Deformation Of Steel Research Articles

Grain boundary-induced stress localization during compression deformation of polycrystalline 316L stainless steel

Grain boundary-induced stress localization during compression deformation of polycrystalline 316L stainless steel

The influence of V microalloying on the hot deformation behavior and microstructure evolution of high-manganese steel for LNG storage tanks.

Herein, the high-temperature hot deformation and dynamic recrystallization (DRX) behavior of high-manganese steel were investigated through the measurement of true stress-strain curves, the establishment of constitutive equations, the construction of recrystallization and hot processing maps, and the characterization of microstructure evolution. Furthermore, the influence of V on the DRX behavior of high-manganese steel during the hot deformation process, particularly for LNG storage tanks, was systematically evaluated. The results indicate that both the critical stress (σc) and peak stress (σp) of the tested steels increase as the deformation temperature decreases and the strain rate increases. Additionally, a higher V content leads to an increase in σc and σp, thereby suppressing the occurrence of DRX. Compared to 0.1V steel, 0.2V steel precipitates a greater quantity of carbides at the grain boundaries (GBs), which effectively stabilizes the GBs and inhibits the growth of DRX grains. In contrast, 0.1V steel achieves DRX over a wider range of Z parameters (at lower temperatures and higher strain rates). The activation energies for hot deformation (Q) of the two tested steels are 479.100 kJ/mol and 438.274 kJ/mol, respectively. The hot processing maps indicate that an increase in V content reduces the hot workability of high-manganese steel. The optimal temperature and strain rate for hot processing of 0.1V steel are 1035–1095°C and 0.01–0.0451 s⁻1, respectively. For 0.2V steel, the optimal hot processing parameters are a temperature of 1065–1100°C and a strain rate of 0.01–0.07 s⁻1.

Modeling of elastic plastic deformation of near-surface layers of materials

According to the results of strain measurements, a kinematically hardening body model is used to describe the process of elastic-plastic deformation of 1X18H9T steel. Special attention is paid to the processes occurring in the surface layers. The model takes into account the increasing tightness of shear deformations deep into the material. The increase in the stress of the plastic flow in depth is described by a second-order polynomial. The main parameters of the surface effect were determined experimentally and by calculations using the method of reduction coefficients in the process of successive approximations: depth, coefficient of hardening of the material, stresses of plastic flow on the surface and inside the material. It is shown that in order to study the near-surface effect by the strain gauge method, it is necessary to give preference to bending tests of samples rather than stretching. The presence of the surface effect explains the following facts: the destruction of the sample during the tensile test does not begin from the surface, but from the inside, the origin of fatigue cracks occurs under the surface, the surface effect practically does not affect the deformed state of the elastic body, but very strongly affects the stress state at the surface.

Wear mechanisms and failure analysis of a tool used in refill friction stir spot welding of AA6061-T6

Investigating tool wear in refill friction stir spot welding (RFSSW) is essential for understanding its limitations and improving its efficiency. Increasing the tool's service life is important to push the technology's readiness level and transfer the technology from the laboratory to industrial applications. In this study, the quasi-static lap shear performance of AA6061-T6 similar welded spots was investigated and tool wear was continuously monitored until tool failure at 3450 welding cycles. Furthermore, the fundamentals of the wear mechanisms in RFSSW were further elucidated. The investigation shows that it is possible to achieve steady quasi-static lap shear performance of the spot welds over advancing tool wear by adjusting the heat input to compensate for losses in frictional heat generation efficiency (related to tool profile changes by abrasion). A subsequent tool failure case analysis showed the main causes for the continuous wear degradation of the shoulder. Tool wear was driven by plastic deformation of the hot-work tool steel and subsequent break-out of tool steel ridges, introducing big hard particles into the contact region between the moving and rotating tools. In addition, the formation and detachment of Fe-Al intermetallic compounds counteract with the rotating tools and increase tool wear.

