Color Stability Of Resin Composites Research Articles

Effect of Toothpaste Fluoride Concentration on Color Stability of Resin Composites: An In Vitro Study

Effect of Toothpaste Fluoride Concentration on Color Stability of Resin Composites: An In Vitro Study

Digital Photography versus Spectrophotometry Assessment ofColor Stability of Resin Composite

Purpose: To compare digital photography to spectrophotometry in evaluating the color stability of resin composite. Materials and methods: Thirty- two disc-like specimens of Filtek Z350 resin composite were prepared and color-assessed; before and after 30 days of submersion in coffee solution. For each specimen, color was assessed according to Commission Internationale de I’Eclairage (CIE) color space values using: Two different versions of Canon Digital Single Lens Reflex (DSLR) camera; with standard lenses, flash, and settings: Canon 600d (Group I) and Canon 1100d (Group II), and a digital spectrophotometer (Vita Easyshade advance 4.0; Vita Zahnfabrik, Bad Sackingen, Germany) as a control (group lll). Color change (ΔE) was recorded for individual devices, tabulated, and statistically analyzed using oneway ANOVA, then Tukey’s post hoc test (P ≤ 0.05). Results: Statistically, no significant difference appeared among the used devices (P≤ 0.05) while assessing the color stability of Filtek Z350 resin composite. Conclusions: Both devices are similarly valuable for color assessment of resin composite.

Wear and Color Stability of Preheated Bulk-fill and Conventional Resin Composites.

Bulk-fill resin composite is commonly used in direct restorations. It is recommended that the high-viscosity version of these materials be preheated to improve flowability and adaptability. It is unknown what effects preheating (PH) might have on the wear resistance and color stability of these resin composites. This study compared the wear and color stability of high-viscosity bulk-fill and conventional resin composites with and without PH, using the CIEDE2000 formula. Thirty-two disc-shaped specimens (n=16, 10×3 mm) were prepared with Filtek One Bulk Fill Restorative (FOBFR; 3M ESPE) and Filtek Supreme Ultra (FSU, 3M ESPE) to determine wear. Each group was divided into subgroups based on preparation conditions, that is, PH and room temperature (RT) (n=8). Thermomechanical fatigue was applied to specimens, and volumetric material loss was calculated using a laser scanner (LAS-20, SD Mechatronik, Feldkirchen-Westerham, Germany) and three-dimensional imaging software (Geomagic, 3D Systems, Rock Hill, SC, USA). An additional 124 disc-shaped specimens (n=64, 10×1 mm) were prepared with FOBFR and FSU, and subgroups were formed based on preparation conditions (PH and RT, n=32). Specimens were aged for 14 days in coffee, grape juice, distilled water, and thermocycling (20,000 cycles, 5°C-55°C). To determine color change, the lightness (L), chroma (C), and hue (H) values were measured at baseline and after 14 days using the CIEDE2000 formula. All data were statistically analyzed, and a 95% significance level was set. In both the PH and RT groups, FSU exhibited greater wear than FOBFR (p<0.05). Both materials were subjected to increased wear as a result of PH. After aging, a significant difference in color change was observed (p<0.05) when controlling for time and resin composite type, except for deionized water and thermocycling (p>0.05). PH had no effect on the color stability of the resin composite at any time (p<0.05). The high-viscosity bulk-fill resin composite displayed superior wear resistance and similar color stability compared with its conventional counterpart. PH resin composite may increase its susceptibility to wear and has no effect on its color stability.

Effect of finishing protocols and staining solutions on color stability of dental resin composites.

