Development Of Residual Stresses Research Articles

The effect of fine particle peening on aviation gear performance, Part I: Surface integrity

AbstractAs a fundamental component of aviation equipment, the gear has an essential effect on the service performance of the whole machine. Fine particle peening (FPP) technology is a good choice for the precision requirements of aviation gears. Therefore, a FPP model of aviation gears was constructed based on the discrete element‐finite element coupling method (DEM‐FEM) to simulate the evolution of surface roughness and residual compressive stress, and its results were verified by experiments. The effects of FPP intensity, coverage rate, and particle diameter on surface integrity were investigated. In addition, the importance degree of the intensity, coverage rate, and particle diameter of FPP on surface integrity was carried out by the random forest decision method. It demonstrates that the surface roughness Sa was mainly influenced by the FPP intensity and particle diameter. And the distribution state of the residual compressive stress was mainly affected by the particle diameter.

Effect of heat treatment processes on the Cu-electrodeposited through glass vias (TGV) plate

Based on laser-induced deep etching technology and through-hole filling techniques, TGV interposers were successfully fabricated. The residual stress in the Cu overburden film directly affects the yield improvement after subsequent grinding of the interposer. Therefore, we studied the evolution of residual stress, microstructural changes, and micro-nano mechanical properties within the Cu overburden film after heat treatment at different temperatures. Residual stress analysis using the sin2Ψ method with an X-ray diffractometer (XRD) indicates that during the process of increasing temperature from 100°C to 200°C, the internal residual stress in the Cu overburden film changes from compressive stress to tensile stress. Furthermore, the maximum absolute value of the residual stress, 70.09 MPa, appears at room temperature, and the minimum absolute value of the residual stress, 15.59 MPa, occurs after the heat treatment process at 200°C. Electron backscatter diffraction (EBSD) microstructural analysis shows that the application of heat treatment can effectively accelerate static recrystallization (SRX), promote a higher proportion of high-angle grain boundaries (HAGB), and refine grain size. Additionally, a (001) preferred orientation at high residual stress states and a (111) preferred orientation at low residual stress states are observed. Nanoindentation test results indicate that the Cu overburden film treated at 100°C has the most potential for removal during the grinding process.

Phase transformation effect on residual stress development in fusion welding of dissimilar stainless steels with different thickness

Phase transformation effect on residual stress development in fusion welding of dissimilar stainless steels with different thickness

Evolution of 2-inch AlN single crystal grown on SiC seed via PVT method

The crystallization of aluminum nitride (AlN) hetero-epitaxial seeding on silicon carbide (SiC) by physical vapor transport (PVT), was systematically studied using XRD, UV–Vis, PL, SIMS, Raman and stress simulation. The evolution of crystal quality, transmittance, purity and residual stress of 2-inch AlN crystal in the growth process are described. The crystal quality of AlN growth layer gradually improves with the crystal thickness, as reflected in the decrease of XRD full width at half maximum (FWHM) from higher than 300 arcsec to 85 arcsec, SIMS yielded Si concentrations decreases from 1020 cm−3 to 1018 cm−3, absorbance coefficient @320 nm from 56 cm−1 to 9 cm−1, and simulated residual stress from 270 MPa to 50 MPa, indicating a comprehensively improved quality by simply increasing the crystal thickness of AlN crystal on SiC seed. Furthermore, a 2-inch crack-free AlN single crystal with high quality was successfully fabricated by inducing a layered structure.

Multimethod cross-sectional characterization approaching the limits of diamond monophase multilayers

Chemical vapour deposited diamond draws significant scientific interest due to its wide range of mechanical and functional properties, which can be easily tuned by the applied deposition conditions. Here, hot filament chemical vapour deposition was used to synthesize four monophase multilayer diamond thin films with individual layer thickness down to ∼ 300 nm. Extensive structural characterization by scanning electron microscopy and Raman spectroscopy on the cross-section confirmed the different diamond morphologies originating from the different applied process parameters of the individual sublayers, where Raman spectroscopy could give a clear distinction between nano- and microcrystalline diamond down to a layer thickness of ∼ 1 μm. Cross-sectional X-ray nanodiffraction identified exclusively the diamond crystal structure throughout the cross-section of the multilayered diamond thin films. Cross-sectional phase and FWHM analysis allowed to discriminate between the diamond morphologies down to ∼ 500 nm, thus identifying the limitations of monophase diamond multilayers. While the microcrystalline diamond sublayers all exhibit pronounced structural gradients expressed in (i) increasing intensity of the 111 Debye-Scherrer ring, (ii) ⟨110⟩ fibre texture, and periodic variations of (iii) grain size and (iv) residual stress, the nanocrystalline diamond sublayers showed no pronounced cross-sectional variations. In summary, the experimental results provide insights into the cross-sectional evolution of microstructure and residual stress and the limitations of monophase multilayered diamond thin films.

