Compressive Creep Tests Research Articles

Investigation of the Mechanical Properties of Reinforced Calcareous Sand Using a Permeable Polyurethane Polymer Adhesive.

Calcareous sand has been widely used as a construction material for offshore projects; however, the problem of foundation settlement caused by particle crushing cannot be ignored. Although many methods for reinforcing calcareous sands have been proposed, they are difficult to apply on-site. In this study, a permeable polyurethane polymer adhesive (PPA) was used to reinforce calcareous sands, and its mechanical properties after reinforcement were investigated through compression creep, direct shear, and triaxial shear tests. The reinforcement mechanism was analyzed using optical microscopy, CT tomography, and mercury intrusion porosimetry. The experimental results indicate that there is a critical time during the compression creep process. Once the critical time is surpassed, creep accelerates again, causing failure of the traditional Burgers and Murayama models. The direct shear strength of the fiber- and geogrid-reinforced calcareous sand reinforced by PPA was approximately nine times greater than that without PPA. The influence of normal stress was not significant when the moisture content was less than 10%, but when the moisture content was more than 10%, the shear strength increased with an increase in vertical normal stress. Strain-softening features can be observed in triaxial shear tests under conditions of low confining pressure, and the relationship between the deviatoric stress and strain can be described using the Duncan-Chang model before softening occurs. The moisture content also has a significant influence on the peak strength and cohesive force but has little influence on the internal friction angle and Poisson's ratio. This influence is caused by the different PPA structures among the particles. The higher the moisture content, the greater the number of pores left after grouting PPA.

Features and Constitutive Model of Hydrate-Bearing Sandy Sediment’s Triaxial Creep Failure

In the longstanding development of hydrate-bearing sediment (HBS) reservoirs, slow and permanent deformation of the formation will occur under the influence of stress, which endangers the safety of hydrate development projects. This paper takes hydrate-bearing sandy sediment (HBSS) as the research object and conducts triaxial compression creep tests at different saturation degrees (20%, 30%, and 40%). The results show that the hydrate-containing sandy sediments have strong creep characteristics, and accelerated creep phenomenon will occur under the long-term action of high stress. The longstanding destructive power of the specimen progressively raises with the increase in hydrate saturation, but the difference in the triaxial strength of the specimen progressively increases. This indicates that the damage to the hydrate structure during long-term loading is the main factor causing the strength decrease. Further, a new nonlinear creep constitutive model was developed by using the nonlinear Burgers model in series with the fractional-order viscoplastic body model, which can well describe the creep properties of HBSS at different saturation levels.

High-Temperature Creep Resistance of FeAlOY ODS Ferritic Alloy.

A significant effort in optimizing the chemical composition and powder metallurgical processing led to preparing new-generation ferritic coarse-grained ODS alloys with a high nano-oxide content. The optimization was aimed at high-temperature creep and oxidation resistance at temperatures in the range of 1100-1300 °C. An FeAlOY alloy, with the chemical composition Fe-10Al-4Cr-4Y2O3 (wt. %), seems as the most promising one. The consolidation of the alloy is preferably conducted by hot rolling in several steps, followed by static recrystallization for 1 h at 1200 °C, which provides a stable coarse-grain microstructure with homogeneous dispersion of nano-oxides. This represents the most cost-effective way of production. Another method of consolidation tested was hot rotary swaging, which also gave promising results. The compression creep testing of the alloy at 1100, 1200, and 1300 °C shows excellent creep performance, which is confirmed by the tensile creep tests at 1100 °C as well. The potential in such a temperature range is the target for possible applications of the FeAlOY for the pull rods of high-temperature testing machines, gas turbine blades, or furnace fan vanes. The key effort now focuses on expanding the production from laboratory samples to larger industrial pieces.