ObjectiveThe objective of this study was to evaluate the effect of finishing protocol and exposure to staining solutions on color stability of dental resin composites.Materials and MethodsA nanofill and microhybrid composite, three finishing protocols (mylar, Soflex disc, and white polishing stone) and four staining solutions (tea, red wine, khat extract—two concentrations, control—distilled water) were evaluated. A digital spectrophotometer was used for color change (ΔE) measurements employing the CIE‐Lab‐color system. Paired/independent‐sample t test and two‐way analysis of variance (ANOVA) followed by Tukey's honestly significant difference posthoc test were used for inferential statistics at α = .05.Results Soflex finish was associated with least staining and comparable color stability for the two materials in tea and red wine. In Khat 2, microhybrid composite had statistically significant better color stability than nanofill for Soflex finish (14 days t = 3.270, p = .011). For microhybrid composite, mylar resulted in highest mean ΔE, whereas Soflex recorded the least in all staining solutions. For nanofill composite, white stone resulted in highest mean ΔE, whereas Soflex demonstrated the least mean ΔE in all staining solutions, except red wine where mylar demonstrated the least mean ΔE. For mylar finish, nanofill demonstrated statistically significant better color stability than microhybrid in both red wine (14 days t = 4.902, p = .001) and Khat 1 (14 days t = 3.252, p = .012). For stone finish, microhybrid demonstrated statistically significant better color stability than nanofill in all staining solutions (14 days t ≥ 4.785, p ≤ .001). Two‐way ANOVA showed a statistically significant difference in mean ΔE between and within specimens (F = 42.658, p < .001). All staining solutions caused clinically unacceptable discoloration for mylar and white stone finish. For Soflex finish, red wine produced clinically unacceptable color difference beyond 48 h.ConclusionThere was a difference in color stability of resin composites depending on filler type, further influenced by finishing protocol. Soflex disc finish results in better color stability than mylar and white stone in both microhybrid and nanofill composites.Clinical significanceEsthetic dental restorations such as resin composites are routine in contemporary restorative practice. Color stability of composites may be influenced by surface finish, dependent on the filler type, and consumption of chromogenic substances such as khat. To prolong their service, selection of suitable finishing protocols is an important consideration.

Effect of surface sealants on color stability of different resin composites

The aim was to assess the effect of surface sealants on the color stability of different composite materials. 120 samples were prepared using Filtek Ultimate (3M, USA), Charisma Topaz (Kulzer, Germany), and Clearfil Majesty Es-2 Premium (Kuraray Noritake, Japan) composites. The samples were polished with polishing discs and divided by test groups (n=10 for each), regarding the sealant used; Permaseal (Ultradent Products, USA), Biscover LV (Bisco, USA), Optiglaze Clear (GC Corp., Japan) and control. The samples were discolored for 144 hours in coffee solution at constant 37ºC, renewing daily. Color measurements were performed at the baseline, following the sealant application, and after discoloration procedure, using a spectrophotometer (EasyShade 5, Vita-Zahnfabrik, Germany). The collected L*C*h* coordinates were converted to corresponding L*a*b* coordinates and the color changes (ΔE) were calculated. All the sealants presented perceptible (>1.2) and unacceptable (>2.7) color changes. Biscover LV presented the lowest ΔE among all sealants (p<0.001). The highest ΔE was observed for Permaseal (p<0.001). Color changes for Optiglaze and control groups were similar (p≥0.05). Filtek Ultimate presented the highest color stability (p<0.001), followed by Charisma Topaz and Clearfil Majesty. The combination of Filtek Ultimate with Biscover LV was considered to have the highest color stability, whereas the combination of Clearfil Majesty with Permaseal was considered the lowest, among all. Experimented sealants were considered relatively effective on color stability of resin composites depending on the type of the sealant and the composite material. However, the use of surface sealants may not be advantageous every time. Biscover LV have inhibited the level of discoloration, whereas Permaseal had an increasing effect generally.

Color stability of resin composites for orthodontic attachments: an in vitro study.

