Disc Specimens Research Articles

Curculigoside upregulates BMAL1 to decrease nucleus pulposus cell apoptosis by inhibiting the JAK/STAT3 pathway

BackgroundIntervertebral disc degeneration (IVDD) is a natural process that occurs with aging and is the main cause of low back pain (LBP). Basic helix-loop-helix ARNT-like 1 (BMAL1) plays key roles in the pathogenesis of many diseases. The present study investigates the role of curculigoside (CUR), which has been reported to be a potential anti-apoptotic compound in other diseases. MethodsDysregulated genes were identified by RNA sequencing (RNA-seq). Western blotting (WB), immunohistochemistry (IHC), immunofluorescence (IF) staining, and real-time fluorescent quantitative PCR were used to detect BMAL1 expression in 25 human intervertebral disc (IVD) specimens (male: female =13:12), tissues from BMAL1-knockout mice and from an IVDD mouse model. The regulatory effects of CUR and BMAL1 in NP cells after siRNA transfection were examined by flow cytometry, IF staining and WB. The therapeutic effect of intraperitoneal CUR injection was also evaluated in mice. ResultsBMAL1 expression was negatively correlated with IVDD severity and was significantly lower in degenerative NP cells. After BMAL1 knockdown using siRNA, the apoptosis rate of degenerative NP cells was significantly higher, while transfection with a lentivirus overexpressing BMAL1 exerted the opposite effect. Bioinformatics analysis revealed that BMAL1 is regulated by the JAK-STAT3 pathway, and CUR upregulated BMAL1 expression by inhibiting STAT3 phosphorylation, subsequently alleviating NP cell apoptosis and increasing extracellular matrix (ECM) components., thus alleviating IVDD. ConclusionsCUR can inhibit apoptosis and improve the ECM by upregulating BMAL1 expression, which is reduced in IVDD. This study provides a therapeutic strategy to alleviate apoptosis associated with inflammation-induced IVDD.

Evaluation of ring test with reference to deformation rate and specimen geometry in assessing the tensile behaviors of granite

Ring test for indirect tensile strength measurements utilizes disc specimens with a hole at the center of the disc. Such specimens are found to limit the stresses at the specimen-platen contact and transfer the tensile stress to the upper- and lower-hole boundaries in ring specimens. Researchers observed that the tensile strength of a ring specimen tends to decrease as the ratio of the hole-radius to the disc-radius (ρ) increases. However, there has been no research on how the tensile strength derived from ring specimens varies when loaded under different quasi-static strain rates or deformation rates. The strain analysis in case of ring tests also does not seem to have gained attention. In this study, ring specimens of Malanjkhand granite (India) with varying ρ (0.13, 0.17, 0.21 and 0.25) were quasi-statically loaded at 0.5 mm/min, 1.5 mm/min and 5.5 mm/min corresponding to strain rates of 1.75 × 10−4 s−1, 5.26 × 10−4 and 1.93 × 10−3 s−1, respectively. The combined effect of the deformation rate and specimen geometry (ρ) on the indirect tensile strength and deformation behavior was investigated. The Ring Tensile Strength (RTS) is found to be higher than the Brazilian Tensile Strength (BTS). RTS shows dependency on both the geometry of the ring specimen as well as the deformation rate. The tensile Tangent Deformation Modulus (Dv) and the ratio of the horizontal strain to vertical strain, coined as Ring Strain Ratio (RSR), were estimated in this study from the tensile stress and vertical-horizontal strain data. A numerical finite element analysis was also performed in Abaqus to observe the stress distribution in both ring and Brazilian discs, where the results were found to be broadly conformable.

Flexural strength, surface roughness, and color stability of various CAD-CAM denture teeth materials.

