Conventional Mechanical Testing Research Articles

Equivalent stiffness analysis of flexible lithium-ion batteries with repeated unit cell: A computational approach

Flexible batteries have recently developed significant advancements in structural design, diverging substantially from traditional battery architectures. However, conventional mechanical testing methods and metrics, tailored for standard battery structures, prove inadequate when evaluating the flexibility of these innovative designs. How to assess the mechanical performance of diverse structural configurations of flexible batteries poses a considerable challenge. In this study, a general computational approach is proposed to evaluate the equivalent stiffness of flexible lithium ion batteries (FLIBs) by analyzing the force–deformation response of a repeated unit cell (RUC), thereby enabling a comprehensive comparison of different FLIB designs. Moreover, to further enhance their deformability, the interconnected supple components of FLIBs have been optimized. This research lays a critical foundation for comparing the mechanical performance and optimizing the design of flexible batteries in the future.

Parallel-beams magnetic actuator for in-situ transmission electron microscope observation of mechanical testing

Abstract Understanding the microscopic mechanisms behind mechanical fractures is essential for enhancing material properties and increasing reliability through fatigue suppression. Conventional mechanical testing methods, such as indentation tests that press a sharp needle into a specimen or tensile tests using hydraulic pumps, are unable to capture nanoscale deformations under applied forces. As a result, the microscopic mechanisms that influence mechanical properties are often inferred indirectly, and material design largely depends on the engineer’s intuition and occasional serendipity To overcome these challenges, in-situ observation techniques utilizing transmission electron microscopes (TEMs) have been developed to enable the observation of sample deformations at the nanoscale. However, despite their high resolution, conventional TEMs are limited by a small available space -often just a few millimeters- that restricts the application of sufficient force to fracture specimens. Traditional actuation methods, such as thermal expansion, electrostatic force, and piezoelectric actuators, fail to generate significant forces within such confined spaces. In response to these limitations, our research involved the development of a micromachine with multiple parallel beams. This device leverages the Laplace force generated by an electric current passing through the beams and the magnetic field of the TEM. We demonstrated the capability to produce significant force using the magnetic field from the microscope’s magnetic lens. The actuator developed in our study successfully generated forces exceeding 50 µN, marking a significant advancement in the in-situ observation capabilities for mechanical testing.

Developing a lightweight corrugated sandwich panel based on tea oil camellia shell: correlation of experimental and numerical performance

This study presents an experimental and numerical comparison between the mechanical performance of a lightweight corrugated sandwich panel based on the tea oil camellia shell (TOCS). Hence, TOCS was mixed in two groups with Poplar particles and fibers. After that, in the experimental part, the conventional mechanical tests, including the 3-point bending test, flatwise compression, dowel bearing, and screw resistance, and in the numerical part, finite element analysis (FEA), including the normal, maximum principal, and equivalent (von Mises) stress by Ansys Mechanical software carried out. The specimens for experimental and numerical tests were prepared in transverse and longitudinal directions. Before that, the engineering data (shear modulus, Young's modulus, and Poisson's ratio) for improving the FEA simulation were obtained from TOCS-based flat panels fabricated with a mixture of Poplar particles and fibers. The results of FEA are used to compare the mechanical behavior and failure mechanism with the results of experimental tests. According to the mean values of bending stiffness and maximum bending moment, sandwich panels made with 100% particles demonstrated an advantage in both directions. Nevertheless, the compression strength and screw resistance showed the same trend, but the dowel bearing showed higher values for panels made with fibers. The observed results of equivalent (von Mises) stress indicated a coloration with the results of failure mechanisms.

Investigation of Fiber-Matrix Interface Strength via Single-Fiber Pull-Out Test in 3D-Printed Thermoset Composites: A Simplified Methodology.