Synchrotron EDXRD strain-temperature measurement during laser welding

Synchrotron EDXRD strain-temperature measurement during laser welding

Formation mechanism and evolution of interfacial residual stress between composite propellant and rubber liner during curing process

This study focuses on the solid rocket engines, which are commonly used in satellite launches and space exploration. The residual stress at the interface between the composite propellant and rubber liner generated during the curing process can lead to several issues, such as debonding, shrinkage, and deformation. This study aims to examine the mechanism and evolution law of the residual stress development. A finite element model is established to examine the residual stress during the full curing process. The composite propellant undergoes intricate temperature and curing gradients. The stress in various parts of the propellant and liner is monitored throughout the entire curing cycle. The propellant's temperature exhibits a delayed response during the heating and cooling phases of the curing process. The interface undergoes curing throughout the stage of constant temperature, with its chemical shrinkage primarily taking place prior to the cooling step. Considerable stress exists at the contact before cooling. The stress caused by thermal influences becomes more noticeable during the cooling phase. The influence of propellant composition and curing process parameters on interface stress is investigated. In addition, a specific vision-based device is innovatively designed to monitor deformation changes during the curing process. The key parameters of the simulation are optimized by combining the detected deformation, aiming to minimize the deformation difference between the experiment and the simulation, so as to realize the corresponding stress evaluation. The measurement results show an average deformation error of 10.71% and an average stress error of 10.58%.

Matrix curing and stress field development around fiber during the solvent evaporation-induced repolymerization of recycling composites

When recycling fiber-reinforced composites using depolymerized polymer solutions, oligomers reconnect through covalent bond exchange reactions (BERs), which ultimately forms a crosslinked network with mechanical properties comparable to those of virgin materials. This process offers exciting opportunities for the primary recycling of engineering composites, but it is intricately influenced by a few material and process parameters, such as heating temperature, duration, and fiber volume fractions. These parameters collectively determine the matrix's curing degree and the evolution of stress fields around the fiber, which are significant factors determining the quality and mechanical performance of recycled composites. This study introduces a diffusion-reaction-mechanics finite-element computational model to examine the solvent-induced repolymerization process in recycling composites. The model predicts the matrix curing degree, residual stress development around the fiber, and the composite's mechanical properties, aligning with experimental results. Parametric computational studies are then conducted to assess the influences of temperature, fiber content, solvent diffusivity, and the reactivity of BERs. The objective is to identify material and processing conditions that ensure efficient composite recycling while minimizing the development of residual stress. Overall, this study enhances our understanding of the mechanisms behind composite recycling using organic solvents and provides valuable insights for industrial stakeholders looking to optimize processing conditions and advance the commercialization and widespread adoption of this innovative recycling technique.

The Effect of the Deposition Strategy and Heat Treatment on Cold Spray Additive Manufactured 316L Stainless Steel

Herein, the effect of heat treatment on the characteristics and properties of cold spray additive manufactured 316L stainless steel employing traditional and a new metal knitting strategy is investigated. 316L feedstock powder characteristics, the geometry of the bulk, microstructure, porosity, microhardness, mechanical isotropy, and residual stress are analyzed in both strategies in as‐sprayed and heat‐treated conditions. Results show that the traditional deposition strategy produced higher mechanical resistance, whereas metal knitting presents a better part geometry accuracy. The heat treatment significantly improves the material strength and the quality of the parts by recovery and recrystallization phenomena. The same microhardness and planar isotropy are achieved after heat treatment of samples produced by both strategies. A discussion about the mechanisms, microstructural, and residual stress evolution is presented.

