Texture Evolution Research Articles

Achieving ultrahigh strength and ductility in biodegradable Zn-xCu alloys via hot-rolling and tailoring Cu concentration

In this present paper, a biodegradable Zn-xCu alloys with an ultrahigh strength and ductility can be achieved via hot-rolling and tailoring Cu concentration, and the role of Cu concentration on the microstructure and texture evolution in the Zn-xCu alloys during hot-rolling were investigated by XRD, EBSD and TEM analysis. The results show that the microstructure of as-cast Zn-xCu alloys consisted of large sized CuZn5 phase and Zn matrix grains before hot-rolling, and numerous submicron CuZn5 phase can dynamically precipitate during hot-rolling of Zn-xCu alloys. The existence of CuZn5 phase can result in the particle stimulated nucleation of recrystallization (PSN), and then result in the formation of fine recrystallized grains. Moreover, three texture components including 0001<112¯0>, 101¯1<1¯012> and 112¯0<0001> textures can form in the Zn-xCu alloys after hot-rolling. With boosting Cu concentration, the intensity of 112¯0<0001> texture gradually reduced, while the intensity of 0001<112¯0> and 101¯1<1¯012> texture components firstly raised with the augment of Cu concentration, and then reduced. For the Zn-xCu alloys with 8 wt%Cu concentration, a combination of high yield strength, ultimate tensile strength and elongation (269.7 MPa, 322.9 MPa and 26.3 %) can be achieved, which can meet the high-performance demands of biodegradable metal vascular stents.

Evolution of microstructure and properties of nanocrystalline NiCo alloy under high-energy laser shock

In this study, nanocrystalline NiCo alloy was prepared through electrodeposition and subjected to high-energy laser shock (HELS) treatment to investigate the influence of laser shock on the microstructures and properties. An analysis of phase composition, microstructural evolution, texture evolution, and hardness was conducted. The results indicated that under HELS, there was no change in phase composition, while there was a slight reduction in grain size, as well as in the quantities of Low-angle grain boundaries (LAGBs) and twin boundaries (TBs). The texture evolution revealed that HELS led to a more uniform overall texture due to grain boundary (GB) mediate deformation mechanisms, along with the generation of a significant amount of 9R phases, causing a shift in texture orientation from (110) to (100). The internal structure of nanocrystalline NiCo showed an accumulation of numerous dislocations post-laser shock, with randomly oriented dislocations interacting to form Lomer-Cottrell Locks (L-C Locks) and 9R phases. Additionally, interactions with large stacking faults (SFs) also resulted in their dissociation into multiple 9R phases. The hardness enhancement was mainly attributed to the accumulation of dislocations within the grain and the generation of a significant quantity of 9R phases.

Performance prediction of 304 L stainless steel based on machine learning

With the development of testing technology and data mining methodologies, machine learning (ML) has been widely applied for predicting the performance of materials in various systems including stainless steel with improved performance. To address the limitations of traditional experimental and statistical methods in predicting the thermal deformation of materials, a predictive machine learning model was developed based on the data obtained from thermal simulation compression tests. Specifically, the Arrhenius and the Modified Johnson-Cook (J-C) Constitutive Model were developed utilizing experimental data to initially predict the rheological behavior of 1.52% Cu-304L stainless steel. Then, a physical metallurgy (PM)-guided Back Propagation (BP) model was developed, and Genetic Algorithm (GA), Whale Optimization Algorithm (WOA), and Mind Evolutionary Algorithm (MEA) were incorporated into the model for optimization purposes, respectively. Finally, the results indicate that the PM-MEA-BP model exhibits superior predictive performance, accurately forecasting the texture evolution of 304L stainless steel with random crystal orientation under rolling deformation conditions. Additionally, the present work also clearly demonstrated that the model not only satisfies precision requirement but also has certain guiding significance for optimizing process parameters and forecasting the microstructure and properties of stainless steel.