To assess the flexural strength (FS), surface roughness, and color stability of additive manufactured (AM) and subtractive manufactured (SM) denture teeth materials, as well as the effect of thermocycling on these properties. Eighty strips (20/material type; 64×10×3.3mm) and 60 discs (15/material type; 12×4mm) were fabricated from four different denture teeth materials (Straumann, Flexcera, Ivoclar, and Candulor). The specimens were divided into two subgroups (nonthermal cycled and 5000 thermal cycled,10 per subgroup), and subjected to a 3-point test for FS using a universal testing machine at a crosshead speed of 5.0mm/min. Surface roughness (Ra, µm) and color differences (ΔE00) of disc specimens were measured before and after thermocycling using a noncontact optical profilometer and a spectrophotometer, respectively. The CIEDE2000 formula was used to calculate the color differences (ΔE00) before and after thermocycling. Data were analyzed using 2-way ANOVA followed by post hoc multiple comparison tests (α=0.05). There was no significant difference in flexural strength between nonthermal cycled SM materials (p=0.15), which were significantly higher than AM materials (p<0.001). The flexural strength values of all tested materials weresignificantly reduced after thermocycling (p<0.05). The material type had a significant effect on the Ra values (p<0.001), whereas thermocycling did not (p=0.81). After thermocycling, all materials exhibited color changes lower than the clinical perceptible threshold (ΔE00=2.7). Thermocycling decreased the FS of denture teeth materials manufactured with AM and SM, but did not affect the surface roughness. The FS values of SM groups were significantly higher than AM materials, irrespective of thermocycling. No clinically significant color changes of the denture teeth material were noted.

A comparative study of strength and surface properties of permanent 3D-printed resins with CAD-CAM milled fixed dental prostheses.

To compare the strength, surface roughness, and hardness of newly introduced permanent three-dimensional (3D)-printed resin in comparison with computer-aided design and computer-aided manufacturing (CAD-CAM) milled materials. Three 3D-printed resins (NextDent C&B, Formlabs Permanent Crown, and VarseoSmile Crownplus) and two CAD-CAM milled (IPS e.max ZirCAD LT and VITA Enamic) resins were used to fabricate discs specimens. A total of 200 disc specimens were fabricated according to manufacturer recommendations. Within each group, half of the specimens were subjected to thermal cycling (5°C-55°C, the 30s, 5000 cycles). Aged and nonaged specimens were evaluated for biaxial flexural strength (BFS), surface roughness, and hardness. Results were statistically analyzed using analysis of variance (ANOVA) and t-tests (α=0.05). Significant differences (p<0.05) were observed in the BFS, surface roughness, and hardness between the 3D-printed and milled groups, before and after thermal aging. Overall, the CAD-CAM milled ceramic group had superior strength, surface roughness, and hardness when compared to all other groups (p<0.001), except for surface roughness after thermal aging, which was similar in all groups (p=0.063). Within each group, there was no significant difference (p>0.05) in surface roughness after thermal aging. BFS values of 3D-printed materials were statistically similar. In terms of surface roughness, Formlabs specimens displayed the highest value before and after thermal cycling, when compared to other 3D-printed materials. Regarding hardness, the VarseoSmile Crown plus group demonstrated the highest values compared to other 3D-printed materials, before and after thermal cycling. Permanent 3D-printed resins have lower strength than CAD-CAM milled materials. 3D-printed permanent resin materials exhibited high roughness and comparable hardness to CAD-CAM materials. Thermal aging negatively affected the properties of 3D-printed permanent crowns. Owing to the low strength of 3D-printed permanent resins, they may not be recommended for clinical practice until further improvements in flexural strength are made to meet clinical standards.

Influence of substrate properties on fracture behavior of rock-concrete bi-material central interface cracked Brazilian disks at different loading angles

Rock-concrete (R-C) bi-material structures are crucial for safety in tunnel construction and similar projects. The load-bearing properties and fracture patterns of structures made of concrete combined with rocks of varying properties exhibit notable differences. This study conducts experiments and numerical simulations on R-C central interface crack Brazilian disk specimens, investigating the effects of rock type, interface crack length, effective modulus ratio, and tensile strength ratio on fracture behavior under different loading angles. Quasi-static compression tests were carried out on sandstone-concrete (S-C) and granite-concrete (G-C) specimens at varying angles, revealing significant differences in fracture patterns and load-bearing capacity. The fracture patterns of S-C show interface extension cracks, tensile wing cracks, and vertical tensile cracks, while, G-C specimens exhibit additional single-wing crack patterns; Peak loads increase with loading angle, with G-C specimens initially having lower peak loads than S-C specimens at angles from 0° to 15°, but surpassing them at higher angles. Then, discrete element models of R-C were constructed using PFC2D and validated with experiments. The influence of interface crack length on the fracture patterns of S-C and G-C specimens was initially investigated using numerical methods. Subsequently, fracture propagation simulations for R-C samples with varying effective modulus and tensile strength ratios were performed. The simulation results show that smaller interface cracks lead to more secondary cracks in concrete, resulting in a heightened degree of fragmentation. Increasing effective modulus and tensile strength ratios result in various crack patterns: interface propagation crack, wing crack in rock and concrete, wing crack only in rock or concrete, vertical tensile crack in rock and concrete, and vertical crack only in rock or concrete; The peak load shows an increasing and then decreasing trend with increasing effective modulus ratio, while with the increase of tensile strength ratio exhibits an increasing and then steadily changing pattern.