In-situ synchrotron high energy X-ray diffraction study on the compressive creep behavior of an extruded Ti-45Al-8Nb-0.2C alloy

Wrought high Nb containing (high Nb-TiAl) alloys are potential materials for low pressure turbine blades in aero-engines. The performance and microstructure evolution under high temperature creep condition is of importance to the service stability of these materials. In this study, the internal strain and FWHM evolution of an extruded TNB-based high Nb-TiAl alloy during compressive creep are characterized by in-situ high energy X-ray diffraction (HEXRD) technique for the first time. The compressive creep test was conducted under a constant load of 300 MPa at 900 °C for 10 h in vacuum. The final creep strain is approximately 1.72 %. The microstructure and phase constitution after creep shows little difference from that before creep. Lattice strain analysis shows that γ phase is plastically deformed while the α2 phase deforms elastically due to the low creep strain. The lattice strain of α2 grains is dependent upon the deformation of surrounding γ grains. Creep induces dynamic recovery, exerting a softening effect. A high number of dislocations are visible in the γ lamellae while almost no dislocations exist within the α2 lamellae. α2 lamellae are partially decomposed and refined via the α2→γ transformation.

Experimental study on the mechanical properties of red sandstone with fractures under different loading rates

In order to study the effects of crack inclination angle and loading rate on rock mechanical properties, creep characteristics, and failure characteristics. Taking homogeneous red sandstone with different fracture angles as the research object, uniaxial compression tests and uniaxial compression creep tests were conducted at different loading rates. The results showed that under the same fracture angle, the loading rate was positively correlated with the peak strength, elastic modulus, instantaneous strain, creep strain, and steady-state creep rate of the sample, while negatively correlated with the peak strain. At the same loading rate, the mechanical properties and creep properties of the sample were controlled by the crack inclination angle α. With the increase of α, the peak strength, peak strain, instantaneous strain, creep strain and steady-state creep rate decreased first and then increased, and the elastic modulus increased. On the basis of rock creep testing, it is also important to establish a creep model that conforms to the actual test situation for studying rock creep characteristics. However, many models currently used cannot accurately describe the three stages of rock creep, especially the accelerated creep stage. Therefore, based on Burgers elements, this paper introduces plastic damage bodies based on damage rates and software components based on fractional calculus, A new creep model was obtained and its rationality was verified through experimental results. The results showed that the fit between the model and experimental data was above 0.97, indicating that the model can better describe the three stages of rock creep, especially reflecting the non-linear characteristics of the accelerated creep stage.

Deposition morphology and mechanical properties of lean cemented gangue backfill material: Laboratory test and field application

Backfilling mining technology provides an efficient and environmentally-friendly solution for treating additional products (such as tailings, coal gangue and other solid waste) in coal mining process, which are filled into the underground goaf area, thus reducing surface subsidence, roof strata damage, and associated geological disasters. In this study, a novel backfill material called lean cemented gangue backfill material (LCGBM) is introduced, and various experiments, including uniaxial compression tests, creep tests, CT-SEM scanning and reconstruction are carried out to evaluate its mechanical properties and engineering practicability. The test results indicate that the strength and volume fraction of self-compacting cement (SCC) slurry and solid waste aggregate jointly control the uniaxial compressive strength and failure mode of LCGBM, reflecting the bucket effect under the influence of two components. Although the volume fraction of aggregate and SCC slurry is intentionally reduced to control the cost, this cemented granular material shows excellent compressive strength, overall stiffness and long-term bearing capacity in laboratory and field tests. In the process of engineering application, the uniaxial compressive strength of the LCGBM reaches 14 MPa, and the initial setting time is 120 s, which reduces the consumption of gangue aggregate by 35 % and greatly reduces the construction time. In addition, a calculation method of the optimal mixing ratio of raw materials is proposed, which can adjust the strength and volume fraction of SCC slurry according to the optimal mixing range, so as to maximize the utilization of the strength of LCGBM, and reduce the construction time and aggregate of backfilling. The research findings emphasize the potential of the LCGBM in promoting clean and sustainable coal mining practice.

