With the growth of people's consumption capacity, the production and consumption of energy are rapidly increasing every year, and the emissions of nitrogen oxides are also increasing. Nitrogen oxides include many types of compounds, such as nitric oxide (NO), nitrogen dioxide (NO2), nitrous oxide (N2O), etc. Except for nitrogen dioxide, the properties of other nitrogen oxides are extremely unstable. Therefore, in the actual atmosphere, nitric oxide (NO) and nitrogen dioxide (NO2) are usually collectively referred to as nitrogen oxides (NOx). This article measured and compared the nitrogen oxide concentration and other meteorological indicators in the public, commercial, and civilian areas at the southwest corner of the city wall in Jingzhou City in March and April 2022. The following conclusions were drawn: the mass concentration of nitrogen oxide pollutants was highest around noon and evening, and the concentration was relatively small before and after sunrise and afternoon, with a "double peak and double valley" distribution. The nitrogen oxide concentration began to decrease at night and reached the first valley in the early morning, then it gradually rises, reaching its peak around 8:00 and then showing a downward trend. A second trough will appear around 13:00, followed by a continuous increase in concentration, and finally a small peak will appear at 18:00.