Fracture Characteristics and Tensile Strength Prediction of Rock–Concrete Composite Discs Under Radial Compression

To investigate the fracture mechanism of rock–concrete (R–C) systems with an interface crack, Brazilian splitting tests were conducted, with a focus on understanding the influence of the interface crack angle on failure patterns, energy evolution, and RA/AF characteristics. The study addresses a critical issue in rock–concrete structures, particularly how crack propagation differs with varying crack angles, which has direct implications for structural integrity. The experimental results show that the failure paths in R–C disc specimens are highly dependent on the interface crack angle. For crack angles of 0°, 15°, 30°, and 45°, cracks initiate from the tips of the interface crack and propagate toward the loading ends. However, for angles of 60°, 75°, and 90°, crack initiation shifts away from the interface crack tips. The AE parameters RA (rise time/amplitude) and AF (average frequency) were used to characterize different failure patterns, while energy evolution analysis revealed that the highest percentage of energy consumption occurs at a crack angle of 45°, indicating intense microcrack activity. Moreover, a novel tensile strength prediction model, incorporating macro–micro damage interactions caused by both microcracks and macrocracks, was developed to explain the failure mechanisms in R–C specimens under radial compression. The model was validated through experimental results, demonstrating its potential for predicting failure behavior in R–C systems. This study offers insights into the fracture mechanics of R–C structures, advancing the understanding of their failure mechanisms and providing a reliable model for tensile strength prediction.

Increasing accuracy in predicting mode I fracture toughness of rock structures: a comparative analysis of the rock engineering system method

The investigation of crack initiation and expansion is vital for the stability of structures. The Mode I fracture toughness (KIc) of rocks is a key property used to predict crack propagation in tension and hydraulic fracturing. Various methods have been introduced to determine KIc, but results differ due to factors like sample dimensions, crack geometry, groove type, and loading conditions. The cracked chevron notched Brazilian disc (CCNBD) sample is commonly used in laboratory tests for its easy preparation. This study employs the rock engineering system (RES) technique to overcome the challenges of time-consuming and costly laboratory tests and the uncertainty in traditional methods (analytical, numerical, experimental, laboratory, regression). Using 88 CCNBD rock samples proposed by ISRM, input parameters include thickness of the disc specimen (B), uniaxial tensile strength (σt), initial crack length (α0), radius of the disc specimen (R), crack length (αB), and the length of the final crack (α1). The RES-based model used 70 data points (80% of the dataset) for development, and 18 data points (20%) for evaluation. Regression analysis compared the performance of the RES method, using statistical indicators such as squared correlation coefficient (R2), mean square error (MSE), and root mean square error (RMSE) to measure accuracy. The RES-based method outperformed other regression techniques, demonstrating significantly enhanced accuracy. This highlights the effectiveness and superior performance of the RES method in estimating fracture toughness, particularly for CCNBD samples, showcasing its potential as a robust analytical tool.

A comparative study of polishing systems on optical properties and surface roughness of additively manufactured and conventional resin based composites

This study aimed to compare polishing systems on color stability, surface roughness, and gloss of additively manufactured permanent and conventional resin composites. Totally 250 disc specimens (6 mm*2 mm) were prepared from resin-based materials [G-ænial Posterior (GP), Clearfil Majesty Esthetic (CME), SonicFill-2 (SF), Tescera (Tes), and Crowntec (CT)]. Following baseline color (ΔE00), gloss (GU), and surface roughness (Ra) measurements, the specimens were randomly divided into 5 groups (n = 10/group) according to polishing systems: Control (mylar strips); OneGloss; OneGloss + Platina Hi-Gloss; OptiDisc; and OptiDisc + Platina Hi-Gloss. Specimens were immersed in coffee for 144 h following polishing. ΔE00, GU, and Ra measurements were repeated. Atomic force microscopy images were taken in all groups. Spearman’s rho correlation coefficient, Robust ANOVA, and Bonferroni correction were used for statistical analysis. Significance level was taken as p < 0.050. Significant differences in ΔE00 values were found among resin-based materials, polishing systems, and their interactions (p < 0.001,p < 0.01, and p = 0.001). Regardless of polishing system, the lowest ΔE00 values were observed in CT, while lowest gloss (GU) values were found in Tes. The lowest surface roughness (Ra) values were detected at OptiDisc group (p < 0.001). A single type of polishing system may not be sufficient to achieve optimal results in resin-based materials.