ABSTRACTObjective: The aim of the present study was to evaluate the color stability of Filtek Z350 XT, Filtek Z250 XT, Z100 resin composites and Transbond XT orthodontic resin, all used in orthodontic attachments, when immersed in popular beverages. Methods: Thirty disk-shaped specimens of each resin composite (2 x 5mm) were manufactured and randomly divided into six groups according to immersion solutions: coffee, red wine, white wine, regular beer, dark beer and deionized water (control). The specimens were fully immersed in each of the solutions for six days at 37°C, representing approximately six months of consumption. The color measurements were evaluated by a reflection spectrophotometer, at baseline (before immersion) and after staining. L*a*b* coordinates were measured and the color change (ΔE00) was calculated using the CIEDE2000 formula. The data were analyzed by ANOVA/Tukey tests at a significance level of 0.05. Results: The resin composites immersed in white wine and regular beer showed either imperceptible or clinically acceptable ΔE00, and no difference from the control group (p= 0.4449 and p= 0.467 respectively). Immersion in coffee and red wine were considered clinically unacceptable and were significantly different from the control group (p= 0.0028 and p= 0.0475 respectively). Conclusion: Based on the results of the present study, the consumption of coffee and red wine may cause color change of the resin composite attachments above the visual acceptability threshold, and impair aesthetics during treatment.

Influence of Storage Media on Color Stability of Different Resin Composites as Determined by ΔE and ΔE00

Abstract Objective: To evaluate the color stability of 3 different resin composites when exposed to storage in water, air or artificial saliva. Materials and Methods: <span style=font-size:10.0pt; font-family: times= new= roman,serif;mso-ansi-language:en-us=>Initial color of 81 specimens was assessed by a calibrated reflectance spectrophotometer over a black as well as a white background. Specifically, 9 disc shaped specimens made out of 3 resin composite materials were kept in distilled water, air and artificial saliva (Glandosane) at 37°C. After a storage period of 4 weeks, spectrophotometric measurements were repeated and the color changes calculated by means of ΔE and ΔE00. Results: When analysed over a white background, median ΔE values varied from 0.6 (Filtek Supreme Dentin/water) to 7.1 (Filtek Supreme Enamel/Glandosane). When analysed over a black background median ΔE values varied from 0.4 (Filtek Supreme Dentin/water) to 5.0 (Filtek Supreme Enamel/Glandosane). When analysed over a white background, median ΔE00 values varied from 0.4 (Filtek Supreme Dentin/water) to 4.6 (Filtek Supreme Enamel/Glandosane). When analysed over a black background median ΔE00 values varied from 0.4 (Filtek Supreme Dentin/water) to 4.6 (Filtek Supreme Enamel/Glandosane). Statistical analysis performed by means of ANOVA and Fisher’s LSD post hoc tests showed differences between groups. The correlation between ΔE and ΔE00 was 99.09% and 99.65% over black and white background, respectively. Conclusion: Within the limits of the present study, storage media significantly influenced color stability of resin composites.

Comparison of color stability of two resin composites in blood area

Introduction: Color change of composite restorations in different color media over time is a common problem in esthetic dentistry, creating the need to replace the restoration and spending a great deal of cost and time by patients. The aim of this study is in vitro comparison of color stability of resin composites in blood area. Materials and Methods: Fifteen disk-shaped specimens of each resin composite (valux plus and filtek supreme) were prepared. The samples were kept in distinct water containers for 24 h in order for the primary water absorption to happen by restorative materials. Then, for 1 month, they were immersed in blood every day for 20 min. The color values (L*, a*, and b*) were measured using the CIE L*a*b* system. The color change values were calculated before and after 1, 7, and 30 days of immersion. The amounts of ΔE1, ΔE7, ΔE30 for each group were calculated with ΔE = [(ΔL*)2 + (Δa*)2 +(Δb*)2]½. Repeated measures and paired t-tests and one-way analysis of variance (ANOVA) were applied for the statistical analysis. Results: The discoloration in two groups was not significant and visually perceptible. However, microhybrid samples at primary time (less than 7 days), under the significant level, showed more discoloration, but nanofilled’s samples discoloration increased till the 30th day. Conclusion: Blood as a biological agent that contains globulin as a large molecule, did not have a significant impact on changing the color of the resin composite.

Correlation between three-dimentional surface topography and color stability of different nanofilled composites.