Role of surface grain refinement in AZ31 Mg alloy by shot peening on surface energy, biomineralization and degradation behavior

Grain refinement of magnesium (Mg) alloys to improve their performance as potential candidates for degradable implant applications is a promising strategy in the field of materials engineering. Surface properties play an important role in promoting higher implant tissue interactions which dictate the healing rate of the fractured bone. In the present work, AZ31 Mg alloy was subjected to shot peening by using steel balls of 2 mm diameter. From the microstructural studies carried out at the cross section, fine grain structure was observed up to 50 μm depth from the surface. Grain refinement up to ∼1.5 μm was achieved at the surface of shot peened AZ31. X-ray diffraction analysis confirms the development of non-basal texture at the surface. Increased surface energy was measured by contact angle measurements for the shot peened AZ31. Higher hardness was measured from the surface in the thickness direction of the AZ31 after shot peening. Corrosion behavior assessed by potentiodynamic polarization tests indicated marginally increased corrosion resistance for shot peened AZ31. In vitro bioactivity studies carried out in simulated body fluids demonstrated higher mineral depositions and lower weight loss for the surface grain refined AZ31. The results demonstrate the potential of shot peening to promote higher biomineralization and to control the degradation in improving the performance of biodegradable AZ31 Mg alloy.

Evolution of microstructure, texture, and mechanical performance of Mg-13Gd-2Er-0.3Zr alloy by double extrusion at different temperatures

Evolution of microstructure, texture, and mechanical performance of Mg-13Gd-2Er-0.3Zr alloy by double extrusion at different temperatures

Electron Beam Additive Manufacturing of SS316L with a Stochastic Scan Strategy: Microstructure, Texture Evolution, and Mechanical Properties

This study examines the microstructure, crystallographic texture evolution, and mechanical properties of stainless steel 316L fabricated through electron beam melting using a stochastic scan strategy at a preheat temperature of 1123 K. X-ray diffraction confirmed the presence of a pure austenitic phase in the fabricated material. Equiaxed cellular structures were observed in the center of the melt pool regions and elongated cellular structures observed at the melt pool overlap regions. A finite element-based numerical model was employed to estimate the thermal gradients and solidification rates within the melt pool of an electron beam spot. Microstructural analysis indicated a generation of columnar grains from the bottom to the top of the build owing to high thermal gradients. A crystallographic texture investigation showed a generation of strong &lt;110&gt; fiber texture along the build direction of the material and reported that the stress distributions within the melt pool led to a strong crystallographic texture driven by the stress evolution observed from thermokinetic computational modelling of the electron beam-melting process. Mechanical properties were assessed using profilometry-based indentation plastometry, demonstrating strain hardening at a high temperature of 773 K.

Atomic‐Scale Order and Disorder Induced Diverse Topological Spin Textures in Self‐Intercalated Van der Waals Magnets Cr1+δTe2

AbstractThe intercalation of magnetic atoms into van der Waals (vdW) gaps offers a versatile approach for manipulating local magnetic ordering in vdW magnets. However, these intercalated magnetic atoms are often intricately positioned within the gaps, resulting in an ambiguous impact on local magnetic interactions and spin configurations. Herein, the atomic and magnetic structures of self‐intercalated prototype materials Cr1+δTe2 are comprehensively investigated using transmission electron microscopy, elucidating the correlation between the concentration and distribution of intercalated Cr atoms and the evolution of spin textures. The observed transitions from topological Néel‐type skyrmions to non‐topological type‐II bubbles, and ultimately to trivial ferromagnetic domains, underscore the complex nature of these magnetic spin textures. The complexity of the local structural arrangements is further revealed through integrating atomic‐resolution imaging, revealing the disorder‐order‐disorder transitions manifested by the distribution of intercalated atoms. The modulation of intercalated atomic structure shapes the observed spin textures by affecting the Dzyaloshinskii−Moriya interaction (DMI), inter/intra‐layer coupling, and magnetic anisotropy. These findings provide profound insights into the structure‐magnetism relationship, offering promising avenues for engineering the magnetic properties of vdW magnets at the atomic level.