Fracture toughness of alkali-activated concrete subjected to aggressive environment

This study investigates the fracture toughness of alkali-activated granulated blast-furnace slag (GBFS)-based geopolymer concrete (GPC), non-activated slag cement concrete, and ordinary Portland cement (OPC) concrete in acidic, alkaline, and chloride solutions over six months. A total of 580 centrally straight-notched Brazilian disc (CSNBD) specimens were cast to assess pure mode-I (0°), pure mode-II (28.7°), and mixed-mode (15° and 45°) fractures under these conditions. Microstructural analyses (SEM) were performed to evaluate microstructural changes after six months of exposure. Results showed that GPC exhibited the lowest initial fracture toughness but the smallest reduction (7 %-11 % depending on the mode) across all environments, with slag cement concrete and OPC experiencing reductions of 11 %-14 % and 14 %-21 %, respectively, in acidic conditions. In alkaline environments, GPC showed a 3 %-6 % decrease in fracture toughness, while OPC and slag cement concrete showed reductions of 6 %-13 %. The gradient boosting regressor accurately predicted the failure load of CSNBD specimens, achieving an R² score of 0.948. Finally, SHAP sensitivity analysis identified concrete type, exposure time, and environment as critical input features, consistent with experimental results.

Investigating the influence of geometric configurations and loading modes on mixed mode I/II fracture characteristics of rocks: Part I-Numerical simulation

The influence of geometric configurations and loading modes is a bottleneck that restricts the accurate determination of rock fracture parameters and the precise understanding of fracture mechanisms. Therefore, the phase field method is employed to analyze the influences of specimen geometry and loading modes on the dimensionless stress intensity factors, peak load, fracture toughness, and crack initiation angle during the rock mixed mode I/II fracture process. Three new configurations of specimens are proposed to test rock mixed mode I/II fracture. The research results indicate that as the prefabricated crack inclination angle increases, the peak load of three-point bending type specimen increases, while the peak load of diametric-compression type specimen decreases. Moreover, the influence of geometric configurations on the fracture parameters of three-point bending specimens is greater than that of diametric-compression disk specimens. The research findings of this work can provide basic supporting data for the establishment of mixed mode I/II fracture testing standards.

Experimental study on fracture properties of heat-treated granite in I-II mixed mode suffered from water and liquid nitrogen cooling methods

Hot dry rock (HDR) development is significant for solving energy problems and realizing energy conservation and emission reduction. Liquid nitrogen (LN2) fracturing and hydraulic fracturing can form cracks in the HDR and improve the efficiency of geothermal energy mining. Therefore, it is necessary to study the fracture characteristics of high-temperature granite under different cooling methods. In this study, the deterioration of the physical and mechanical properties of granite subjected to high-temperature treatment under water cooling and LN2 cooling was studied. Two I/II mixed modes (tensile orientation mode and shear orientation mode) and a pure II mode fracture characteristics of cracked straight-through Brazilian disc (CSTBD) specimens made of granite were explored. The displacement and strain fields of cracked granite specimens were measured by using a digital image correlation (DIC) method. The results show that when the temperature is 25℃, 200℃, and 400℃, the loading angle and cooling method have a great influence on the fracture mechanical characteristics of the granite. In general, the increase of loading angle and LN2 cooling will lead to the decrease of peak load. For example, at 200℃, β = 15°, the deterioration degree of water-cooled and LN2-cooled specimens is 13.77 % and 16.69 %, respectively. When β = 23°, it increases to 14.62 % and 19.91 %, respectively. At the same time, an interesting phenomenon was found in the study. At 400℃, due to the Leidenfrost effect, the peak load of LN2-cooled specimens was higher than that of water-cooled specimens, and the further increase of temperature weakened the effect. When the temperature is 600℃, the difference between the loading angle and the cooling method is weakened.