Residual stress in air-plasma-sprayed thermal barrier coatings under long-term high-temperature oxidation

The accumulated residual stress in yttria-stabilized zirconia top coat (YSZ TC) and thermally grown oxide (TGO) is regarded as the key driving force for the delamination of air-plasma-sprayed thermal barrier coating system (APS-TBCs). In this study, the synchronous evolution of residual stress of both YSZ TC and TGO, as well as the TGO thickness, are characterized via the Raman spectroscopy (RS) and photoluminescence piezo-spectroscopy (PLPS) methods. For the APS-TBCs where one surface is coated with YSZ TC, while the other surface remains directly exposed to high temperature, the service life can be categorized into four distinct stages: the early stage with tensile stress state (0–40 h), the medium stage with reversal compressive stress state (40–100 h), the late stage with re-inverted tensile stress (100–140 h), and the final stage with compressive stress state (140–300 h). Such stress reversal phenomenon may be attributed to the competition between the growth of TGO and substrate oxide (SO). It is advisable to apply an oxidation-resistant coating on the inner wall of high-temperature blade cooling passages, to prevent the formation of SO and consequently avoid complex stress transitions during high-temperature service of the APS-TBC, ultimately preventing local stress concentration-induced cracking and delamination.

Identifying multiple synergistic factors on the susceptibility to stress relaxation cracking in variously heat-treated weldments

The 347H austenitic stainless steel has been widely used for pressure vessels and pipeline (PVP) applications due to its excellent creep and corrosion resistance, which fit ideally to the harsh conditions in petrochemical industries, fossil fuel or nuclear power plants, and modern energy storages. However, a failure mode has been commonly observed with cracks emerging at the heat affected zone (HAZ) of weldments during post-weld heat treatment (PWHT) or under intermediate to high temperature service conditions. This phenomenon is termed as Stress Relaxation Cracking (SRC) since the purpose of PWHT is to relieve the welding-induced residual stress fields, or as Stress Age Cracking (SAC) if failure happens during service. A leading literature explanation of this failure suggests that the residual stress relaxation and the precipitation dissolution and/or re-precipitation occur in the same temperature range, which can lead to locally high strains and thus to crack at the grain boundaries. Since in situ spatial measurements of residual stress fields, microstructural evolution, and failure processes are nearly infeasible, this work recourses to a micromechanical finite element framework that models the high temperature failure as the nucleation and growth of grain boundary cavities, whereas various parameters such as thermomechanical loading history and its evolution, the competition of grain-interior dislocation creep and grain-boundary diffusion in failure lifetime, and microstructural heterogeneities (such as the precipitate free zone near grain boundaries) can be quantitatively incorporated. It can be concluded from these microstructure-explicit simulations that an accurate knowledge of residual stress evolution and a carefully calibrated set of material constitutive parameters are the essential prerequisites for lifetime predictions. The understanding of individual governing factors also leads to a mechanistic interpretation of the observed SRC susceptibility C-curves. These results suggest that the criticality of residual stress evolution, but not the precipitation-induced local strains, be the leading factor for SRC.

Optimizing SLM process parameters using FE analysis for distortion mitigation

The investigation aimed to determine the optimal value of process parameters to minimize distortion while reducing the overall printing time. To achieve this, different combinations of process parameters are selected, and 25 sets of FE experiments are prepared using an orthogonal matrix. The coupled thermomechanical analysis with the element birth technique is used to mimic the behavior of Selective Laser Melting (SLM). Initially, a mesh convergence study is performed to reduce computation time with the least sacrifice in results. To minimize the temperature gradient, simulations are performed at different levels of bed temperature ranging from 303 K to 843 K. The minimum distortion was observed for a higher bed temperature of 843 K, as at this temperature, the gradient in temperature is minimum, resulting in the least development of residual stresses. The interactive behavior between laser power and scanning speed is studied, revealing an approximately linear trend with respect to distortion while keeping all other parameters constant. Additionally, it was observed that laser power and layer thickness also exhibited a similar linear trend with respect to distortion. To identify the optimal process parameter value within the design space, the Multi-Island Genetic Algorithms (MIGA) technique is employed, leading to a remarkable minimum distortion of 0.45 mm for a specific set of input process parameters.