The emergence of additive manufacturing technologies for fiber-reinforced thermoset composites has greatly bolstered their utilization, particularly within the aerospace industry. However, the ability to precisely measure the interface strength between the fiber and thermoset matrix in additively manufactured composites has been constrained by the cumbersome nature of single-fiber pull-out experiments and the need for costly instrumentation. This study aims to introduce a novel methodology for conducting single-fiber pull-out tests aimed at quantifying interface shear strength in additively manufactured thermoset composites. Our findings substantiate the viability of this approach, showcasing successful fiber embedding within composite test specimens and precise characterization of fiber pull-out strength using a conventional mechanical testing system. The test outcome revealed an average interfacial strength value of 2.4 MPa between carbon fiber and the thermoset epoxy matrix, aligning with similar studies in the existing literature. The outcome of this study offers an affordable and versatile test methodology to revolutionize composite material fabrication for superior mechanical performance.

The bonding performance of desert sand self-compacting concrete overlay on normal strength concrete substrate: Macro, micro, and ultrasonic testing

This study investigates the performance of concrete containing desert sand (desert sand concrete and desert sand self-compacting concrete) as overlay concrete to bond with normal-strength concrete substrate, with different bonding interfaces being considered. The impermeability of the bonding interface is determined by the electrical resistance test. Static bonding strength is tested by conventional mechanical tests. The dynamic properties of bonded specimens are also studied by dynamic response tests. Non-linear parameters, low-frequency energy parameters and ultrasonic velocity are included in the bonding interface ultrasound detection. The microstructural and chemical compositional of the overlay transition zone (OTZ) are analysed to reveal the mechanisms of bonding behaviour. The results indicate that the interface electrical resistance is positively related to bonding strength. Using concrete containing desert sand as the overlay concrete improves bonding interface adhesion for 30 % at most. Bonding performance can be affected by the interface pattern and volume density in both static and dynamic conditions. The bonding strength and damping ratio with properly treated interfaces can be increased by over 300 % and 38 % than those of untreated groups, respectively. The dynamic response of the bonded specimens can effectively reflect the bonding performance. The non-linear ultrasound method and the ultrasound energy method are more accurate and sensitive than traditional way (ultrasonic velocities) in detecting the bonding interface. The incorporation of desert sand in the concrete or lowering W/B considerably contributes to a series of benefits to the microstructure of the bonding interface. The bonding gap width is reduced by 17 % and 72 % for DS incorporation and lower W/B, respectively. Characterized by Ca/Si, the OTZ width is reduced by 10 % and 31 % for DS incorporation and lower W/B, respectively. Characterized by micro-hardness, the OTZ width is reduced by 21 % and 24 % for DS incorporation and lower W/B, respectively, which provides an important reference for the engineering application of desert sand self-compacting concrete.

Experimental study on failure mode and fracture evolution characteristics of red shale in Kaiyang Phosphorus mining area

In order to study the failure mode and fracture evolution characteristics of red shale in Kaiyang Phosphorus mining area, conventional triaxial compression mechanical tests of red shale with different bedding dip angles were carried out by using DSTD-1000 electro-hydraulic servo rock mechanics experiment system. Based on the laboratory test results, the conventional triaxial particle flow simulation of red shale samples with different bedding dip angles was carried out using discrete element PFC2D. The results show that: (1) the failure mode of red shale is controlled by bedrock when the bedding dip angle is 0° and 60° ~ 90°. When the bedding dip angle is 15° ~ 45°, the rock failure mode is controlled by bedding. The compressive strength of rock is the minimum when the bedding dip angle is 30°and the maximum at 0°, which is about 2 times of the minimum. (2) In the failure process of red shale, the cracks with different bedding dip angles show slow growth stage, accelerated growth stage and stable stage with axial strain. The whole failure process is dominated by tensile cracks, accompanied by a few shear cracks. (3) The type of displacement field varies with the bedding dip angle: tensile failure and shear failure are the main displacement field types at 15° ~ 45°, and mixed failure is often the main mode at 60° ~ 90°and 0°. The research results provide the basis and reference for the safety control of red shale roadway.