Experimental study on the creep acoustic emission of fractured sandstone reinforced by anchor rods

To investigate the reinforcement and crack-stopping effect of anchor rods on fractured rock masses, Triassic sandstone from the Xiaolangdi Reservoir area was selected and fabricated into double-fractured specimens. Subsequently, 1 and 2 horizontal anchor rods were used to reinforce the double-fractured sandstone specimens sequentially. Using the RLJW-2000 rock rheological servo tester and the PCI-II type acoustic emission (AE) tester, indoor uniaxial compression creep and AE tests were conducted under the same experimental conditions for the unanchored, singly-anchored, and doubly-anchored sandstone specimens. Based on the experimental results, the creep mechanical characteristics and the three-dimensional spatial evolution of the AE events of the specimens with different numbers of anchor rods were analysed. This study focuses on the reinforcement and crack-stopping effect of anchor rods on fractured rock masses. The experimental results indicate the following: (1) Compared with those of the unanchored specimens, the creep failure strengths of the singly- and doubly-anchored specimens increase by 7.79 % and 22.14 %, respectively. (2) At a stress level of 60 MPa, the axial strains of the single-anchor and double-anchor specimens decreased by 8.41 % and 32.97 %, respectively, compared to the corresponding strain of the unanchored specimen, and the radial strains decreased by 9.21 % and 28.13 %, respectively. (3) Anchor rods have a good reinforcement effect on fractured sandstone, enhancing specimen strength and reducing deformation. (4) With an increase in the number of anchor rods, the reinforcement effect of anchor rods on fractured rock masses strengthened, and the reinforcement effect of double anchors was superior to that of single anchors. (5) Compared with those of the unanchored specimens, under relatively low stress levels, when the AE events extended to the area where the anchor rods were located, the number of AE events for both types of specimens decreased significantly, forming a blank area in the AE events, and the blank area of the double-anchored specimens was larger than that of the single-anchored specimens. (6) With increasing stress, many AE events originated, expanded, and passed through the anchor rod area, indicating that the specimen was about to undergo creep instability failure. (7) The evolution characteristics of the AE events are in good agreement with those of the macroscopic cracks on the specimen surface. The AE characteristics indicate that anchor rods have a significant crack-stopping effect on fractured rock masses, suppressing the initiation, expansion, connection, and penetration of internal microcracks in the specimens. Moreover, the crack-stopping effect of double anchors is superior to that of single anchors.

Simulation method of asphalt mixture based on fracturable digital aggregate model

This study proposed an approach to construct a fracturable aggregate model to make the fracture patterns consistent with the real situation. Firstly, this study utilized three-dimensional structured light technology to obtain the geometric shell of aggregate and divide them into four categories of spherical, angular, elongated and flaky aggregates according to the minimum bounding box algorithm. Secondly, this study proposed a discrete-spheres filling algorithm based on the Bubble Pack Filling algorithm to fill the shell accurately. Thirdly, this study established the conversion equations between the macro and micro parameters of aggregate by using the linear parallel bonding model, and used it to establish the fracturable aggregate model. Through the indoor and virtual static fracture tests, this study found that the fracture patterns of the fracturable aggregate models are similar to the real situation and characterized the fracture patterns of four types of aggregates. Further analyzing the virtual static fracture tests, this study found that the bearing capacity of aggregates is determined by the compressive strength of host rocks and the shape of aggregate. Through the indoor and virtual uniaxial compression creep tests, this study investigated the behavior of the mixture specimens consisted by the fracturable aggregate model. The stress-strain curves of the fracturable and unfracturable aggregate model in this test were plotted in this study, and the results showed that the relative error between the results obtained by the fracturable model and those of the indoor test is much smaller than that of the unfracturable model. Considering that existing simulation tests on asphalt mixture often ignore aggregate deformation and fracture, so this study used the method mentioned above to obtain the fracturable aggregate model, which can improve the confidence of asphalt mixture simulation results.