The Evolution of Cube Texture in Directionally Solidified Fe-3.0 wt. % Si Alloy Assisted by a High Static Magnetic Field

The Evolution of Cube Texture in Directionally Solidified Fe-3.0 wt. % Si Alloy Assisted by a High Static Magnetic Field

Rules to identify and track the evolution dynamics of [formula omitted] twin variants in hexagonal close-packed metals

Twinning evolution laws derived based on physics are required to model plasticity and texture evolution resulting from the twinning in hexagonal close-packed structures. Atomistic simulations are employed to study the evolution of {101̄2} twins in Ti at 5 K temperature. The misorientation angle between the twinned region and parent matrix differs from the expected misorientation angle of 85.03∘. This closely aligns with the experimental findings. The deviation of twinning from {101̄2} twin plane makes it difficult to identify conjugate twins, leading to their coalescence. Both the c-vector and disorientation angle analyses are unable to track the variant type of the conjugate twins. The disorientation angle analysis can identify the conjugate twin variants but is unable to identify the variant type of the twin. The c-vector analysis can identify the conjugate twin variants as well as the variant type of the twin but is unable to track the variant type of the twin during its evolution. A set of rules are proposed to track the variant type of the twin during its evolution. These rules should help to understand the twin evolution dynamics in HCP metals and can be applied to study the twinning evolution dynamics at ambient conditions, even though they are designed for twinning evolution at 5 K temperature. The fundamental understanding of twin evolution dynamics should motivate the construction of the physics-based evolution laws for twinning.

Microstructure evolution and grain refinement mechanism of 316LN steel

Abstract The hot compression behavior of 316LN stainless steel for the supporting system in a magnet confinement fusion reactor was isothermally compressed at 1,050℃ and 0.1 s−1. Electron backscatter diffraction was used to study the microstructure and texture evolution during the deformation process. The results showed that the necklace structure is eventually formed by increasing compression strain due to dynamic recrystallization (DRX). The proportion of low-angle grain boundaries first increases and then decreases. The dominant DRX mechanism of 316LN is discontinuous DRX, which is characterized by the grain boundary bulging. Besides, twinning is found to be induced to accommodate the plastic strain, helping the development of DRX.

Evolution of microstructure and texture during severe plastic deformation of the aluminium alloy AA2099

Evolution of microstructure and texture during severe plastic deformation of the aluminium alloy AA2099

The dynamic of magmatic system and volcano hazard implications of the Damavand volcano (N. Iran) inferred from the textural data

The Damavand stratovolcano (N Iran) consists mainly of lavas with trachyandesite-trachyte composition, and subordinate pyroclastic deposits. The intensity of explosive eruptions and the volume of pyroclastic deposits have increased over time, which may be related to increasing viscosity due to the development of crystal-rich magmas. This research integrates microanalytical and quantitative textural measurements to understand the textural evolutions from the old to the young lavas and their relationships with the physical processes occurred in the plumbing system. Age-constrained samples from the lavas were analyzed using crystal size distribution (CSD), the newly proposed multifractal analysis, including the Number-Length of crystals (N-LoC) and the Number-Area of crystals (N-AoC), along with mineral chemistry. Three to five populations of feldspars can be identified, which have undergone evolution and coarsening over time. We propose a textural development sequence established at mid to shallow crustal levels, involving several physicochemical processes, such as cycles of polybaric differentiation and episodic magma recharge into the crystal-rich magma chambers. This, in turn, caused disaggregation of crystal mushes and textural coarsening due to crystal aggregation and temperature cycling. The increasing population of microphenocrysts in younger lavas may be linked to pulsating groundmass crystallization resulting from degassing at a newly formed shallow chamber (0.5–1 kbar) beneath the young cone. The final stages of crystallization occurred during multi-step decompression in the conduits. The comparison of age data from lava samples and their stratigraphic positions suggests that triggering groundmass crystallization might have caused shifts in eruptive behavior.