Shear strength of soil by using rice husk ash waste for sustainable ground improvement

In the global construction industry, areas characterized by weak and expansive soils are on the rise, necessitating effective solutions for strength enhancement. Addressing this concern, sustainable soil amendments have gained attention, with rice husk ash (RHA) from rice milling industries being a notable focus. Our experimental study aimed to assess the shear strength of this innovative construction material, introducing a unique approach that considers subgrade layers with minimal cement dosage, including upper, bottom, and double layers a novel contribution yet unexplored in existing literature. In addition to conventional mechanical testing, we employed SEM (Scanning Electron Microscopy) and EDS (Energy-Dispersive X-ray Spectroscopy) analyses to comprehensively explore the treated soils' microstructural and elemental composition aspects. Examining sixteen specimen combinations of weak expansive soil-RHA-cement, varying proportions of RHA (2%, 4%, 6%) and cement (2%, 4%, 6%) were mixed to understand their effects on shear strength parameters. Our findings revealed significant shear strength improvement in each subgrade layer, with specimen 6%RHA6%C in the lower subgrade layer exhibiting the highest cohesive strength at 143 kN/m2. Notably, the double layer configuration, specimen 2%RHA6%C, achieved maximum deviatoric stresses of 383 kN/m2. This novel construction material contributes to effective waste management and presents an innovative engineering solution for sustainable ground improvement, offering promising prospects for future geotechnical advancements.

Alternative Approaches for Rapid Evaluation of Frictional Resistance of Aggregates

Skid resistance of pavements plays a crucial role in ensuring the safety of road users, particularly under wet weather conditions. The standardized method for evaluating the skid resistance of aggregates, AASHTO PP103, requires using a three-wheel polishing device. That test procedure requires significant time for specimen preparation, testing, and monitoring of aggregate stockpiles. This study aims to propose alternative test methods to reduce the time required for the evaluation of skid resistance of aggregates. Two approaches were examined as alternatives to the AASHTO PP103 method. The first approach involved using a micro-deval abrasion device to polish the aggregates before evaluating the skid resistance of the aggregates using a dynamic friction tester. In the second approach, a multiple linear regression equation was proposed that uses conventional mechanical performance test results as independent variables to predict skid resistance. Twenty-one aggregate samples were collected from various sources in Texas for this study. The study results indicate that both approaches can be used as surrogate methods for AASHTO PP103 for rapid screening of the skid resistance of aggregates, which could help manage aggregate quality control and assurance.

Hypergravity prompt thermal crack in 1060 aluminium slat

High-speed rotation instruments that apply gradient hypergravities can induce local variations in structure and thus induce cracking. Rotation-induced hypergravity is a kind of gradient force, and it has a gradient value that depends on distance and local weight. Conventional mechanical testing applies a constant force or periodic force instead of true gradient hypergravity to rotating components. In this study, a dedicated instrument was designed and assembled, and a special sample of 1060 aluminium slats with multiple thinned necks was used to reveal the difference between gradient hypergravity and conventional constant forces. Hypergravity caused more significant damage to the aluminium slat, and the ultimate crack strength was approximately 10% of the strength observed under the constant force applied at the same temperature. All the samples cracked on the inner neck which bears the highest hypergravity. Two types of cracks were categorized based on the relative extension: type Ⅰ mode cracks occurred in the centre of the neck with long extension before cracking under hypergravity more than 3.5 MPa, while type Ⅱ cracks occurred in the root of the neck without long extension before cracking under hypergravity less than 3.5 MPa. Combination of hypergravity and torsional force in high-speed rotation system prompt cracking and exhibit similar microstructure with that under high constant force. Typical cracking and its microstructure under the effects of hypergravity and temperature provided a convenient and practicable method for evaluating service safety of commercial rotating machines for industrial applications and raw alloys.

Rheology of Crumb Rubber-Modified Warm Mix Asphalt (WMA).