Uniaxial compressive creep tests by spark plasma sintering of 70% theoretical density α-uranium and U-10Zr

Metallic fuels hold numerous advantages over conventional uranium dioxide fuels and are a key component of several liquid metal-cooled advanced reactor concepts including sodium fast reactors. These fuels undergo rapid swelling during early burnup; consequently, they spend most of their reactor lifetime in a porous state. The presence of this porosity alters many of the mechanical properties of the fuel including creep impacting fuel deformation during axial swelling. This work investigates the creep behavior of the porous fuel using a spark plasma sintering technique. Creep tests were performed for the first time on porous α-phase uranium and uranium with 10 wt. % zirconium (U-10Zr) samples. The samples of α-phase uranium and U-10Zr were fabricated from depleted uranium by spark plasma sintering and subjected to uniaxial compressive creep testing. Calculated stress exponents were found to be 2.6±1.6 and 5.7±1.4 for α-U and U-10Zr, respectively, and calculated activation energies were found to be 61.6±1.1kJ/mol for α-U. The creep data were also used to evaluate existing porosity inclusive in creep models.

Short term creep properties of WPC at different temperatures—An experimental and numerical investigation at different stress levels

AbstractUsing a two‐step molding process, wood plastic composite (WPC) were prepared under temperatures ranging from 160 to 180°C. Uniaxial compression tests of WPC were conducted at temperatures of −20°C, 0°C, 20°C, and 40°C, determining stress levels of 30%, 45%, and 60% based on the test results. Subsequently, 24‐hour compression creep tests were performed for WPC under 12 different conditions. The Findley power law model was employed to fit the experimental results, indicating that creep deformation increased with both stress level and environmental temperature. Notably, specimens at 0°C failed after sustaining a load for 13.6 hours at 60% stress, while those at 20°C failed after only 0.72 hours under the same conditions. Overall, the Findley model effectively predicted the creep behavior of WPC under all temperature conditions and stress levels.Highlights The influence of temperature variation on the strength of WPC. Short term creep of WPC under different stress levels. Creep of WPC at different temperatures. Prediction of creep performance under different operating conditions.

Creep Characteristics of Reconstituted Silty Clay under Different Pre-Loading Path Histories

Due to the long-term deformation settlement of foundations, issues such as damage and functional failure of buildings and structures have long been a concern in the engineering field. The creep of soil is one of the primary causes leading to long-term deformation of foundations. In this paper, the consolidation deformation, creep characteristics, and creep model of reconstituted saturated silty clay were studied using the isotropic consolidation creep test and triaxial compression creep test. The results show that for the isotropic consolidation creep test, although the applied load adopted different stages of loading, as long as the final applied confining pressure was the same, the number of stages applied by the confining pressure had little effect on the final isotropic consolidation deformation of the sample and the triaxial undrained shear strength after creep. However, for the triaxial shear creep test, it was found that under the same final deviatoric stress, the final deviatoric strain of the sample was closely related to the number of loading stages of deviatoric stress. The test showed that the more loading stages with the same deviatoric stress, the smaller the final deviatoric strain, and the triaxial undrained shear strength of the sample after creep increased. In addition, it was reasonable to set the pore pressure dissipation of the sample at 95% ((u0 − u)/u0 = 95%) as the time (t100) at which the primary consolidation of the soil sample was completed. The isotropic consolidation creep curves and the triaxial compression creep curves showed certain non-linearity. Then, the logarithmic model and the hyperbolic model were used to fit the creep curves of the samples. It was found that the hyperbolic model had a better fitting effect than the logarithmic model, but for the triaxial compression creep test, the creep parameters of the sample changed greatly. Therefore, studying the creep characteristics of soil under different pre-loading steps is of significant engineering importance for evaluating the long-term deformation of underground structures.

