Evaluation of permittivity (e) and permeability (μ) of magnetic/dielectric material in microwave band becomes more important with the rapid expansion of microwave technologies. Transmission/reflection line method is well known as a simultaneous measurement method of e and μ in the band. However in this method material under test (MUT) is limited to solid state. On the other hand, for measuring liquid material open ended coaxial probe method was proposed. The method is disadvantageous in terms of requiring deciliter volumes of MUT for approximating a semi-space filled by MUT. We propose a new measurement method with the aim of simultaneous measuring both of permittivity and permeability of not only solid material but also a small amount of liquid, powder, and gel state material. A plastic toroidal case was utilized to encapsulate non-solid state MUT and whole the case was evaluated by coaxial line method. In this study the cases were modeled using Acrylic 3-D printer (Stratasys, Objet 260 Connex). An example of the plastic case with a cap fabricated is shown in Fig. 1. Outer and inner diameter (7.00 and 3.00 mm) of the case was designed to fit to a coaxial sample holder (KEAD Inc., CSH2-APC7). The length of the case including a cap thickness measured by digital vernier caliper was 5.00 mm. In the same way, thickness of wall, bottom, and cap was 0.45, 0.50, and 0.50 mm, respectively. Accordingly the volume of MUT required for the case was about 70 microliters. The specimen which MUT was encapsulated was inserted to the coaxial sample holder and complex scattering (S) parameters from 1–10 GHz were taken using a vector network analyzer (Hewlett-Packard, HP 8720D). S-parameters whose reference planes were both upper and lower surface of the specimen were obtained by shifting reference planes of the measured S-parameters. After that we obtained S-parameters of MUT in numerical calculations mentioned below in order to take away unwanted plastic case portions. The specimen can be divided into three coaxial portions: Inner cylindrical wall, outer cylindrical wall, and middle core including MUT between their walls. From the viewpoint of electric circuit it corresponds to a series connection of the three two-port networks. Impedance (Z) parameters of the middle core were obtained using the relationship: Z-matrix of the specimen equals to the sum of their three Z-matrices. Z-matrix of the specimen was obtained by converting S-matrix of it by a reference impedance. Z-matrix of outer and inner wall was obtained from e and μ measured in advance using solid specimens of the plastic material and outer and inner diameters of their cylindrical walls. Z-matrix of the middle core was converted S-matrix again. The middle slender core can be divided into three coaxial portions: a part of cap, a part of bottom, and MUT. The core corresponds to a cascaded connection of the three two-port networks. Transfer (T) parameters of MUT were obtained using the relationship: T-matrix of the core equals to the product of their three T-matrices. T-matrix of the core was obtained by converting S-matrix of it. T-matrix of a part of bottom and cap was obtained from e and μ of the plastic material used and bottom and cap thickness. Finally e and μ of MUT were calculated from S-parameters of it using Nicolson-Ross-Wier algorithm [1, 2]. In this study, the air at the volume was measured as MUT in order to confirm a validity of the proposed method. The dependences of real and imaginary part of relative permittivity of air obtained by this method on frequency were shown in Fig. 2(a) and Fig. 2(b). Although the both values had a margin of error of plus or minus 10% a constant and nearly ideal relative permittivity of air was confirmed in the band measured from these figures. This result indicates that the proposed method is effective for measuring non-solid materials.
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