Wood Content Research Articles

Scott Blair Fractional-Type Viscoelastic Behavior of Clear Spruce Wood: Influence of Compression Wood on Power-Law Stiffness Parameters

In this paper, we investigate the influence of intrinsic compositional parameters on the viscoelastic compliance by employing three-point bending creep tests on clear, i.e., defect-free, spruce samples with a dimension of 15 × 15 × 280 mm3. In addition to the regular samples, a prominent wood variation was investigated: so-called compression wood, stemming from an adaptive response of the growing tree to maintain structural stability. Tests were conducted at constant ambient conditions: isothermal at 20 degrees Celsius and at a relative humidity of 65 percent. These conditions were also employed during sample conditioning, leading to an equilibrium moisture content of the specimens of approximately 12 percent. Hence, so-called basic creep properties were investigated. Furthermore, we show that the experimentally observed compliance can be exceptionally well-modeled by a Scott Blair fractional-type element, with the latter calibrated by a mere number of two independent material parameters. This allows to render rather explicit dependencies of these parameters with respect to the dry density and the volumetric content of the compression wood. There, the quasi-instantaneous stiffness of the employed Scott Blair element is an increasing function of the dry density. While this primary dependency is also observed for compression wood, the quasi-instantaneous stiffness is significantly smaller over the investigated density range.

Predicting wood moisture classes by sound frequency spectra and Explainable Machine Learning during milling

ABSTRACT Varying moisture content in wood lead to problems in the automatic selection of optimised machining parameters. Therefore, production in the wood sector can be improved by the automatic identification of moisture classes during machining. In this work, wood milling was monitored by a novel optical microphone to detect differences in wood moisture classes. A full factorial randomised design was executed along with four moisture classes (dried, conditioned, wet and frozen) and two cutting speeds as independent variables. The measured signals were segmented by extracting information from each cut and were transformed to the frequency domain. A supervised univariate feature ranking based on χ ²-tests was applied to select the most important frequencies. Machine Learning was applied to the selected spectral data to classify the cutting speeds and moisture classes. After testing several classification models, ensemble models with regression-tree learners were the best-performing model type achieved an average validation accuracy of 97.2%. The model explanation was done by Local Interpretable Model-Agnostic Explanation based on regression trees as a simple model, where the frequencies that are responsible for the separation of the data could be identified and were used for retraining the model, achieving a validation accuracy of 90.5%.

Leveraging Spruce Bark Particle Morphology for Enhanced Internal Bonding in Particleboard Production.

The continuous rise in global demand for wood products has led to an increase in prices and a surge in research into alternative resources. As a byproduct of the timber industry, bark has emerged as a promising supplement in particleboard (PB) production. However, its anatomical structure, the presence of extractives, and its inferior mechanical properties complicate the production process, which have not yet been fully overcome at a commercial scale. This study proposes a paradigm shift, advocating for separate and specialized bark constituent processing in a wet state. Three bark-based raw materials-namely, outer bark particles, bark fiber clumps, and bark fibers-were investigated under varying wood content scenarios. PBs with a target density of 0.7 g/cm3 and a thickness of 16 mm were produced using mixtures of these bark-based materials and wood particles in different ratios bonded with a urea-formaldehyde adhesive. The results demonstrated that these bark constituents exhibit distinct properties that can be optimized through tailored processing techniques. Compared to bark fibers, outer bark particles displayed about 40% lower water absorption and thickness swelling. However, bark fibers improved the internal bond by about 50% due to their favorable morphology compared to outer bark. These findings highlight the potential of bark as a valuable resource for particleboard production and pave the way for its efficient utilization through specialized processing strategies.

Effect of Material Extrusion Process Parameters to Enhance Water Vapour Adsorption Capacity of PLA/Wood Composite Printed Parts

This study aims to optimise the water vapour adsorption capacity of polylactic acid (PLA) and wood composite materials for application in dehumidification systems through material extrusion additive manufacturing. By analysing key process parameters, including nozzle diameter, layer height, and temperature, the research evaluates their impact on the porosity and adsorption performance of the composite. Additionally, the influence of different infill densities on moisture absorption is investigated. The results show that increasing wood content significantly enhances water vapour adsorption, with nozzle diameter and layer height identified as the most critical factors. These findings confirm that composite materials, especially those with higher wood content and optimised printing parameters, offer promising solutions for improving dehumidification efficiency. Potential applications include heating, ventilation, and air conditioning systems or environmental control. This work introduces an innovative approach to using composite materials in desiccant-based dehumidification and provides a solid foundation for future research. Further studies could focus on optimising material formulations and scaling this approach for broader industrial applications.