The aim of this study was to evaluate the 3-dimensional (3D) surface topography and color stability of four different resin composites after immersion in different soft-beverages. One hundred sixty disk-shaped specimens (diameter: 10 mm, and thickness: 2 mm) were made from four different resin composites (i.e., Filtek Z550, Tetric N-Ceram, Clearfil Majesty Esthetic, and Cavex Quadrant Universal LC). Each specimen was cured under mylar strips for 20 sec for both top and bottom surfaces. All of the specimens were stored in distilled water for 24 h at 37°C. Surface measurements were carried out using a noncontact 3D-optical-profilometer in terms of surface topography (Ra values). Color measurements of each specimen were performed with Vita Easy Shade system. All the measurements were performed at baseline and after 30 days of immersion in the selected soft-beverages (Redbull, Coca-Cola and Dimes-Lemonade). Control groups were stored in distilled water during the study. Ra values and color changes (ΔE values) of the groups were recorded. The data were statistically analyzed using a one way ANOVA and Tukey's post-hoc tests (SPSS 18.0). The tested soft-beverages in the present study caused color changes at a 30-day evaluation period for the tested resin composites (p < 0.05). However, 3D surface topography of resin composites was not influenced by the tested soft-beverages (p > 0.05). There was no significant interaction between the composite and beverage type on the Ra values of the resin composites (p > 0.05). No correlation was found between color stability and 3D surface topography of the resin composites. Color stability of resin composites may be affected by soft beverages.

Effect of finishing and polishing on color stability of a nanofilled resin immersed in different media

OBJECTIVE: The purpose of this study was to evaluate the effect of finishing and polishing on color stability of a nanofilled composite resin (Filtek Z350 XT) according to different immersion media.MATERIAL AND METHOD: Composite disks (10 mm diameter, 2 mm thickness) were prepared for each group (n = 6) using a stainless steel mold. The groups were divided according to the presence or absence of finishing and polishing procedure and immersion media (artificial saliva, artificial juice- KAPO(r) Coca-Cola(r)flavors: pineapple, orange, strawberry and grape). The finishing and polishing procedures were performed using Super -Snap(r) disks. The specimens were stored in artificial saliva for 24 hours (baseline) and were analyzed using a color spectrophotometer by CIELab system. Then, they were immersed in different media for 5 minutes, 3 times a day, every 4 hours during 60 days. They were stored in artificial saliva at 37 ± 1°C during the immersion intervals. After this time, new measure of color was performed. The data were analyzed using Kruskall-Wallis test and Mann- Whitney test. The significance level was 5%.RESULT: The results showed that the finishing/polishing not significantly influence the color stability of resin composite (p &gt; 0.05). There was no statistically significant difference in the color stability of the studied resin after immersion in different media (p &gt; 0.05).CONCLUSION: The finishing and polishing procedures and the immersion media did not have influence on color stability of nanofilled resin Filtek Z350 XT.

Effect of Different Polishing Systems and Drinks on the Color Stability of Resin Composite

The purpose of this study was to evaluate the color stability of resin composit using different finishing systems and drinks. Composit disks (5 mm diameter, 2 mm thickness) were prepared for each nanofilled composite using a brass mold. The specimens were divided into 5 finishing system groups Mylar strip (Mylar, DuPont, Wilmington, Del., USA), Soft Lex (3M(™) ESPE(™) St. Paul, MN, USA), Enhance (Dentsply-DeTrey GmbHD Konstanz, Germany), Hiluster (KerrHawe, Bioggio, Switzerland), Opti Disc (KerrHawe, Bioggio, Switzerland) and each group was divided into 10 subgroups (n = 10) and stored for 24 hours at 37°C in different drinks water coffee, coffee with sugar, tea, tea with sugar, diet coke, coke, light sour cherry juice or sour cherry juice. Color of all specimens was measured before and after exposure with a spectrophotometer using CIE L*a*b* relative, and color changes (ΔE*) were then calculated. The data were analyzed with a twoway analysis of variance (ANOVA), and mean values were compared by the Tukey HSD test (p = 0.05). For the drinks, the lowest ΔE* values were observed in the water and highest ΔE* values were observed in sour cherry juice. When drinks with and without sugar were compared, all groups with sugar demonstrated a higher color difference than without sugar. For the different finishing systems, Mylar strip group demonstrated significantly highest color change; Enhance groups demonstrated significantly lowest color change. Finishing treatments and storage solutions significantly affect the color stability of resin composite. The presence of sugar in drinks increased the color difference compared to drinks without composit. Polishing techniques and drinking drinks with sugar may affect the color of esthetic restorations.