The development of crystallographic texture during porthole die extrusion of Al-Mg-Si alloys

The development of crystallographic texture during porthole die extrusion of Al-Mg-Si alloys

Texture Evolution of α‐Ti and β‐Ti Alloys During Rolling and Recrystallization

Texture Evolution of α‐Ti and β‐Ti Alloys During Rolling and Recrystallization

Mechanism of microstructure and texture evolution during hot rolling of pure Mg and Mg-0.2%Ce alloy

ABSTRACT The extruded samples of pure Mg and Mg-0.2%Ce alloy were subjected to a 90% reduction in thickness at 250°C during hot rolling. The microstructure, texture, and mechanical properties of the hot-rolled samples were evaluated. The microstructural evolution shows the presence of shear bands in Mg-0.2%Ce alloy at an angle of 30-35° concerning the normal direction and no such bands are observed in pure Mg. Upon annealing the samples at 400°C for one hour, it is observed that the grain size of Mg-0.2%Ce is smaller than pure Mg indicating that the precipitates of Ce arrest grain boundary mobility. The ex-situ EBSD microstructure analysis results show a higher change in the value of α33 components after annealing for pure Mg compared to Mg-0.2%Ce alloy suggesting the precipitates of Mg12Ce stabilises the pyr. <c + a > dislocations. The basal texture is observed in both samples after hot rolling. The experimental texture was simulated using the visco-plastic self-consistent (VPSC) modelling where it is observed that the initial extruded texture is favourable for the higher activity of pyr. <c + a > dislocation and extension twinning in Mg-0.2% e alloy. Further, the yield locus shows that Mg-0.2%Ce alloy shows relatively lower anisotropy compared to pure Mg. The yield strength and UTS of the pure Mg are higher than the Mg-0.2%Ce alloy which is attributed to the relatively more dislocation-dislocation interaction in pure Mg compared to Mg-0.2%Ce alloy resulting in the lower mean free path of the dislocations in pure Mg.

Analysis of the Ni-5%at.W Alloy Substrate Texture Evolution at Different Strain Levels Using the EBSD Technique.

In this paper, the texture evolution of the Ni-5%W alloy baseband with different strain variables (εvM = 3.9, 4.9, and 5.1) during rolling and annealing was studied using the electron back scattering diffraction (EBSD) technique. The results indicate that after high-temperature annealing at 1150 °C, all three strain levels of the alloy substrates can achieve a strong cubic texture, with a content exceeding 99% (<10°). However, the texture evolution trajectory is significantly influenced by the strain level. When the content of cubic texture in the alloy substrates under strain levels of 3.9 and 5.1 is the same, significant temperature differences exist. Additionally, the different strain levels result in varying nucleation rates and growth rates of cubic texture in the Ni-5%W alloy substrates. The study reveals that in the alloy substrates under strain levels of 3.9 and 4.9, recrystallized cubic grain nuclei grow within a layered structure, resulting in larger grain sizes and lower nucleation rates. In contrast, in the alloy substrates under a strain level of 5.1, recrystallized cubic grain nuclei form from small equiaxed grains, leading to higher nucleation rates but smaller grain sizes, competing with random orientations. In the later stages of nucleation, recrystallized grains in the alloy substrates under a strain level of 5.1 exhibit a significant size advantage, rapidly growing by engulfing randomly oriented grains. Compared to the alloy substrates with lower strain levels, the recrystallized cubic grains in the alloy substrates under a strain level of 5.1 have higher nucleation rates and faster growth rates.

In-situ synchrotron high energy X-ray diffraction study on the deformation mechanisms of D019-α2 phase during high-temperature compression in a TiAl alloy

The α2 phase with an ordered hexagonal structure has a strong mechanical anisotropy. The limited plasticity interacting with crystallographic texture formation undoubtedly complicate the deformation mechanisms of the α2 phase. Taking advantage of in-situ synchrotron high energy X-ray diffraction (HEXRD), this study unveils the origin of the α2 texture and its correlation with plastic deformation. Upon loading at 800 °C, the dislocation glide in the γ phase initiates at a stress of 370 MPa and that in the α2 phase at a stress of 670 MPa. Nevertheless, the texture evolution of the α2 phase sets in in parallel with that of the γ phase, and these textures are preliminarily established at a stress of 650 MPa. A main <11 2‾ 0> fiber texture with the c axis of the α2 unit cell aligned vertically to the compression axis has been unexpectedly evolved. This texture forms primarily via rigid body rotation and is correlated with glide and twin activation in the neighboring γ phase. The preferential orientation primarily favors double prismatic glide in α2 and in addition triggers the tensile twin activation. The grain rotation caused by the tensile twin slightly affects the α2 transverse texture evolution. The results unveil a complex interaction between the α2 phase deformability, texture evolution and the combined elastic-plastic deformation of the phases γ and α2 in TiAl alloys.