This study explores the impact of adding waste vehicular crumb rubber to the commercially available warm mix additives Sasobit® and Zycotherm® on modified asphalt binders' physical and rheological properties. Various concentrations of crumb rubber (0%, 10%, 15%, and 20%) were introduced to asphalt binder samples with 2% and 4% Sasobit and 1.5% and 3% Zycotherm. The investigation employed conventional tests (penetration and softening point) and advanced mechanical characterization tests, including Superpave rotational viscosity (RV), Dynamic Shear Rheometer (DSR), DSR multi-stress creep recovery (MSCR), DSR linear amplitude sweep (LAS), and Bending Beam Rheometer (BBR). Traditional tests measured the asphalt consistency, while workability was assessed through the RV test. The results showed that the Zycotherm binders experienced a more significant penetration reduction than the Sasobit binders. Additionally, an increased crumb rubber content consistently elevated the softening point and rotational viscosity, enhancing the complex shear modulus (G*) values. Rubberized binders exhibited an improved rutting performance and low-temperature PG grades. Increasing the crumb rubber content enhanced fatigue life, with Z1.5CR20 and S2CR20 demonstrating the longest fatigue lives among the Zycotherm and Sasobit binders, respectively. Overall, Z1.5CR20 is recommended for colder climates, while S2CR20 is suitable for hot-climate applications based on extensive analysis.

Improving Mining Sustainability and Safety by Monitoring Precursors of Catastrophic Failures in Loaded Granite: An Experimental Study of Acoustic Emission and Electromagnetic Radiation

Effective monitoring and early warning methods are crucial for enhancing safety and sustainability in deep coal resource extraction, particularly in mitigating rock burst disasters triggered by abrupt rock failure under high–ground–stress conditions. This paper presents the results of experimental investigations that involved conventional uniaxial direct and graded mechanical tests on granite that concurrently collected acoustic emission (AE) and electromagnetic radiation (EMR) signals. This study focused on the temporal evolution patterns of characteristic parameters in AE and EMR signals during granite deformation and fracture processes. To deconstruct and understand these temporal evolution characteristics, multifractal and critical slowing–down theories are introduced. The research findings reveal significant correlations between the evolution of AE and EMR characteristic parameters and the stages of rock deformation and fracture. Notably, dynamic changes in multifractal parameters (Δα and Δf) quantitatively reflected the deformation and fracture processes, with abrupt increases in Δα and sudden decreases in Δf closely associated with large–scale rock fractures. The temporal continuity of critical slowing–down parameters (variance and autocorrelation coefficient) demonstrated increased sensitivity as rock destruction approaches, with the variance emerging as a crucial indicator for large–scale fractures. This study observed a sudden increase in the variance of AE and EMR signals when the stress level reached 80–90% of the peak stress. Joint monitoring through diverse methods and multiple indicators enhanced the effectiveness of rock burst disaster warnings, contributing to the safety and sustainability of coal resource extraction. Further refinement and exploration of these indicators offer promising avenues for advancing rock failure monitoring and early warning capabilities in coal mines.

Rockburst hazard assessment and prevention and control strategies in the Ruihai gold mine

Ruihai gold mine is a super large underwater gold mine with an initial mining depth of more than 1,400 m. Deep mining may face rockburst disaster. In order to scientifically control the potential rockburst risk, ensure the safety of underground personnel and equipment, and realize the safe and efficient mining of the mine, it is necessary to evaluate the rockburst risk of the mine and formulate appropriate rockburst risk warning and mitigation strategies. XRD mineral composition analysis and conventional rock mechanical tests were carried out on the parent rock granite samples. The results show that there are differences in the lithologic composition and rock mechanics parameters of the three colors of granite, which are preliminarily determined as three kinds of granite; The rockburst tendency of three kinds of granites is evaluated by using three classical rockburst criteria, and the discrimination results of the three rockburst criteria are not completely consistent or even contradictory. The application limitations rockburst risk assessment based on index criteria are discussed and analyzed in detail. It is proposed to apply microseismic monitoring technology to warn and manage the rockburst risk of Ruihai gold mine in development and mining stages, and put forward microseismic monitoring layout schemes and targeted rockburst prevention and control measures in different stages. The research results can provide reference for similar projects.