Experimental study on I/II/III mixed mode fracture characteristics of a combined rock mass under creep loading

I/II/III mixed mode fractures of intersecting joint fissures often occur in natural rock masses, and jointed rock masses are prone to rockbursts in deep underground engineering when subjected to long-term crustal stresses. However, most studies of the mechanical mechanisms of these intersected joints have been conducted by simplifying two-dimensional joint model tests. Furthermore, the fracture mechanisms of two-dimensional intersected joints under tension and compression are completely different from those of three-dimensional joints. This paper presents a novel prefabricated specimen with combinations of intersecting joints capable of detecting the failure behaviours of rock I/II/III mixed mode fractures under creep loading. Uniaxial compression and multistage creep tests are performed on prefabricated sandstone specimens with intersecting joints of 0°/0°, 0°/30°, 0°/60°, and 0°/90°. The experimental results show that with the increase in the number of prefabricated intersecting joints, the uniaxial compressive strength and elastic modulus values of the sandstone specimens gradually decrease. In addition, the sandstone specimens experience relatively few AE events and minor axial strain variations in the first creep stage and the second creep stage of the multistage creep test. The axial strain increases sharply due to the sharp increase in the number of AE events in the third creep stage. The 0°/60° sandstone specimen undergoes accelerated creep failure, resulting in mixed X-shaped tensile‒shear rupture. The RA value is high based on the quantification of the creeping cracks using the acoustic emission parameters of the rise angle (RA) and average frequency (AF). The AF values of the 0°/0°, 0°/30°, and 0°/90° sandstone specimens are high. The experimental results show that a larger joint intersection angle leads to greater mutual restraints and greater effects of prefabricated crack propagation in the rock specimens, thus increasing the final failure strength. Finally, based on the acoustic emission count, a characteristic variable D suitable for characterizing the creep damage evolution of a joint rock mass is established. The findings of this paper can facilitate an effective understanding of the creep effect of I/II/III mixed mode fracture and its micromechanism. The research results will have a certain reference value for the detection and risk mitigation of instantaneous and time-delayed rockbursts.

Anisotropic characteristics and creep model for thin-layered rock under true triaxial compression

The failure phenomenon of thin-layered rock tunnels not only exhibits asymmetric spatial characteristics, but also significant time-dependent characteristics under high in-situ stress, which is attributed to the time-dependent fracture of thin-layered rocks. This paper conducted a series of true triaxial creep compression tests on typical thin-layered rock siliceous slate with acoustic emission technique to reveal its anisotropic time-dependent fracture characteristics. The anisotropic long-term strength, creep fracturing process, and fracture orientation characteristics of thin-layered rocks under different loading angles (β, ω) and intermediate principal stress were summarized. A three-dimensional (3D) non-linear visco-plastic creep model for thin-layered rock was developed to simulate its anisotropic creep behavior. The time-dependent fracturing of rocks during true triaxial creep loading is reflected through the change of equivalent strain based on an improved Euler iteration method. By constructing the plastic potential function and overstress index related to loading angles and stress state, the anisotropic time-dependent fracturing process and propagation of thin-layered rocks under different loading angles and intermediate principal stress are expounded. The model was validated experimentally to show it can reflect the long-term strength and creep deformation characteristics of thin-layered rocks under true triaxial compression.

Quantitative investigation on the individual contribution of twinning and dislocation slip to creep in dilute Mg-Y alloys with various grain sizes

This work investigated the individual contribution of twinning and dislocation slip to creep in Mg-2 wt%Y alloys with different grain sizes. Three samples with the grain sizes of d = 31.2 μm, d = 63.5 μm and d = 127.7 μm were prepared by regulating the annealing treatment conditions, and the compressive creep tests were conducted at 473 K under 80 MPa along the rolling direction. It was found that the volume fraction of twins and the density of dislocations were continuously increased with increasing creep time regardless of grain size. During the first 50 h, the contribution of twinning was gradually increased while the contribution of dislocation slip was gradually decreased. Afterwards, the contributions of twinning and dislocation slip remained stable with increasing creep time in all samples. In addition, it was suggested that decreasing grain size could reduce the contribution of twinning but enhance the contribution of dislocation slip to creep. The results may provide reliable reference to the understanding and modeling of creep behaviors in Mg-RE alloys.