Effects of different polishing methods on color stability of resin composites after accelerated aging

The purpose of this study was to evaluate the effect of polishing procedures on the color stability of different types of composites after aging. Forty disk-shaped specimens (Ø10×2 mm) were prepared for each composite resin type (an ormocer, a packable, a nanohybrid, and a microhybrid) for a total of 160 specimens. Each composite group was divided into four subgroups according to polishing method (n=10): control (no finishing and polishing), polishing disk, polishing wheel, and glaze material. Color parameters (L*, a*, and b*) and surface roughness were measured before and after accelerated aging. Of the polishing methods, glazed specimens showed the lowest color change (∆E*), ∆L*, and ∆b* values (p<0.05). Of the composite resins, the microhybrid composite showed the lowest ∆E* value, whereas the ormocer showed the highest (p<0.05). For all composite types, the surface roughness of their control groups decreased after aging (p<0.05). In conclusion, all composite resins showed color changes after accelerated aging, with the use of glaze material resulting in the lowest color change.

Color stability, conversion, water sorption and solubility of dental composites formulated with different photoinitiator systems

ObjectivesThe aim of this study was to formulate materials with high color stability and reduced degradation by using photoinitiator systems derived from phosphine oxides alternative to the traditional camphorquinone (CQ)/amine system. MethodsMaterials were formulated with the monomers BisGMA and TEGDMA as organic matrix. The photoinitiators tested were CQ+amine (EDMAB), phenylbis(2,4,6-trimethylbenzoyl)phosphine oxide (BAPO), BAPO+EDMAB, diphenyl(2,4,6-trimethylbenzoyl)-phosphine oxide (TPO) and TPO+EDMAB. A 60% mass of silanated glass filler particles was added. Degree of CC conversion was evaluated by Fourier-transformed infrared spectroscopy 10min after photopolymerization. The color properties were evaluated by a digital spectrophotometer, applying the CIELab parameters, either before photoactivation, immediately after photoactivation, 24h after dry storage, and one month after water immersion. Water sorption and solubility were assessed by mass gain or loss after storage in water for 30 days. Data were analyzed using ANOVA and Tukey's test (5%). ResultsDegree of conversion did not differ statistically among all the tested formulations. Regarding color, only groups with TPO presented satisfactory color stability after one month of water storage (ΔE<3.3). Water sorption and water stability did not differ among the groups. ConclusionsDegree of conversion, water sorption and water solubility did not differ among all the tested groups. The TPO-based groups were the only materials with satisfactory color stability after one month of water storage. Clinical significanceThe use of a photoinitiator system containing TPO might improve the color stability of resin composites compared with the traditional CQ/amine system while attaining similar physico-chemical properties for the composite.

Effect of the difference in spectral outputs of the single and dual-peak LEDs on the microhardness and the color stability of resin composites

Objectives: To determine the effect of the spectral output of single and dual-peak light emitting diode (LED) curing lights on the microhardness and color stability of commercial resin composites formulated with camphorquinone and alternative photoinitiators in combination. Materials and Methods: Three light-polymerized resin composites (Z100 (3M ESPE), Tetric Ceram (Ivoclar Vivadent) and Aelite LS Posterior (Bisco)) with different photoinitiator systems were used. The resin com- posites were packed into a Teflon mold (8 mm diameter and 2 mm thickness) on a cover glass. After pack- ing the composites, they were light cured with single-peak and dual-peak LEDs. The Knoop microhardness (KHN) and color difference (ΔE) for 30 days were measured. The data was analyzed statistically using a student' s t-test (p < 0.05). Results: All resin composites showed improved microhardness when a third-generation dual-peak LED light was used. The color stability was also higher for all resin composites with dual-peak LEDs. However, there was a significant difference only for Aelite LS Posterior. Conclusions: The dual-peak LEDs have a beneficial effect on the microhardness and color stability of resin composites formulated with a combination of camphorquinone and alternative photoinitiators. (J Kor Acad ABSTRACT