Interplay between deformation and fracture mechanism in gradient nanostructured austenitic stainless steel

The plastic deformation parameters are crucial for the grain size of gradient nanostructured (GNS) materials, and the multiscale grain structure within the GNS layer has a significant impact on fracture behavior. In this study, the detailed depth-dependent microstructures of GNS310S stainless steel fabricated by surface mechanical rolling treatment (SMRT) were investigated, and the relationship between the geometrically necessary dislocation (GND) density and the strain gradient was established through the local misorientation obtained by electron backscatter diffraction. The critical deformation parameters (strain gradient, shear strain, and strain rate) of SMRT-induced grain refinement at different scales were quantitatively evaluated. The tensile results show the yield strength and tensile strength of GNS310S are improved by 103% and 23.1% respectively compared to CG310S. Additionally, we elucidate the underlying tensile fracture mechanism of GNS310S stainless steel through detailed microstructural analysis. Due to the poor ductility of the near-equiaxed nanograins, cracking occurred on the surface of the SMRT specimen at low strain during the tensile testing. These cracks evolved into competitive shear offsets and multi-cracks with increased strain on the specimen surface, eventually leading to a hybrid fracture mode. In contrast, the subsurface nanotwinned lamellae layer displayed good ductility during tension, which can accommodate the deformation through lamellae widening and forming secondary twinning. This nanotwinned lamellae layer can suppress the inward propagation of surface cracks when the strain was not large. This work provides new insights into the fabricating parameters of the GNS stainless steel, as well as the deformation and fracture mechanisms.

Understanding low-temperature microstructure and mechanical properties of a newly designed ultra-low carbon medium manganese steel

This study examines the relationship between microstructure and low-temperature mechanical properties of newly designed medium manganese steel with ultra-low carbon, low-Ni content. The microstructural features crucial for impact toughness were identified. The study indicated that post-annealing at 650 °C for 30 min endowed the steel with superior low-temperature mechanical properties, namely tensile strength of 914 MPa, total elongation of 37.2 %, and impact energy of 187 J at −60 °C. With longer intercritical annealing durations, reverted austenite transitioned from a film-like to a blocky morphology, with an increase in both volume fraction and size, accompanied by a substantial decrease in stability. High-stability reverted austenite contributed to sustained work hardening by facilitating a continuous Transformation-Induced Plasticity (TRIP) effect during steel deformation, thereby significantly enhancing the low temperature tensile properties of the steel. Furthermore, enhanced stability of reverted austenite was identified as the pivotal microstructural factor influencing impact toughness.

Thermal creep strain test and model of Q460GJ steel at elevated temperatures

Q460GJ steel is a typical high strength and high-performance structural steel. The thermal creep test on two thicknesses (8 mm and 12 mm) of Q460GJ steel plates at elevated temperatures (400–800 °C) was carried out. The test results showed that the thermal creep strain increases with the increases of temperature and stress. When the temperature exceeds about 500 °C and the stress ratio is greater than about 0.55, the Q460GJ steel plate specimens has obvious creep deformations, so it is necessary to consider the thermal creep deformation of steel at elevated temperatures for steel structural design. The difference in plate thickness does not affect the creep properties of the 8 mm and 12 mm Q460GJ steel plates at elevated temperatures. When the temperature is no more than 600 °C, the second stage creep strain rates of Q460 steel are obviously higher than that of Q460GJ steel while the stress levels are close. The Fields & Fields creep model is suitable for fitting the thermal creep strain-time curves for Q460GJ steel. The findings will contribute to providing theoretical support for design of high-performance steel engineering structures under fire.

Lay-up design and experimental study of the multiple corrugated diaphragms of carbon fiber reinforced polymer composite

Rebound and deformation of stainless steel during processing have brought great difficulties to forming the multiple corrugated diaphragm (MCD), seriously affecting its performance. Carbon fiber reinforced polymer composite (CFRP) provides a new idea for the design and forming methods of MCD due to its excellent performance and designability. This paper uses ABAQUS finite element analysis software to analyze the influence of laying angle and laying angle ratio on the mechanical properties of composite material MCD. Finally, the axial stiffness of the designed CFRP MCD is tested using a flexible coupling stiffness test bench. The findings demonstrate that the design values are consistent with the experimental results within an acceptable margin of error. The investigation validates the feasibility of the proposed laying design method for CFRP multi-waveform membrane discs (MCDs) and establishes a theoretical foundation for their engineering design and practical application.

Analysis of fatigue damage of hot rolling work rolls coupled with wear effect

During the hot rolling process, the work roll experiences cyclic contact stress due to the deformation of the strip steel, as well as thermal stress from periodic heating and cooling. The surface failure of the work roll results from the combined effects of wear and fatigue damage. This study proposes a comprehensive approach to analyzing coupled wear and fatigue damage using a method based on the Manson-Coffin equation, modified slope formula, and the Miner criterion. Finite element models were developed to simulate simplified heat transfer and thermal coupling, taking into account the actual rolling parameters and high-temperature material properties of the work roll. The evolution of the physical field of the work roll during the rolling process was analyzed. The analysis of these models revealed that the maximum strain on the work roll occurred at the rolling exit and was predominantly influenced by temperature. The effects of rolling speed and temperature on work roll strain varied, with fatigue damage being significantly reduced when wear was considered compared to scenarios where wear was not accounted for, under the same number of cycles.