Improved creep resistance of Mo-V-Si-B alloys with a density below 8 g/cm³

Improving the efficiency of turbines for power plants and aircraft engines is an increasingly important research subject. Ternary Mo-Si-B alloys, consisting of a molybdenum solid solution (Moss) phase and two intermetallic phases Mo5SiB2 (T2) and Mo3Si, are able to combine balanced room temperature fracture toughness, high temperature creep strength and good oxidation performance. However, the high density (typically > 9 g/cm3) of this class of alloys is a drawback when used as structural materials for rotating components. In this study, high potential Mo-V-Si-B materials which provide a reduced density by about 17 % as compared with the reference alloy Mo-9Si-8B were investigated. A comparative characterization was carried out on sintered (FAST) and arc-melted Mo-40V-9Si-8B alloys. Compressive creep tests reveal competitive creep resistance of this new type of alloys in the application relevant temperature regime.

Investigation of the influence of pre-crack number on acoustic emission characterization of red-sandstone short-term creep damage and failure precursors

Rock crack is one of the main factors responsible for rock failure. Uniaxial compression creep tests are performed using acoustic emission techniques, a high-sensitivity, non-radiative, non-destructive testing method to understand the influence of crack number on the precursor characteristics of short-term creep damage in the fractured rock mass. Based on the Grassberger-Procaccia (G-P) algorithm, the calculation step size for the correlation dimension value (D 2) of the acoustic emission ringing count rate is consistent with that for the acoustic emission b-value. The influence of the number of pre-cracks on the Acoustic emission precursor characteristics of red sandstone creep is analyzed. The results show that near the destabilization of the specimen, the Acoustic emission accumulative ringing count surges in a stepwise manner, the Acoustic emission b-value decreases, the D 2-value increases, the Acoustic emission amplitude shows high intensity and high frequency, and the ringing count increases sharply, all with the characteristics of failure precursors. During the accelerated creep stage of the specimens, with the increase of pre-cracks number, the precursory time points of acoustic emission b-value and D 2-value advance, and their acoustic emission ringing counts increase sharply.

Effect of Cyclic Loading Treatment on the Compression Energy and Creep Properties of Machine-Harvested Seed Cotton

Machine-harvested seed cotton was taken as the research object to further clarify its creep performance, minimize its power consumption during the loading process, and obtain a better loading method. The uniaxial compression creep test was carried out using the Instron universal material test bench to apply cyclic loading treatment. The test factors included cyclic loading times, cyclic stress peak, and cyclic loading frequency. The energy consumption curve of the machine-harvested seed cotton during cyclic loading was obtained through OriginPro 2019b software, and its energy change law was analyzed. Creep strain was divided into two parts, namely, initial creep strain and creep strain increment, to elucidate the creep mechanism. The Burgers model was chosen to describe the creep strain increment. Results show that machine-harvested seed cotton exhibits energy consumption hysteresis during cyclic loading. The compression energy rapidly decreases with increasing cyclic loading times and then stabilizes. Meanwhile, the compression energy increases with increasing cyclic stress peak and cyclic loading frequency. The creep strain mechanism is also the same, which first rapidly increases and then levels off. Cyclic loading times, cyclic stress peak, and cyclic loading frequency have different effects on creep strain increment, instantaneous elastic modulus, hysteresis elastic modulus, viscosity coefficient, delay time, and relative deformation index. Finally, disregarding power consumption and interaction, extending the cyclic loading time, and increasing the cyclic stress peak while simultaneously minimizing the cyclic loading frequency can reduce the relative deformation index in the creeping stage. Accordingly, the deformation retention ability in the creep is improved, but the compression energy in the cyclic loading increases. The results can provide theoretical and data support for studying the theoretical basis of the rheological properties of machine-harvested seed cotton, the design of seed cotton baling devices, and the study of bale (mold) forming quality.