Tensile strength analysis of additively manufactured CM 247LC alloy specimen by employing machine learning classifiers.

Using a cutting-edge net-shape manufacturing technique called Additive Layer Manufacturing (ALM), highly complex components that are not achievable with conventional wrought and cast methods can be produced. As a result, the aerospace sector is paying closer attention to using this technology to fabricate superalloys based on nickel to develop the holistic gas turbine. Because of this, there is an increasing need for the mechanical characterisation of such material. Conventional mechanical testing is hampered by the limited availability of material that has been processed, especially given the large number of process factors that need to be assessed. Thus, the present study focuses on manufacturing CM247LC Ni-based superalloy with exceptional mechanical characteristics by laser powder bed fusion (L-PBF). This study evaluates the effect of input process variables such as laser power, scan speed, hatch distance and volumetric energy density on the mechanical performance of the LPBF CM247LC superalloy. The maximum value of as-built tensile strength obtained in the study is 997.81 MPa. Plotting Pearson's heatmap and the Feature importance (F-test) was used in the data analysis to examine the impact of input parameters on tensile strength. The accuracy of the tensile strength data classification by machine learning algorithms, such as k-nearest neighbours, Naïve Baiyes, Support vector machine, XGBoost, AdaBoost, Decision tree, Random forest, and logistic regression algorithms, was 92.5%, 83.75%, 83%, 85%, 87.5%, 90%, 91.25%, and 77.5%, respectively.

Automated discovery of interpretable hyperelastic material models for human brain tissue with EUCLID

We propose an automated computational algorithm for simultaneous model selection and parameter identification for the hyperelastic mechanical characterization of biological tissue and validate it on experimental data stemming from human brain tissue specimens. Following the motive of the recently proposed computational framework EUCLID (Efficient Unsupervised Constitutive Law Identification and Discovery) and in contrast to conventional parameter calibration methods, we construct an extensive set of candidate hyperelastic models, i.e., a model library including popular models known from the literature, and develop a computational strategy for automatically selecting a model from the library that conforms to the available experimental data while being represented as an interpretable symbolic mathematical expression. This computational strategy comprises sparse regression, i.e., a regression problem that is regularized by a sparsity promoting penalty term that filters out irrelevant models from the model library, and a clustering method for grouping together highly correlated and thus redundant features in the model library. The model selection procedure is driven by data stemming from mechanical tests under different deformation modes, i.e., uniaxial compression/tension and simple torsion. The data is acquired through conventional mechanical tests that deliver labeled one-dimensional data pairs, and thus the method can be interpreted as a supervised counterpart to the originally proposed EUCLID that is informed by full-field displacement data and global reaction forces. The proposed method is verified on synthetical data with artificial noise. In addition, we present for the first time an experimental investigation of the EUCLID framework by validating the proposed method on experimental data acquired through mechanical tests of human brain specimens, proving that the method is capable of discovering hyperelastic models that exhibit both high fitting accuracy to the data as well as concise and thus interpretable mathematical representations.

Direct measurement and calculation of rubber bulk modulus by piston-cylinder method using conventional mechanical testing equipment

This article describes a method to directly measure the bulk modulus of rubber using a piston-cylinder type apparatus. The function of the testing apparatus is to reliably transfer load to the water inside the vessel and allow for the accurate and continuous measurement of volumetric displacement as the contents are compressed. During the test, load is applied to a piston-cylinder containing the rubber test sample and water using a conventional mechanical testing load frame. Load and the travel of the piston are recorded by a load cell and extensometer, respectfully. A brass or stainless steel plug of the same dimensions as the test sample is tested as a control sample to isolate the compliance of the system, including the compressibility of water and compliance of the o-rings which seal the piston-cylinder system. The results from this control test are used to decouple the compliance of the system from the sample test results. Load-linear displacement data are mathematically converted to pressure-volumetric displacement data, from which bulk modulus is calculated. The test apparatus and method are validated using the known bulk modulus of water. Finally, the bulk moduli for two similar rubbers are evaluated. The validity of the results and limitations of the device are discussed.