Non-invasive method to measure bulk electrical resistivity of spruce wood – influence of moisture content and anatomical direction

ABSTRACT The correlation between electrical resistance and moisture content (MC) of wood has been studied for many years and is the basis for an important method for determining wood MC in practice. This study presents a non-invasive set-up using plate electrodes with a guard ring covered with silver foam and gold leaves to measure the direct-current (DC) electrical resistivity of spruce wood. The design ensures good electrical contact at a pressure of 0.68 MPa, without impairing the wood surface. Measurements were conducted across various moisture contents up to the fiber saturation point (FSP) for the three anatomical directions at a temperature of 21°C. The regression parameters between electrical resistivity and moisture content were determined with high coefficients of determination (R² = 0,97–0.98). The effect of MC on the electrical resistance was significantly more pronounced in the radial direction, and the electrical resistance in the axial direction was lower than in the radial and tangential direction. Those findings support the basic understanding of the electrical properties of spruce wood and provide a basis for non-invasive volume resistivity measurements of wood.

Characterisation of a novel sustainable wood-geopolymer masonry units

Masonry units have been fundamental to building construction for over 6000 years, making them one of the oldest and most widely used materials in the industry. However, their production using ordinary Portland cement has significant environmental impacts, including high carbon dioxide emissions and depletion of natural resources. This highlights the need for more sustainable alternatives. One promising option is the use of recycled aggregates from construction and demolition waste in masonry unit manufacturing. This paper investigates the use of chipped waste timber as aggregates, bound together with geopolymer cement made from industrial by-products such as fly ash and slag. The result is a new type of masonry units, referred to as wood geopolymer masonry units (WGMUs), which were evaluated against established standards and compared with conventional masonry units (CMUs). The innovative WGMUs demonstrated improved ductility and reduced density compared to CMUs, making them easier to handle and lighter in construction. They also have a distinctive, rustic texture and consistent dimensions that meet Australian standards. Although WGMUs exhibited higher water absorption and drying contraction due to their wood content, these characteristics generally remain within acceptable limits, supporting their potential as eco-friendly construction materials.

Structure–property correlation assessment of LLDPE‐based biocomposites with Azadirachta Indica wood flour

AbstractThis research explores the development of new composite material by integrating Azadirachta Indica (AI) with LLDPE to create wood‐plastic composites using the rotational molding process. By examining various proportions of AI wood flour blended with LLDPE, we investigated their impact on mechanical and physical properties. Our tests elucidate a clear correlation between mechanical properties and composite morphologies. Despite identical molding conditions, higher wood particle concentrations reduced mechanical properties compared to lower concentrations. Remarkably, a 12% wood content emerges as optimal, yielding a tensile modulus of 3.69 MPa and a flexural modulus of 468.5 MPa, with an acceptable reduction of 11% density and 13% porosity versus pure LLDPE. Additionally, we observed declines in tensile strength, impact strength, and hardness by up to 23%, 62%, and 11%, respectively, compared to neat LLDPE. Natural fillers enhance aesthetics, making these materials ideal for consumer products like garden equipment and furniture accessories.

Tropical peat composition may provide a negative feedback on fire occurrence and severity

Loss of peat through increased burning will have major impacts on the global carbon cycle. In a normal hydrological state, the risk of fire propagation is largely controlled by peat bulk density and moisture content. However, where humans have interfered with the moisture status of peat either via drainage, or indirectly via climate change, we hypothesise that its botanical composition will become important to flammability, such that peats from different latitudes might have different compositionally-driven susceptibility to ignition. We use pyrolysis combustion flow calorimetry to determine the temperature of maximum thermal decomposition (Tmax) of peats from different latitudes, and couple this to a botanical composition analysis. We find that tropical peat has higher Tmax than other regions, likely on account of its higher wood content which appears to convey a greater resistance to ignition. This resistance also increases with depth, which means that loss of surface peat in tropical regions may lead to a reduction in the subsequent ignitability of deeper peat layers as they are exposed, potentially resulting in a negative feedback on increased fire occurrence and severity.