Effects of Al3Ni compound on localized plastic deformation and creep strain of Al/Si hypoeutectic material

The mechanical resistance of AS10/xNi hypoeutectic alloy with (x = 0.05% and 0.1%) has been investigated. Vickers hardness (HV) was determined for the samples before and after sintering. All samples were subjected to a compressive creep test at a constant temperature of 298 K and a constant load of 45 MPa. Creep parameters, such as creep rate, sensitivity (m), time exponent (n), β, and ɣ have been calculated and related to the Ni content. Microstructure investigation was conducted using the scanning electron microscope technique (SEMT). After sintering, the results showed that there was a significant improvement in the hardness with the addition of nickel. There is an increase in creep resistance as a result of the distribution of Al3Ni chemical compound across grain boundaries, which stops additional dislocation movement and hence reduces the creep rate.

Factors Affecting Properties of Polymer Grouted Sands

The aim of this research was to undertake laboratory testing to investigate the beneficial effects of epoxy resin grouts on the physical and mechanical properties of sands with a wide range of granulometric characteristics. Six sands of different particle size and uniformity coefficients were grouted using epoxy resin solutions with three ratios of epoxy resin to water (3.0, 2.0 and 1.5). A set of unconfined compressive strength tests were conducted on the grouted samples at different curing periods and a set of long-term unconfined compressive creep tests in dry and wet conditions after 180 days of curing were also carried out in order to evaluate the development of the mechanical properties of the sands, as well as the impact of water on them. The findings of the investigation showed that epoxy resin resulted in appreciable strength values in the specimens, especially those of fine sands or well graded sands, grouted with the different epoxy resin grouts. Whilst the higher compressive strength and elastic modulus values at the age of 180 days were obtained for the finer sand, which ranged from 2.6 to 5.6 MPa and 216 to 430 MPa, respectively, the lower compressive strength and elastic modulus values were attained for the coarser sand with low values of the coefficient of uniformity, which varied from 0.68 to 2.2 MPa and 75 to 185 MPa, respectively. Moreover, all grouted sands showed stable long-term creep behaviour, with high values of the creep limit ranging from 67.5 to 80% of compressive strength. The presence of water had a negative marginal effect in the majority of the grouted specimens. In terms of physical properties, the permeability and porosity were estimated. The permeability of fine sands or well graded sands was decreased by two to four orders of magnitude. Using laboratory results and regression analysis, three mathematical equations were developed that relate each of the dependent variables of compressive strength, elastic modulus and coefficient of permeability to particular explanatory variables.

Insights into creep behavior of Mg–14Gd–1Zn–0.4Zr (wt.%) alloy containing β- and γ-type precipitates

Compressive creep tests were performed on sand-cast and peak-aged Mg–14Gd–1Zn–0.4Zr (wt.%) alloys at 250 °C in this study. The microstructures before creep and at the secondary creep stage were analyzed by scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The results showed that plenty of fine precipitates, especially β′-series precipitates or a combination of β-type and γ′ precipitates, could effectively enhance the creep resistance of Mg alloys. Large amounts of β'+β′F precipitate chains in the regions near grain boundaries of the sand-cast alloy blocked the motion of <c + a>-type dislocations, while the interaction of basal and prismatic <a> dislocations could be inhibited by synergy of γ′ and β-type precipitates. In contrast, transformation of β′-series precipitates to β1 or β precipitates in the peak-aged alloy reduced their capacity to impede the <c + a> dislocation movement, seemingly presenting worse microstructures for creep resistance. However, the peak-aged alloy exhibited a uniform distribution of numerous semi-coherent β1 precipitates and dense rectangular networks composed of γ′ and β-type precipitates within the whole grain, which was superior to the uneven distribution of β-type and γ′ precipitates as well as a lack of ample precipitates at the center of grain in the sand-cast alloy. Thus, the peak-aged Mg–14Gd–1Zn–0.4Zr alloy obtained better creep resistance than the sand-cast alloy to some extent.