formation mechanism of blasting funnel due to the distinction between tensile and compressive meridian surfaces and the addition of tensile damage. The modified HJC model is more applicable to the numerical simulation of engineering blasting.