A promising approach to enhance fatigue life of TC11 titanium alloy: Low dislocation density and surface grain refinement induced by electropulsing

The fatigue life of components can be significantly enhanced by the formation of the surface hardness layer through surface strengthening technology. To avoid the geometric distortion of thin-walled components caused by strengthening, the strengthening energy is limited and the ideal strengthening effect cannot be obtained. This work aims to propose a novel approach to address this issue effectively. The surface layer with high-density dislocations was obtained by a low-energy surface strengthening method (shot peening) at first. Then the surface strengthening mechanism changes from dislocation strengthening to grain boundary strengthening after electropulsing treatment (EPT). The evolution of residual stress and microstructure was analyzed using multi-scale characterization techniques. The results demonstrate that EPT followed by surface strengthening makes a remarkable 304 % increase in fatigue life of TC11 titanium alloy. The enhancement of fatigue life can be attributed to the grain refinement accompanied by the formation of nanotwins and sub-grains in the surface-strengthened layer, as well as the reduction in dislocation density within the substrate after EPT. This study demonstrates the significant potential of EPT in further enhancing the fatigue life of surface pre-strengthened thin-walled components.

Characterization of structural and mechanical properties of HfNbTaTiZr refractory high entropy alloy after gas nitriding

This study was initiated to improve surface hardness and wear resistance of a HfNbTaTiZr refractory high entropy alloy (RHEA) by gas nitriding at a medium temperature (600 °C) for 3 h. Structural characterizations conducted by X-ray diffractometer (XRD), X-ray photoelectron spectroscopy (XPS) and energy dispersive spectroscopy (EDS) equipped scanning electron microscope (SEM) revealed that nitriding led to formation of a 1.5 μm thick surface layer containing precipitates of oxides and nitrides of the alloying elements. Detection of oxides within the surface layer was attributed to the presence residual oxygen in the nitriding atmosphere. Nevertheless, the employed gas nitriding provided remarkably higher scratch resistance compared to the untreated state, as the results of increment in the surface hardness and development of larger compressive residual stress.

Finite element simulation and experiment of residual stress evolution in MEMS structures

The MEMS device structure is usually formed by the combination of thick film and thin film deposition of many different materials, and the residual stress generated in the process of integration/superposition of different materials has a significant impact on the performance and reliability of the device.In this study, a test structure of a multilayer thin film was designed and processed. Based on this, finite element modeling analysis and reliability experiment, analyze the evolution of residual stress and construct the corresponding theoretical analysis model. The finite element modeling analysis can characterize the evolution and distribution laws of residual stress. The reliability experiment is mainly by carrying out the temperature shock experiment, and measuring the resistance value, resonance frequency and the surface morphology of the device, so as to better reflect the change of residual stress. Through this study, the resonant frequency and surface morphology of the device can reflect the residual stress of the device, which provides help for the test and analysis of the residual stress. To a certain extent, it can help reduce the harm caused by the residual stress in the design and manufacturing process, and improve the performance and reliability of MEMS devices.

A study on the thermal cyclic behavior of NiCrAlY coatings via femtosecond laser remelting with high repetition rate

NiCrAlY coatings are widely applied bond coatings in thermal barrier coating systems to prevent high-temperature oxidation of turbine blades. However, the uncontrollable microstructure design and high surface roughness seriously affect the oxidation resistance. Herein, NiCrAlY coatings fabricated through arc ion plating were subjected to high-repetition-rate femtosecond laser remelting (HRR-FLR) treatment. This study assessed the surface rumpling behavior, residual stress evolution, and thermally grown oxide (TGO) layer growth under thermal cyclic oxidation at 1100 °C to determine their impact on coating lifetime. The results indicated that the HRR-FLR treatment was effective in reducing surface roughness, restructuring microstructures, and redistributing reactive elements. These improvements facilitated the formation of a flat, continuous, and dense alumina layer, enhancing the spallation and rumpling resistance of TGO. Consequently, the efficiency of HRR-FLR technique was proven in significantly improving the lifetime of NiCrAlY coatings, which provides a new application prospect of femtosecond lasers in remelting and polishing of metallic surfaces.

Characterization of Potting Epoxy Resins Performance Parameters Based on a Viscoelastic Constitutive Model.