Multi-scale deterioration mechanism of shear strength of gypsum-bearing mudstone induced by water-rock reactions

Investigation of water-rock reactions effects on the shear strength of gypsum-bearing mudstone is necessary for underground engineering design and assessment of engineering safety. A comprehensive study of the multi-scale deterioration effects and mechanisms of water-rock reactions on gypsum-bearing mudstone can contribute to developing better engineering applications. The 25 sets of laboratory dissolution tests and 30 sets of conventional rock mechanical compression tests conducted in this study demonstrate the progressive modification of rock properties on multiple scales, including changes in mineralogy, porosity, grain structure, microstructures, and complexity of micropores, with sodium sulfate and gypsum being the most active minerals. Water-rock reactions cause irreversible morphological changes in microstructures. For instance, the number of intracrystalline pores increased, the contact between grains changed from face-to-face contact to line-to-line contact, and the volume of micropores, mesopores and macropores inside the rock increased by a maximum of 80.0%, 59.9% and 71.4% respectively. The maximum increase in the porosity of the samples was 5.33%. The increasing number of microphysical changes leads to defects that develop into weak areas, significantly decreasing the shear strength of gypsum-bearing mudstone. The maximum decrease in the cohesion of the samples was 79.06% throughout the dissolution process. It was found that the decrease in the cohesion of the samples c at the early stage of dissolution is mainly affected by the increase in the micropore volume. In the middle and late stages, the cohesion c of the samples decreased in a straight line, which is mainly caused by the increase in the macropore volume and porosity. The fluctuation in the cumulative pore volume during the whole dissolution process leads to fluctuation in the internal friction angle φ. The multi-scale degradation model of rock samples induced by water-rock reactions should be formulated to accurately evaluate the effect of water-rock reactions on rock shear strength.

Microstructure engineering of fusion zone in resistance spot welding of martensitic stainless steels: The role of Ni interlayer thickness

Martensitic stainless steel (MSS) spot welds show low fracture toughness due to the formation of a brittle microstructure at the joint area. To realize the full advantage of this class of steels in industrial applications, the strategy of altering the microstructure of the weld nugget through introduction of a Ni interlayer was investigated. For this purpose, Ni interlayers with variable thicknesses of 50 to 400 μm were utilized. The microstructural evolutions were thoroughly scrutinized using Scheil-Gulliver solidification modeling and electron backscatter diffraction (EBSD) analysis. Conventional quasi-static mechanical tests, namely, tensile-shear (TS) and cross-tension (CT) were used to correlate microstructure-mechanical properties relationships. In the absence of Ni interlayer, the weld nugget was predominantly composed martensite-M and presumably residual delta ferrite-δ (M+ δ-95%) phases with minor amounts of austenite-γ (5%), failing to meet the minimum peak load requirements under TS and CT loading conditions. By applying Ni interlayers of 50 and 75 μm, a noticeable increase in the fraction of austenite phase (up to 31%) in the weld nugget was detected; nevertheless, a slight to moderate improvement in the mechanical properties was observed since the solidification mode was still primary δ, and M+δ were still the predominant phases in the microstructure. A significant improvement in mechanical properties was achieved in 100 μm Ni interlayer owing to change in the solidification mode from primary δ to γ along with the formation of a mainly austenitic microstructure. However, due to the incomplete mixing of melted base metals and Ni interlayer, a different microstructure consisting of M, δ and γ was also occasionally perceptible in the weld nugget of this sample. The best mechanical properties in terms of strength and ductility occurred with increasing thickness to 200 μm and above, which coincided with the formation of a fully austenitic microstructure in the entire weld nugget.