Effects of heating media on microstructure and chemical composition of heat-treated Pometia pinnata

Changes of microstructure, crystallization, chemical composition, and equilibrium moisture content (EMC) of heat-treated wood (HTW) were investigated to explore the effects of heating media (saturated steam, superheated steam, air) and heat treatment (HT) temperature on HTWs. The results showed that the saturated steam induced more severe cell wall destruction than the other two media. Although the porosity slightly increased with the increasing HT temperature, superheated steam and air HT still decreased the porosity compared to that of control, whereas saturated steam HT increased the porosity. The HT increased both relative crystallinity and crystal size of HTWs. The increasing HT temperature slightly increased the relative crystallinity but decreased the crystal size. The highest crystallinity (55.0%) was observed after saturated steam HT. Leaching led to the increase of crystal size of HTW treated in saturated steam (about 0.15 nm), while those treated in unsaturated steam and air decreased. The increase in relative amount of lignin and cellulose due to the hemicellulose degradation were the main chemical changes of HTWs. Further lignin condensation reaction only occurred after saturated steam HT. Although saturated steam HT induced increased porosity, its lowest EMC (5.91%) indicated the decrease of hydroxyl groups.

Moisture sorption and its induced deformation of juvenile wood at different radial positions in poplar wood at the tissue scale

Juvenile wood exhibits significant variations in its properties across the radial direction, which responds strongly to water and can impact its applications in various scenarios. Wetwood, a specific presence in juvenile wood, is more prevalent in certain species. In this study, we focused on poplar (Populus x euramericana cv. 'San Martino') and analyzed the moisture content (M) and hygroscopic deformation of juvenile wood near the pith (wetwood) and in juvenile wood near the bark (normal wood) in real-time at the tissue scale (earlywood and latewood). To achieve this, we employed a dynamic vapor sorption analyzer in combination with a Dino-Lite Edge digital microscope. By utilizing the Guggenheim-Andersen-de Boer (GAB) model and the Kelvin equation, we examined the relationship between the bound water and hygroscopic deformation. The results revealed that the M in green condition of wetwood was significantly higher than that of normal wood. However, the disparity in moisture sorption capacity between wetwood and normal wood below the fiber saturation point contributed only minimally to this phenomenon. Regarding for hygroscopic deformation, it was observed that not all wetwood samples exhibited a greater shrinkage/swelling compared to normal wood samples. This variation can be attributed to structural factors, such as differences in microfibril angle, crystallinity, and cell wall ratios. Furthermore, it was found that the swelling ratio caused by 1 % of bound water (SwR-B) increased with rising relative humidity (RH) within the range of 0–90 % RH. However, the SwR-B stabilized or slightly decreased in the range of 90 %-95 % RH. This behavior is believed to be linked to the formation of capillary condensed water at higher humidity levels. Additionally, we found that the swelling ratio resulting from 1 % of polylayer water exceeded that caused by 1 % of monolayer water.

Additive manufacturing of wood composite parts by individual layer fabrication - influence of process parameters on product properties

Individual Layer Fabrication (ILF) is a novel additive manufacturing process that was developed to create objects with high wood content and high mechanical strength. Here, thin and individually contoured wood composite panels are created via Binder Jetting and subsequent mechanical pressing. Like in Sheet Lamination, these panels are then laminated onto each other to create a three-dimensional object. With wood contents (more than 85 mass percent) and mechanical properties (more than 30 MPa flexural strength) on par with other engineered wood products like particle boards and plywood, the produced objects are well suited for the construction and furniture industry. To gain a deeper understanding of the process, the influence of processing parameters on the geometric and mechanical properties of the finished objects were investigated. As process parameters the amounts of adhesive and the pressing forces for both panel production and lamination were selected. It was discovered that the interaction between the amount of adhesive and the pressure used to produce the panels is highly relevant for the geometric properties. The three core mechanisms that are responsible for the mechanical properties of produced parts were identified and can be ranked in the following order: 1) the amount of adhesive in the panels binding the particles, 2) the density of the panels, 3) the amount of adhesive for laminating the panels.