To describe the evolution of residual stresses in epoxy resin during the curing process, a more detailed characterization of its viscoelastic properties is necessary. In this study, we have devised a simplified apparatus for assessing the viscoelastic properties of epoxy resin. This apparatus employs a confining cylinder to restrict the circumferential and radial deformations of the material. Following the application of load by the testing machine, the epoxy resin sample gradually reduces the gap between its surface and the inner wall of the confining cylinder, ultimately achieving full contact and establishing a continuous interface. By recording the circumferential stress-strain on the outer surface of the confining cylinder, we can deduce the variations in material bulk and shear moduli with time. This characterization spans eight temperature points surrounding the glass transition temperature, revealing the bulk and shear relaxation moduli of the epoxy resin. Throughout the experiments, the epoxy resin's viscoelastic response demonstrated a pronounced time-temperature dependency. Below the glass transition temperature, the stress relaxation response progressively accelerated with increasing temperature, while beyond the glass transition temperature, the stress relaxation time underwent a substantial reduction. By applying the time-temperature superposition principle, it is possible to construct the relaxation master curves for the bulk and shear moduli of the epoxy resin. By fitting the data, we can obtain expressions for the constitutive model describing the viscoelastic behavior of the epoxy resin. In order to validate the reliability of the test results, a uniaxial tensile relaxation test was conducted on the epoxy resin casting body. The results show good agreement between the obtained uniaxial relaxation modulus curves and those derived from the bulk and shear relaxation modulus equations, confirming the validity of both the device design and the testing methodology.

Microstructure and residual stress evolution during cyclic elastoplastic deformation of AISI316L fabricated via laser powder bed fusion

In metal additive manufacturing (MAM), microstructural properties such as texture, residual stresses, and dislocation density have emerged as key factors ruling the resulting mechanical performances. In this study, cylindrical AISI 316L specimens, fabricated with laser powder bed fusion (LPBF), were tested under cyclic elastoplastic (EP) deformation using a constant strain amplitude to highlight the evolution of residual stresses (RS), dislocation density and texture with increasing number of EP cycles, N, across the hardening-softening (H–S) transition stage, in the attempt to find correlations between relevant microstructural parameters and macroscopic properties. The structural and microstructural analysis is carried out through whole powder pattern modeling (WPPM) of neutron diffraction (ND) data and Electron Back-Scattering Diffraction (EBSD) analysis. The H–S transition is found to occur within 7–9 cycles, with RS fading out already after 5 cycles. Across the H–S transition, the trend of the maximum tensile stress correlates closely with the trend of WPPM-calculated total dislocation density, suggesting a major role of dislocations’ characteristics in the evolution of macroscopic mechanical properties. EBSD analysis reveals the rearrangement of geometrically necessary dislocations (GND) into cellular structures, and moderate grain refinement, which are deemed to be responsible for the quick fading of RS in the very early stage of EP loading. ND-based texture analysis reveals a (220) preferential orientation retained throughout the EP tests but with orientation density functions (ODFs) changing non-monotonically with N, suggesting preliminary partial randomization of grains around the deformation axis followed by the recovery of crystallographic anisotropy and more localized ODFs.

Investigation on Influence of Surface Structuring on Brazed Joint between Tungsten Carbide and Steel

The aim of this project is to investigate the effects of surface structuring on brazed joints made of steel and tungsten carbide as well as how these effects affect the joints' mechanical characteristics. The industry uses brazing as a common connecting method, although brazing is known to produce considerable residual strains because of cooling thermal gradients. The strength, longevity, and fatigue resistance of the brazed joint can be impacted by the existence of residual stress, which might be crucial for applications in aerospace and automotive. The impact of several brazing parameters on the development of residual stress will be examined in this study, including temperature, heating rate, cooling rate, and material choice. To describe the residual stress state and assess the mechanical characteristics of the joint, experimental methods such X-ray diffraction and Shear Strength test will be used. The results of this project can be applied to numerous sectors to optimize the brazing procedure and enhance the performance and dependability of brazed components.

The incipient oxidation behaviors of Haynes 282 at high temperatures

The purpose of this study was to investigate the oxidation behavior and the development of residual stress in the nickel-based superalloy Haynes 282 at temperatures ranging from 800 to 950 °C. Detailed examinations of the oxide scale surfaces were conducted using Scanning Electron Microscopy (SEM) and Focused Ion Beam (FIB). The residual stresses in the Cr2O3 scales were measured using X-ray diffraction (XRD). A layered chromia scale was formed as a result of the oxidation process, and the kinetics of this process were found to be parabolic, controlled by Chromium diffusion. An external Cr2O3 layer was observed in cross-sections, along with Kirkendall voids at the alloy-oxide interface. All residual stresses of chromia observed were tensile intrinsically.