Cracking evolution and failure mechanism of brittle rocks containing pre-existing flaws under compression-dominating stresses: Insight from numerical approach

Comprehending the cracking evolution and failure mechanism of flawed rocks under compression-dominating stresses is essential to evaluating the stability of rock engineering. In this work, a newly developed geometry-constraint-based non-ordinary state-based peridynamic (GC-NOSBPD) theory that can eliminate the numerical oscillation is applied to predict the development of new cracks of flawed rocks under compression-dominating stresses. The failure of bonds between particles is judged by the bond-associated stress-based fracture criteria. The cracking evolution trajectories of semi-disc and disc specimens containing flaws are traced. The effects of flaw inclination angle on the cracking trajectories are analyzed. The cracking evolution paths of rock-like specimens with two flaws under uniaxial and biaxial compression are molded. The effects of confining stress on the growth of new cracks are investigated. The confining stress restrains the propagation of tensile cracks, but it is easy to promote the growth of shear cracks. The concentration and transfer effects of stress can plainly revel the failure mechanism of flawed rocks. The present numerical method is reasonable to predict the tensile and shear failure modes of flawed specimens under compression-dominating stresses.

The effect of failure mechanics on the fatigue responses of lumbar intervertebral disc

Lumbar disc herniation is usually caused by the accumulation of long-term mechanical loads and sudden overload damage. Therefore, this study aims to illustrate how fatigue failure in lumbar spine segments is influenced by both cyclic loading magnitude and pre-existing damage. Eighty-six sheep intervertebral disc samples were divided into four groups to test the fatigue responses in healthy and damaged intervertebral discs. Both before and after fatigue loading, the specimens were performed on loading–unloading tests to analyze the viscoelasticity changes, while the specimens were performed on MRI examination to analyze the geometric and morphological changes. The Stress-Failure curve (SN curve) was examined, while the number of cycles to failure of damaged specimens was much smaller than that of healthy specimens at the same stress level during cyclic loading, and the relationship was approximately linear on a logarithmic scale. In addition, the healthy specimens will not accumulate fatigue failure if the compression force remains below 50% of the ultimate compressive tolerance (UTC). Before and after fatigue loading, the loading–unloading curves do not coincide and show obvious strain-rate-dependent viscoelastic characteristics, while the elastic modulus of the damaged specimen is significantly smaller. For magnetic resonance imaging, morphological changes included the changes of nucleus pulposus (NP) shape and area, while fatigue has a more significant effect on ruptured and herniated disc specimens. The dissipated energy of the intervertebral discs under cyclic loading was then calculated based on viscoelastic constitutive equations, which show that the load and preexisting damage both have significant effects on the dissipation rate.

Factors Influencing Measurement of Dynamic Elastic Modulus from Disk-Shaped Concrete Specimen

The decrease in dynamic elastic modulus is a primary indicator of quantitative damage in concrete. To quantitatively assess depth-by-depth damage within a concrete structure, cylindrical specimens obtained through coring can be cut into disk specimens to measure the dynamic elastic modulus of concrete at each depth. To minimize external damage during coring, it is essential to extract cylinders with the smallest possible diameter. In addition, for higher resolution in depth-based damage assessment, creating disk specimens with the smallest possible thickness is necessary. However, there is no information available in the literature on experimental limitation of smallest possible diameter and thickness for dynamic elastic modulus of disk-shaped specimens. This study evaluated whether the dynamic modulus measured from various sizes of concrete disk specimens provided sufficient reliability compared to reference values obtained from cylinders. Moreover, the study examined how the presence of coarse aggregate and variation in the water–cement ratio significantly influenced the dynamic modulus measurement. In addition, test results from impulse excitation technique (IET) and impact resonance (IR) were compared to find a more reliable test method for dynamic elastic modulus of disk specimen. The experimental findings revealed that as the thickness-to-radius ratio of the disk specimens decreased, measured data variation increased. Mortar specimens without coarse aggregates showed less variability compared to concrete specimens, and the variation in dynamic modulus measured by IR was lower than that measured by IET.

Effect of sintering cycle on the strength and translucency of multilayered zirconia.