Snowpack permanence shapes the growth and dynamic of non-structural carbohydrates in Juniperus communis in alpine tundra

Climate warming is altering snowpack permanence in alpine tundra, modifying shrub growth and distribution. Plant acclimation to snowpack changes depends on the capability to guarantee growth and carbon storage, suggesting that the content of non-structural carbohydrates (NSC) in plant organs can be a key trait to depict the plant response under different snow regimes.To test this hypothesis, we designed a 3-years long manipulative experiment aimed at evaluating the effect of snow melt timing (i.e., early, control, and late) on NSC content in needles, bark and wood of Juniperus communis L. growing at high elevation in the Alps.Starch evidenced a general decrease from late spring to summer in control and early melting, while starch was low but stable in plants subjected to a late snow melt. Leaves, bark and wood have different level of soluble NSC changing during growing season: in bark, sugars content decreased significantly in late summer, while there was no seasonal effect in needles and wood. Soluble NSC and starch were differently related with the plant growth, when considering different tissues and snow treatment. In leaf and bark we observed a starch depletion in control and early melting plants, consistently to a higher growth (i.e., twig elongation), while in late snow melt, we did not find any significant relationship between growth and NSC concentration.Our findings confirmed that snowpack duration affects the onset of the growing season promoting a change in carbon allocation in plant organs and, between bark and wood in twigs. Finally, our results suggest that plants, at this elevation, could take advantage from an early snow melt caused by climate warming, most likely due to photosynthetic activity by maintaining the level of reserves and enhancing the carbon investment for growth.

Особенности роста и структуры древесины сосны на вырубке и под пологом древостоя в условиях Республики Карелии

The intraspecific variability of the anatomical and hydraulic characteristics of xylem in the undergrowth in Scots pine (Pinus sylvestris L.) has been assessed during natural regeneration in the felling areas and under the canopy of a middle taiga blueberry pine forest in the conditions of the European North (Republic of Karelia). The influence of habitat conditions on the formation of structural elements of wood cells has been revealed. In felling areas under conditions of higher illumination, air and soil temperatures, the transition of pine undergrowth to the category of large with a height of more than 1.5 m occurs at the age of 6 years, whereas under the canopy of a mature stand the undergrowth reaches this category no earlier than 15 years. At the same time, in the 1st decade of growth under felling conditions, the growth of pine in diameter has been 4 times higher than that of pine under the canopy of a mature stand due to the formation of a larger number of rows of tracheids in the early and late zones. In addition, the pine undergrowth in the felling area has the highest potential hydraulic conductivity of the xylem, and, on the contrary, the lowest specific density of tracheids, the basic wood density and late wood content relative to the pine undergrowth under the canopy of the stand. The latter exhibited a significant decrease in the structural and functional characteristics of wood, with the exception of the thickness of the cell membranes of late tracheids. In the interanual dynamics, more stringent linear regression dependencies between the indices of early and late tracheids have been observed in pine undergrowth under the forest canopy. The results obtained indicate a greater correspondence of the environmental conditions in the felling area to the optimum for the growth and formation of wood of young pine trees relative to the conditions under the canopy of a mature blueberry pine forest. Inhibition of the growth activity of undergrowth under the canopy occurs due to high intraspecific competition from the dominant pine stand for light, moisture and soil nutrition.

Mathematical modeling and performance evaluations of a wood drying process using photovoltaic thermal and double-pass solar air collectors