Microstructural Deformation and Fracture of Reduced Activation Ferritic-Martensitic Steel EK-181 under Different Heat Treatment Conditions

Abstract TEM studies were performed to examine the effect of holding of dispersion-strengthened heat-resistant reduced activation 12% chromium ferritic-martensitic steel EK-181 in static liquid lead for 3000 h at 600°C on the steel microstructure in comparison with the steel after conventional heat treatment by quenching and tempering at 720°C. It was found that the steel microstructure has good thermal stability under the specified experimental conditions. Microstructural deformation of EK-181 steel was studied in the neck region of tensile specimens tested at the temperatures 20, 680, 700, and 720°C with and without holding in liquid lead, and their fracture mechanisms were investigated. As a result of plastic deformation during tensile testing at room temperature, martensite plates and laths near the fracture surface are distorted and fragmented with the formation of new low-angle boundaries, and the dislocation density increases. At the deformation temperatures 680–720°C, nearly equiaxed ferrite grains are formed, the density and size of second-phase particles (M23C6 and MX) increases due to dynamic strain aging, and the dislocation density decreases locally. As the test temperature rises, the degree of martensite tempering increases. At T ≥ 700°C, some dynamic polygonization and dynamic recrystallization are observed. At elevated tension temperatures, ferrite coarsening is more significant in the specimens held in lead as compared to the conventionally treated material. The plastic deformation and fracture behavior of the steel are largely determined by the test temperature, rather than by the treatment mode.

PECULIARITIES OF CRACK FORMATION IN HETEROPHASE INCLUSIONS OF THE “EUTECTICS OF INCLUSION − MATRIX” TYPE

Purpose. The goal of the work was to study the peculiarities of crack nucleation in heterophase inclusions of the “eutectic inclusion − matrix” type during steel deformation. Methods. The research was carried out after deformation of samples from steels 08Yu, 12GS, 08kp, 09G2S, NB-57, 08GSYUTF in the temperature range of 20…1 200 °C with the speed of movement of grips 1 680 mm/min. The research methods were used − petrography, micro-X-ray spectral analysis (Cameca MS-4, Nanolab-7), optical microscopy (Neophot-21). Results. It is established that the variety of phases that make up heterophase inclusions of the type “eutectic of inclusion − matrix” leads to their different behavior under conditions of plastic deformation. It is shown that the nucleation of brittle or viscous microcracks occurs along the internal interfacial boundaries between the metal matrix and the second phase of the eutectic. It is determined that the nature of cracks is determined by the level of plasticity of the inclusion phases and the deformation temperature. It is shown that the critical degrees of deformation of the samples, at the achievement of which there were noticeable microcracks along the internal interfacial boundaries, depend on the temperature and nature of the phases of inclusions “eutectic of inclusion − matrix”. It is established that the values of critical degrees of deformation determine the level of cohesive strength of the internal interfacial boundaries in heterophase inclusions “inclusion − matrix eutectic”. Scientific novelty. Peculiarities of microcracking nucleation in heterophase inclusions of the “inclusion − matrix eutectic” type have been established. It is shown that the nature of microcracks formed along the interfacial boundaries depends on the temperature, level of plasticity and conditions of combination of brittle and plastic phases in inclusions of the “eutectic of inclusion − matrix” type, as well as on the deformation temperature. It is shown that the critical degrees of deformation of steels, when microcracks occurred along the inner interfacial boundaries, determine the cohesive strength of these boundaries and depend on the temperature and nature of the phases of inclusions such as “inclusion − matrix eutectic”. Practical significance. The use of the results obtained will make it possible to develop technologies for producing steels with regulated types of heterophase nonmetallic inclusions, which will significantly increase their technological and operational characteristics, as well as prevent the formation of various kinds of defects during the processing of steels by pressure and the operation of products.