A newly introduced sintering protocol promises to offer higher translucency while not significantly compromising the flexural strength of the material. However, the effect of the novel sintering protocol has not been thoroughly validated. The purpose of this study was to measure and compare the effect of two sintering protocols on the translucency and flexural strength of two multilayered zirconia materials. Two types of multilayered zirconia materials (ZirCAD Prime and Prime esthetic) were selected. Presintered disk specimens were obtained from Translucent, Gradient, and Dentin layers (n = 20). The disks were allocated to 2 groups: standard sintering protocol (peak temperature 1500°C) and high translucency sintering protocol (peak temperature 1600°C). After the sintering process, 10 specimens from each group were randomly selected. The optical values (L*, a*, b*) were measured and used to assess translucency using the relative translucency parameter (RTP00) and translucency differences (ΔRTP00). Then, all 20 specimens were tested for biaxial flexural strength. The outcomes were analyzed. The analysis of variance is used to analyze any significant effects on translucency and flexural strength. Then, any significant difference in the translucency and flexural strength between all pairs of materials was analyzed using Bonferroni-corrected Student's t-test (α = 0.05). The high translucency sintering protocol significantly decreased biaxial strength in the Prime translucent and dentine layer, Prime esthetic translucent, and gradient layer. RTP00 was significantly reduced in the Prime gradient and Prime esthetic gradient layer when sintered with a high translucency protocol. The lowest ΔRTP00 was observed in the Prime dentine layer, while the highest ΔRTP00 was observed in the Prime esthetic dentin layer. High translucency protocol significantly lowers the biaxial flexural strength of both multilayered materials, but the alteration in translucency is within clinically acceptable thresholds (TAT00 = 2.62).

Effect of Hydrogen Peroxide-Based Bleaching Agents on the Color Dimensions and Surface Roughness of Different Milled Restorative Dental Materials.

To compare the color dimensions, color discrepancies (ΔE00), and surface roughness of milled materials before and after application of a bleaching agent. A total of 10 extracted molars were obtained. Each tooth was cut in transverse sections to create disks (3-mm thick, 10-mm diameter; control group). Disk specimens of eight materials (n &#61; 10 per group) were fabricated: polymethyl methacrylate (PMMA) interim material (PMMA-Telio group), two resin nanoceramics (RNC-Ultimate group and RNC-Cerasmart group), two hybrid ceramics (HC-Shofu group and HC-Enamic group), lithium disilicate (LD-Emax group), zirconia-reinforced glass ceramic (ZGC-Suprinity group), and zirconia (Zr-InCeram group). Color measurements were obtained using a spectrophotometer before and after applying 35% hydrogen peroxide-based bleaching agent. Pre- and postbleaching surface roughness (Sa) analyses were completed using a profilometer. Significant L*, a*, b*, and ΔE00 value differences were found (P < .05). Color discrepancies (ΔE00) ranged from 0.30 ± 0.14 to 4.82 ± 0.10. The highest color discrepancies were measured on the PMMA-Telio group, while the lowest color discrepancies were computed for ZGC-Suprinity, RNCUltimate, and RNC-Cerasmart. Significant surface roughness differences were found (P < .05). The largest increase of surface roughness values between the pre- and postbleaching measurements was obtained in the PMMA-Telio group with a mean ΔSa value of 4.73 ± 3.02, while the largest decrease of surface roughness values between the pre- and postbleaching measurements was obtained in the Zr-InCeram group with a mean ΔSa value of -1.58 ± 0.10. The milled materials showed significant pre- and postbleaching color and surface roughness discrepancies.

Effect of aging on dimensional accuracy and color stability of CAD-CAM milled and 3D-printed denture base resins: a comparative in-vitro study

