This study investigates the substitution of traditional burnt clay bricks (BCB), used since 7000 BCE, with environmentally friendly Fly Ash-Cement and Sand Composite Bricks (FCBs), utilizing industrial waste like Coal Fly Ash (CFA) from thermal power plants. The research encompasses two phases: the first involves experimental production of FCBs, while the second focuses on optimizing FCBs by varying CFA (50%, 60%, 70%), Ordinary Portland Cement (OPC) content (9%–21%), and incorporating stone dust (SD) and fine sand. Comprehensive tests under normal and steam curing conditions, adhering to ASTM C 67-05 standards, include X-Ray Diffraction (XRD), Energy Dispersive X-Ray (EDX), and Scanning Electron Microscopy (SEM) analyses. Results indicate that steam curing enhances early strength, with an optimized mix (MD: 5S) achieving a compressive strength of 15.57 MPa, flexural strength of 0.67 MPa, water absorption rate of 20.08%, and initial rate of water absorption of 4.64 g/min per 30 in2, devoid of efflorescence. Notably, a 9% OPC and 50% CFA mix (MD: 1S) shows improved early strength of 4.95 MPa at 28 days. However, excessive CFA replacement (70%) with lesser cement content negatively impacts physio-mechanical properties. This research underscores the potential of FCBs as a sustainable and economically viable alternative to BCBs in the construction industry.
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