Influence of hydrogen on deformation and embrittlement mechanisms in a high Mn austenitic steel: In-Situ neutron diffraction and diffraction line profile analysis

Austenitic steels have relatively high resistance to hydrogen embrittlement and play a critical role in hydrogen service applications. In particular, high Mn austenitic steels are considered economically viable alloy alternatives for these applications. The current study employed in-situ and ex-situ neutron diffraction techniques combined with diffraction line profile analysis (DLPA) to investigate the influence of hydrogen on deformation and embrittlement mechanisms in a high Mn (approximately 30 wt pct) austenitic steel. Investigation using both neutron diffraction and electron backscatter diffraction revealed the presence of extensive deformation twins and stacking faults within the steel microstructure after tensile deformation in the non-charged condition. These microstructural features suggest planar deformation behavior, which is expected from the relatively low stacking fault energy (SFE) of the alloy (approximately 29 mJ/m2). Hydrogen pre-charging resulted in apparent increases in both dislocations and stacking faults, contributing to macroscopic hardening and embrittlement mechanisms. Overall, numerical parameters obtained through neutron DLPA were used to elucidate the underlying mechanisms associated with hydrogen effects on the mechanical behavior, i.e. macroscopic strengthening, strain hardening rate, and embrittlement.

Experimental behavior and fracture prediction of a novel high-strength and high-toughness steel subjected to tension and shear loading tests

In this study, laboratory testing and numerical simulation methods are used to investigate the mechanical behavior and perform fracture prediction of a novel high-strength and high-toughness steel with a negative Poisson's ratio (NPR) effect under combined tensile-shear loading conditions. A test device capable of meeting different tensile-shear combination test angles is designed and manufactured, wherein the mechanical experiments on the NPR (Negative Poisson's Ratio) steel specimens are carried out at various testing angles. Q235 steel and MG400 steel are used as experimental control groups. The results show that the mechanical deformation of NPR steel is significantly better than that of Q235 steel and MG400 steel. Its tensile-shear test curve has no yield plateau and it has quasi-ideal elastic-plastic mechanical properties. The loading direction gradually changes from tension-dominated to shear-dominated as the tension-shear angle increases, and the strength and deformation of the specimens show a decreasing trend. Based on the laboratory test results, a finite element numerical model of NPR steel is established. A series of numerical simulations are carried out under the conditions of different tension and shear angles and the average stress triaxiality and fracture strain data are obtained. The fracture data of NPR steel are fitted using the Johnson-Cook fracture criterion, and the Johnson-Cook fracture parameters under the tensile-shear test conditions of NPR steel are thus obtained. The numerical simulation verifies that the fracture model can accurately predict the tensile-shear fracture behavior of NPR steel.

Test on progressive collapse of steel moment-resisting frame with upper-and-lower flange angle steel connection

Both of test and numerical simulation methods are employed to study the vertical progressive collapse and collapse assessment methods of steel frame under accidental loads. Firstly, a steel frame collapse test model with a geometric similarity ratio of 1:1.5 is designed and manufactured. The ends of column of test model is fixed. The upper and lower flange angle steel connection is used. The far end of the beam is constrained by a controllable sliding hinge support. The various stages of vertical progressive collapse of structures are simulated by a large displacement loads applied at the far end of the beam. The main focus of the testing is to examine the stress and deformation of beam and joint at various stages, particularly the development of stress and deformation in the angle steel attached to the beam-column connection. The development law of collapse load-displacement curve, joint rotation, beam strain, and angle steel strain are analyzed. The structural resistance mechanism and the transformation relationship between resistance mechanisms during collapse are studied. Subsequently, the relationship between the structural dynamic increase factor curve and the structural collapse process is analyzed using finite element method. The results show that the strain of angle steels can better reflect the destruction and deformation process of substructure during the collapse, the collapse resistance mechanism of structure, and the transition between resistance mechanisms.With the help of the characteristic points on the structural dynamic increase factor curve, the collapse limit state of structure can be reliably determined.