Key Sputtering Parameters for Precursor In2O3 Films to Achieve High Carrier Mobility.

Owing to their extremely high carrier mobility (μ) of >100 cm2/(V s) and suitable low carrier concentrations, transparent conducting films of solid-phase crystallized H-doped In2O3 (spc-IO:H) exhibit high conductivity with high optical transparency over a broad frequency range. These properties can be attributed to solid-phase crystallization of the amorphous precursor film. Therefore, the development of high-quality spc-IO:H films requires the deposition conditions of the precursor films to be optimized. This study systematically investigates the effects of three key sputtering parameters, namely, water vapor partial pressure (PH2O), radio frequency magnetron sputtering power (PRF), and flow ratio of O2 to total sputter gas (fO2) on the crystallographic texture evolution of spc-IO:H films during solid-phase crystallization. In addition, the carrier transport in the resulting films is examined. PH2O, PRF, and fO2 are found to be indispensable for producing high-mobility (>100 cm2/(V s)) spc-IO:H films. Furthermore, it is found that introducing a small amount of PH2O during deposition, a lower PRF, and a suitable fO2 facilitates the formation of precursor films having a lower crystallite density. Moreover, after annealing at a temperature of 200 °C, the IO:H precursor films with a lower crystallite density are found to have larger crystal grains. However, the μ values of the postannealed IO:H films are mainly correlated with the stoichiometric deviation.

Effect of deformation temperature on the microstructure and texture evolution of Ti-6Al-4Zr-2Mo-6V alloy

In this work, the effect of deformation temperature on the microstructure, texture, and tensile properties of a Ti-6Al-4Zr-2Mo-6V (wt. %) alloy was systematically investigated. The whole samples were composed of an equiaxed α phase, a strip α phase, and a β transformed microstructure. The recrystallization area fraction increased with the increase of deformation temperature. The orientation distribution of a retained β phase was {001}β⟨110⟩β texture regardless of deformation temperature. The textured microstructure of an α phase was {12¯10}α⟨101¯0⟩α under the 810 and 840 °C condition. Additional {112¯0}α⟨0001⟩α texture was observed as the rolling temperature increased to 870 °C. The yield strength and the tensile strength of a rolling direction were lower than that of a transverse direction. The yield strength of a rolling direction and a transverse direction were both above 990 MPa when the deformation temperature was 840 °C. In summary, the present study provided theoretical guidance for the high strength titanium alloy applied for the marine engineering field.

Full active counter-roller spinning for thin-walled cylinders: Macroscopic deformation mechanism, mesoscopic texture evolution, and forming performance strengthening

The reliability and lightweight of hydrogen high-pressure storage present pressing global challenges. The forming mechanism of a novel full active counter-roller spinning (FACRS) process for thin-walled cylinders is studied from the perspective of macro‑meso coupling. This innovative process holds promise as a replacement for conventional mandrel spinning, enabling enhanced integration of form and property in manufacturing hydrogen bottle liners. Employing optimal Latin hypercube sampling, a response surface model is constructed for forming consistency (λ) of inner and outer surfaces, yielding an optimal set of process parameters under the Hooke-Jeeves algorithm. The resulting spun parts exhibit a more balanced and superior performance. A macro‑meso gradual cross-scale coupling simulation methodology is proposed, revealing that the process is characterized by the initial aggregation and subsequent reinforcement of texture, culminating in the formation of a "soft" rotated cubic texture, which still faces impediments or diminishes the orientation of texture. It is demonstrated that the evolution of texture is the result of the interactive coordination of various slip systems. Furthermore, the FACRS experiments and performance tests indicate that while enhancing the axial and circumferential mechanical properties of the spun parts, it also reduces material anisotropy. The grain refinement effect of the process has also led to a more uniform distribution of dimples on the fracture surface. The surface performance of the final spun parts improves by 60.11 %. These enhancements can be attributed to the combined effects of improved forming consistency, coordinated action of slip systems, and grain refinement. These results deepen the understanding of the macro‑meso deformation mechanisms underlying the novel process, providing valuable insights for further advancements in counter-roller spinning technology.