A comprehensive study on physico-mechanical properties of non-metallic fibre reinforced SCC blended with metakaolin and alcofine

This study presents a detailed experimental investigation on the effects incorporating non-metallic fibers in hybrid form in self-compacting concrete (SCC). In this regard SCC was prepared with Alccofine and Metakaolin as partial replacement for cement in 15% and 20% respectively along with the hybrid fibre combinations namely abaca fibres (0.25%, 0.5% & 0.75%), polypropylene fibres (0.5%, 1%, 1.5% & 2%) and glass fibres (0.5%, 1%, 1.5%, & 2%). The fresh properties of SCC with and without hybrid fibre combinations were assessed through the standard tests such as slump flow, J ring and V-funnel tests. The conventional mechanical tests such as compressive strength test, split tensile strength test and flexural strength test were performed at 7 and 28 days. The experimental results reveal that the fresh properties of SCC were highly influenced by alccofine and Metakaolin adopted in this research. Furthermore, that the hybrid combination of abaca with polypropylene and glass fibres improved the mechanical properties of SCC and in particular the mix with 1% glass fibre and 0.25% Abaca fibre had shown better flexural and tensile strength behaviour. Microstructure analyses were also done to confirm the improvement in mechanical properties. The Scanning Electron Microscope images of the mix with 1% glass fibre and 0.25% abaca fibre showed less voids presence and presence of more hydrated components conveying that the usage of hybrid fibres had restricted the propagation of cracks there by reducing the percentage of voids and the use of metakaolin and alcofine helping in forming hydrated components at earlier stage leading to better strength.

Multiscale hierarchical and heterogeneous mechanical response of additively manufactured novel Al alloy investigated by high-resolution nanoindentation mapping

Smart alloying and microstructural engineering mitigate challenges associated with laser-powder bed fusion additive manufacturing (L-PBFAM). A novel Al–Ni–Ti–Zr alloy utilized grain refinement by heterogeneous nucleation and eutectic solidification to achieve superior performance-printability synergy. Conventional mechanical testing cannot delineate complex micromechanics of such alloys. This study combined multiscale nanomechanical and microstructural mapping to illustrate mechanical signatures associated with hierarchical heat distribution and rapid solidification of L-PBFAM. The disproportionate hardening effect imparted by Al3(Ti,Zr) precipitates in the pool boundaries and the semi-solid zone was successfully demonstrated. Nanomechanical response associated with heterogeneity in particle volume fraction and coherency across melt pool was interpreted from nanoindentation force–displacement curves. The hardness map effectively delineated the weakest and strongest sections in the pool with microscopic accuracy. The presented approach serves as a high throughput methodology to establish the chemistry-processing-microstructure-properties correlation of newly designed alloys for L-PBFAM.

Performance evaluation of asphalt binders modified with waste engine oil and various additives

ABSTRACT Annually tons of waste engine oil is wasted or dumped in environmentally unfriendly ways. Asphalt binder has been modified with waste engine oil previously and showed, lower consistency, lower moisture damage resistance at higher dosages, and impaired high-temperature performance. In the current study, three different additives were added to solve these issues associated with waste engine oil-modified bitumen. Elvaloy, polyphosphoric acid (PPA), and hydrated lime (H-L) were used as polymer, chemical, and filler-type additives. Waste engine oil-modified bitumen combined with all three types of additives was evaluated using conventional viscosity, moisture susceptibility, dynamic mechanical, and chemical testing. Results showed that waste engine oil inclusion decreased the consistency of binder, reduced viscosity, and impaired high-temperature performance. Elvaloy’s addition to waste engine oil-modified bitumen made it less sensitive to temperature changes, increased the performance grade, improved the stiffness, and enhanced the resistance against rutting and moisture-induced damages. Polyphosphoric acid addition refined the consistency of binder modified with waste engine oil. It drastically increased the complex modulus values and decreased phase angle values by stiffening the binder. PPA enhanced the moisture susceptibility of asphalt and improved its high-temperature performance. Hydrated lime improved moisture resistance and bonding strength but showed less effectiveness in improving high-temperature performance at lower dosages. The results conclude that binder modification with waste engine oil can be effective with other additives like polyphosphoric acid, Elvaloy, and hydrated lime.