This research conducts a novel and complete 4E assessments and introduces an innovative method for examining solar wood drying systems. The software TRNSYS and MATLAB programming are combined to simulate and create a numerical program. This novel combination allows for a thorough examination that goes beyond conventional assessments of wood drying. The aim is to evaluate the effectiveness of a solar wood dryer using two different collectors, a double-pass and a photovoltaic thermal collectors, in terms of four key aspects: energy, exergy, economic, and environmental. Further, the drying process was investigated under various climates in three African cities (Errachidia, Dakar, and Nouakchott). The moisture content of wood was reduced from 74% to 12% in the three cities. Elaborate simulations were performed and the results were confirmed by experimental validation, using methods including Mean Absolute Error, Mean Relative Error, and Root Mean Square Error. The primary findings of this study are the following: In the double-pass dryer, the drying time required in Errachidia, Dakar, and Nouakchott was 139h, 189h, and 170h, respectively. Whereas in the photovoltaic thermal dryer, it needed 192h in Errachidia, 210h in Dakar, and 189h in Nouakchott. Further, using photovoltaic thermal, the dryer exhibited superior exergy efficiency compared to the use of double pass collector. Photovoltaic thermal collector reduces yearly CO2 emissions by an average of 54.87, 66.2, and 44.11 tonnesCO2 in Errachidia, Dakar, and Nouakchott, respectively. In contrast, double pass collector reduces CO2 emissions by an average of 38.49, 57.9, and 38.56 tonnesCO2 in Errachidia, Dakar, and Nouakchott, respectively, throughout the year. Further, the solar dryer, using double pass collector, has a shorter payback time than using photovoltaic thermal collector, indicating a quicker economic return.

New insights into the influencing mechanisms of hemicellulose removal on dynamic wood-water interactions characterized with low-field NMR

Hemicellulose, one of the most hygroscopic components, highly affected wood properties and wood-water interactions. To get more knowledge about the effects of hemicellulose on wood, this study changed hemicellulose content of wood through hydro-thermal removal of about 8 %, 20 % and 70 %. The dynamic cell water state and distribution during 384 h water absorption and air drying were characterized with low-field nuclear magnetic resonance technique (LFNMR). During water absorption, wood with less hemicellulose initially had higher and faster moisture increase, consisting of more free water in cell lumina and some large voids in cell walls than bound water in cell walls. The highest ratio of free water to bound water reached over 4.5, which was higher than that of untreated wood by over 15 %. This was because hemicellulose removal changed wood-water interaction environments suggested by SEM, FTIR and N2 absorption analysis. Specifically, hemicellulose removal enriched porous structures, especially the mesopore in cell walls. Although sorption sites decreased after hemicellulose removal, increased water paths and water accommodations played a more important role during initial water absorption. Besides, hemicellulose removal facilitated wood air drying, and the decreased moisture included more free water than bound water. This was because the enriched water paths accelerated water exchange, and sorption site decrease after hemicellulose loss reduced wood attraction to water molecules. Therein, the bound water leaving was generally slower than free water for hydrogen bond interaction with wood. The T2 s of bound water and free water were both shortened after hemicellulose removal, possibly because mesopore diameter reduction tightened wood-water bonding. This study provided new insights into understanding role of hemicellulose removal in dynamic wood-water interactions and facilitating development of wood processing technology.

Quality of Steam-Treated Bayur (Pterospermum javanicum) and Udu (Litsea accedontoides) Wood

Steam treatment is one of the thermall modification methods that used to improve the quality of wood, especially wood properties related to the presence of water. This study aims to evaluate quality of 2 types of trade wood in the West Nusa Tenggara region, namely bayur wood (Pterospermum javanicum) and udu (Litsea accedontoides) after steam treatment. Steam treatment was carried out at 126 ◦C for 1 hour using an autoclap device. The parameters tested included the physical properties of wood consisting of density, moisture content, volumetric swelling and Anti Swelling Efficiency (ASE). The mechanical properties of wood tested included Modulus of elasticity (MOE) and Modulus of Rupture (MOR). The results showed that steam treatment did not change the density but reduction in moisture content of bayur and udu wood. Based on the Anti Swelling Efficiency value, steam treatment effectively increased the dimensional stability of udu wood with a value of 88.81%. For mechanical property parameters, steam treatment graphically increased the MOE and MOR values of bayur and udu wood. However, according to SNI 03-3527-1194 there was no increase in the strength class of the two types of wood, and both types of wood were included in strength class III.

Prediction Distribution Model of Moisture Content in Laminated Wood Components.