Understanding crack growth within the γ′ Fe4N layer in a nitrided low carbon steel during monotonic and cyclic tensile testing

Nitriding is a cost-effective method to realize simultaneous improvements in tensile and fatigue properties and resistance to abrasion and corrosion. Previous studies reported that nitriding pure Fe enhances tensile strength by ~ 70% and fatigue limit by ~ 200%. It is due to the increase in surface hardness caused by the formation of γ′(Fe4N) and ε(Fe2-3N) nitrogen-containing intermetallic compound phases. However, the intermetallic compound layer is prone to brittle-like cracking. To better design nitrided steels, it is crucial to identify the crack growth mechanisms via analysis of the microstructural crack growth paths within the ~ 4–6 µm thick nitride layer. In the current work, we statistically evaluate the crack propagation behavior in the γ′ Fe4N layer during monotonic and cyclic tensile deformation in nitrided low-carbon steel (0.1 wt% C). Since nitriding typically results in the formation of columnar grains, the effect of morphology needs to be clarified. To this end, the steel was shot-peened and subsequently nitrided to promote equiaxed nitride grains morphology (~ 16% increase). Crack growth paths were comparatively evaluated for multiple cracks, and no significant effect of nitride morphology was observed. {100}γ′ is the predominant transgranular crack path in the monotonic tensile tested specimen, followed by {111}γ′. It is despite the elastic modulus of {111}γ′ < {100}γ′. This contrary behavior is explained by {100}γ′ plane having the lowest surface energy (density functional theory calculations). In the cyclic tensile loaded specimen, experiments revealed that transgranular cracking along {100}γ′ (cracking via symmetric dislocation emission) or {111}γ′ (slip plane cracking) is equally likely.Graphical abstract

Micromechanism insights and constitutive modeling for deformation in a novel high manganese austenitic steel

We explore the mechanical behavior and microstructural evolution of a novel high manganese austenitic steel (HMAS), extensively applied in underground engineering and structural construction. Our investigation focuses on two variants of HMAS, namely HMAS-1.9 and HMAS-10, which exhibit distinct yield strengths and elongation behaviors. Electron backscatter diffraction (EBSD), transmission electron microscopy (TEM) and X-ray diffraction (XRD) were employed to elucidate the evolution of microstructures during plastic deformation. Based on these experimental results, we developed a new phenomenological multiscale constitutive model that captures the mechanical behavior of HMAS, integrating micromechanisms and microstructural evolutions. Optimized with the MATLAB genetic algorithm toolbox, this model was successfully implemented in a uniaxial tensile finite element model (FEM) within ABAQUS, proving its efficacy in predicting both macroscopic flow stress and microstructural evolutions. Our findings highlight the important roles of initial grain size, dislocation density, and twin fraction in determining the mechanical properties of HMAS. Throughout the deformation process, both HMAS variants demonstrate similar plastic deformation behaviors, characterized by comparable rates of increase in dislocation density and twinning fraction, accompanied by a consistent trend of grain refinement. These findings not only deepen our understanding of the complex relationship between microstructure and mechanical properties of the HMAS steel, but also provide an effective multiscale constitutive modeling approach for predicting its deformation behavior.

In-situ tensile deformation of austenitic stainless steels with various grain sizes during synchrotron and neutron diffraction

In-situ tensile deformation of austenitic stainless steels with various grain sizes during synchrotron and neutron diffraction

Digital holographic microscope for high spatial and temporal resolution in situ observation of dynamic phenomena of metals

A digital holographic microscope (DHM) was developed for the purpose of simultaneous observation and measurement of surface relief formation during deformation and phase transformation of steels. It was designed to accommodate the sample mounting component of a custom tensile tester. The Gabor wavelet transform method was used in the image reconstruction. To verify performance, the DHM was used to observe and measure height of slip bands formed during the monotonic loading 316L stainless steel. Data obtained has high temporal resolution (limited only by the camera’s frame rate capability) with lateral resolution approaching the diffraction limit. The results clearly show the evolving microstructures with height information available within each captured image.

Deformation and Fracture Resistance of Steel with a Structure of a Natural Ferrite-Martensite Composite Under High-Speed Impact

Deformation and Fracture Resistance of Steel with a Structure of a Natural Ferrite-Martensite Composite Under High-Speed Impact

Multi-stage strain-hardening behavior of dual-phase steels: A review

Regardless of the abundant studies that have been published on various characteristics of dual-phase (DP) steels, a comprehensive review paper on the strain-hardening behavior of such materials is still lacking. Therefore, the present study endeavors to summarize the existing results and findings regarding the strain-hardening phenomena during deformation in DP steels. The focus of this review article is on common methods used to investigate the strain-hardening characteristics of DP steels. Moreover, it encompasses a discussion on the microstructural characteristics and their correlation with strain-hardening behavior within these materials. Furthermore, this review aims to elucidate the limitations, bottlenecks, and scientific challenges to guide researchers to gain a deeper knowledge of the strain-hardening behavior of DP steels.