BackgroundThere is a lack of studies comparing the dimensional accuracy and color stability of denture base resins made using computer-aided design and computer-aided manufacturing (CAD-CAM) milling, 3-dimensional (3D) printing, and conventional denture processing techniques. This makes it challenging to determine the best method to fabricate complete dentures. The objective of this in vitro investigation was to assess and contrast the color stability and dimensional accuracy of denture base resins that were 3D printed and CAD-CAM milled, both before and after aging by thermocycling using digital surface matching technology and a benchtop laser scanner without using a spray, to optimize adaptation of the denture base and cast to minimize any imperfections and to evaluate the impact of the denture cleansing solution on the stability of color.MethodsEvaluation of the dimensional accuracy (n = 27) was completed on a sectional maxillary stone cast using a digital 3D-surface matching software before and after 5000 thermocycles. A spectrophotometer was used to measure the color change (△E00) of all disc specimens (N = 54) before and after 500 thermocycles and immersion in denture cleansing solution for 30 cycles (3 min each) daily for 6 days. The Kruskal Wallis test, Dunn’s post hoc test, Tukey’s test with Bonferroni adjustment, one sample t test and independent t test were used to statistically analyze the data (α < 0.05).ResultsThermocycling decreased the dimensional accuracy of the heat polymerized group at all 5 locations and the 3D-printed group at locations 1, 3 and 5 (P > .05), while it had no significant difference on the CAD-CAM milled group at all locations (P < .05). The color change (△E00) was lowest in the CAD-CAM milled group, moderate in the heat-polymerized group and highest in the 3D-printed group. After immersion in denture cleanser, the color change (△E00) was significantly higher in the 3 groups compared with after thermocycling (P > .001).ConclusionsCAD-CAM milled resins had the highest dimensional accuracy and the best color stability, conventional heat polymerized acrylic resins showed moderate change in dimensional accuracy and color stability, while the 3D- printed resin had the lowest dimensional accuracy and color stability after aging by thermocycling.

Investigation of Indirect Shear Strength of Black Shale for Urban Deep Excavation

This study thoroughly investigated the compressive and tensile strength characteristics of black shale using both experimental and analytical approaches. Uniaxial compression tests were conducted to determine the elastic constants of black shale modeled as idealized, linear elastic, homogeneous, and transversely isotropic. Additionally, Brazilian tests were carried out on shale, considering it a transversely isotropic material. Strain measurements were recorded at the center of disc specimens subjected to diametric loading. By placing strain gages at the disc centers, the five elastic constants were accurately estimated. The effects of experimental methods and diametric loading on the elastic constant determination were evaluated and analyzed, and the indirect shear strength of the black shale, considering anisotropy, was determined using the estimated stress concentration coefficient. This study revealed that the indirect tensile strength of black shale is significantly influenced by the angle between the anisotropic planes and the diametric loading direction. Moreover, it was revealed that the stress concentration coefficients for anisotropic rocks vary from those of isotropic rocks, depending on the inclination angle of the bedding planes. This study confirms that the shear (tensile) strength of anisotropic black shale is not constant but varies with the orientation of the anisotropic planes in relation to the applied load.

Investigation on dynamic splitting mechanical properties of weakly cemented siltstone based on digital image correlation method and FracPaQ algorithm

Soft strata composed of weakly cemented rock are frequently subjected to dynamic loads in underground energy mining engineering, yet the dynamic mechanical properties of these materials remain insufficiently explored. In this study, dynamic splitting tests were conducted on Brazilian disc specimens of weakly cemented siltstone to assess their dynamic mechanical and failure characteristics. The findings revealed that both dynamic strength and dissipated energy increased under higher stress rates. A dynamic splitting strength model for weakly cemented siltstone was subsequently developed based on the incubation time criterion. Additionally, the digital image correlation technology was employed to analyze strain variations during the initiation of the main crack, and the quantitative analysis of the fragmentation process indicated that average opening rates increased with rising stress rates. The FracPaQ algorithm was also applied to further characterize fracture patterns under varying stress rates, demonstrating that the Gaussian function accurately represented the relationship between deflection angles and fracture trace lengths. These research outcomes can provide essential mechanical parameters and a theoretical foundation for the safety assessment of weakly cemented rock strata in coal mining.

On the importance of the cracking process description for dynamic crack initiation simulation

A dynamic implementation of the coupled criterion under quasi-static loading, based only on the mean velocity during crack initiation, is proposed. It relies on a simultaneous node release method. It consists of computing the dynamic incremental energy release rate by simultaneously opening a crack of a finite length during a given time increment rather than progressively opening smaller crack increments following a velocity profile as in the progressive node release method. Both methods result in significantly different kinetic energy variations as a function of the crack length, and thus different incremental energy release rates for large enough crack velocities, for which the kinetic energy magnitude is similar to the elastic strain energy magnitude. Both simultaneous node release method and progressive node release method can however be equivalently used for small enough crack velocities since similar incremental energy release rates are obtained with both methods. Inverse identification of fracture properties based on dynamic crack initiation at a hole in Brazilian disk specimens yields critical energy release rates in the same order of magnitude as the one obtained based on dynamic crack propagation modeling.