Shrinkage cracks are some of the most common defects in timber structures obtained from woods with an uneven distribution of moisture content and are subject to external dynamic environmental changes. To accurately predict the changes in the moisture content of wood components at any time and position, this study first applied the principles of food drying and established a moisture field model for laminated wood based on the analogy between heat and humidity transfer. A model for predicting the moisture content of wood that considers time and spatial distribution was then proposed. Second, by collecting relevant experimental data and establishing a finite element analysis model, three moisture absorption conditions (0-9.95%, 0-13.65%, and 0-17.91%) and four desorption conditions (34-5.5%, 28-8.3%, 31-11.8%, and 25.5-15.9%) were analyzed. In the moisture absorption comparison, the time needed to reach 95% equilibrium moisture content was 2.43 days, 4.07 days, and 6.32 days. The rate at which the internal components reached equilibrium moisture content exceeded 10 days. The temporal and spatial distribution of wood moisture content revealed the correctness of the proposed wood moisture field model. Finally, the moisture content prediction model was applied in the order of characteristic equation solutions, moisture content gradient difference, and laminated wood size. The results revealed that the established humidity field model can predict the wood moisture content and how it changes over time and in space. Notably, 1-2 orders for the solution of the characteristic equation are recommended when applying the prediction model. The greater the difference in moisture content, the faster the equilibrium moisture content is reached. The moisture content varies greatly based on the component size and position. Notably, the influence of moisture gradient and wood size on the average wood moisture content cannot be ignored.

The hygroscopic behavior of surface compressed wood in response to superheated steam treatment at varying steam pressures

Superheated steam treatment has been shown to be an efficient strategy for enhancing the dimensional stability of compressed wood. This study evaluated the hygroscopic behavior of surface compressed (SC) wood subjected to superheated steam treatment (SHTSC wood) at varying steam pressures (0.1 MPa, 0.3 MPa, 0.5 MPa, and 0.7 MPa). As the steam pressure increased, the equilibrium moisture content (EMC) of SHTSC wood showed a gradual decrease throughout the hygroscopic range, indicating improved hygroscopic stability. The reduction in EMC for SC wood was associated with a decrease in polylayer moisture content (Ms) from 0% to 95% RH, while the EMC reduction for SHTSC wood was attributed to the combined effect of diminished monolayer (Mh) and Ms. The superheated steam treatment resulted in a range of chemical alterations in the SHTSC wood, including a decrease in hemicelluloses content and the quantity of sorption sites (–OH, C–O groups). Concurrently, there was a relative augmentation in the content of cellulose and extractives, alongside a heightened degree of lignin cross-linking. Furthermore, the superheated steam treatment also affected the cellular structure of the SHTSC wood, resulting in an increased ratio of macropores to mesopores, as well as the formation of microcracks within the cell wall. These changes became more pronounced as the steam pressure elevated, contributing to the reduced hygroscopic characteristics and improved dimensional stability of SHTSC wood.

Minimizing the polymer content of compressed transparent synthetic wood from renewable biomass sources: A comparative life cycle assessment

Transparent wood derived from renewable biomass resources has an enormous potential for utilizing in constructions, electrons devices, energy storage, etc. However, due to its high polymer content, the currently described transparent wood could not be developed in a sustainable manner. Herein, a feasible strategy for synthesizing compressed transparent wood was proposed to minimize the content of polymerized poly(methyl methacrylate) in composites, involving the poly(methyl methacrylate) partial-filling into the delignified wood and densification. This synthesis method prompted a substantial reduction of poly(methyl methacrylate) content (58.8%) in the obtained compressed transparent wood contrasted with the typical transparent wood (91.8% poly(methyl methacrylate) content). Besides, an ideal optical transmittance of 77.9% with 0.4 mm thickness and an optical haze of 49.2% with 0.7 mm thickness at 800 nm wavelength were achieved. Also, the improved tensile strength and flexural strength of compressed transparent wood were up to 85.0 MPa and 145.3 MPa, respectively. Additionally, a comparative life cycle assessment was conducted to assess the environmental impacts. The total environmental impact score was separately reduced by 23%, and 28% compared to the typical transparent wood and poly(methyl methacrylate) polymer, suggesting the feasibility of sustainable manufacture of transparent wood materials by decreasing polymer content. The compressed transparent wood also showed much lower thermal conductivities (0.28–0.31 W/mk) than glass and contributed to offering uniform illumination.

Protein content and antioxidant enzymes activity in reaction wood of poplar and their response to different levels of sustained bending stress

Protein content and antioxidant enzymes activity in reaction wood of poplar and their response to different levels of sustained bending stress