Color stability of resin composites after immersing in coffee of different temperature - An in vitro study

Color stability of resin composites after immersing in coffee of different temperature - An in vitro study

Effects of Mouth Rinses on Color Stability of Resin Composites

The aim of this study was to evaluate the effects of 3 commercially available mouth rinses on the color stability of 4 different resin-based composite restorative materials. Forty disc-shaped specimens (10x2 mm) were prepared from each of the following materials: A nanofill composite Filtek Supreme XT (3M/Espe, St. Paul, MN, USA); a packable low-shrinkage composite, AeliteLS Packable (BISCO, Inc, Shaumburg, IL, USA); nanoceramic composite resin Ceram-X (Dentsply, Konstanz, Germany); a microhybrid composite, and Aelite All-Purpose Body (BISCO). The specimens were then incubated in distilled water at 37 degrees C for 24 hours. The baseline color values (L*, a*, b*) of each specimen were measured with a colorimeter according to the CIELAB color scale. After baseline color measurements, 10 randomly selected specimens from each group were immersed in 1 of the 3 mouth rinses and distilled water as control. The specimens were stored in 20 mL of each mouth rinse (Oral B Alcohol-free, Listerine Tooth Defense Anti-cavity Fluoride Rinse and Klorhex) for 12 hours. After immersion, the color values of all specimens were remeasured, and the color change value DeltaE*ab was calculated. Data were analyzed using a 2-way analysis of variance at a significance level of .05. All specimens displayed color changes after immersion, and there was a statistically significant difference among restorative materials and mouth rinses (P<.05); however, the change was not visually perceptible (DeltaE*ab<3.3). The interaction between the effect of mouth rinses and type of restorative materials was not statistically significant (P>.05). It may be concluded that although visually nonperceptible, all resin restorative materials tested showed a color difference after immersion in different mouth rinses.

The Effect of Curing Units and Staining Solutions on the Color Stability of Resin Composites

This study investigated the effects of two different light curing units and two staining solutions on the color stability of a hybrid composite and a nanohybrid composite after different immersion periods. Thirty disk-shaped specimens (10 mm in diameter, 2-mm thick) were fabricated for each of the resin composites, Clearfil AP-X and Filtek Supreme. The specimens were randomly divided into two groups according to the curing unit used: Group I specimens (n = 15) were cured with a quartz-tungsten-halogen (QTH) light for 40 seconds, and Group II specimens (n = 15) were cured with a light-emitting diode (LED) unit in standard mode for 40 seconds. The specimens were incubated in 100% humidity at 37 degrees C for 24 hours. Then, the baseline color values (L*, a*, b*) of each specimen were measured with a spectrophotometer according to the CIELab color scale. After baseline color measurements, five randomly selected specimens from each group (Groups I and II) were immersed in one of two staining solutions (tea or coffee) or distilled water (control). After 1, 7 and 30 days of immersion, the color values of each specimen were remeasured and the color change value (deltaE*ab) calculated. Color changes caused by immersion in tea and coffee for 30 days were only perceptible in the Clearfil AP-X specimens cured with QTH or LED. In the Filtek Supreme specimens, coffee perceptibly stained the teeth after all immersion periods and tea stained after 30 days. Polymerization with QTH or LED did not cause any significant difference in the color stability of Clearfil AP-X or Filtek Supreme. While there were no significant differences between staining solutions in the Clearfil AP-X specimens cured with LED after one and seven days of storage and one day of storage in the QTH cured specimens, significant differences were observed between water and coffee after seven days of storage. In the Filtek Supreme specimens cured with QTH or LED, there were statistically significant differences between the staining solutions after one and seven days of storage. After 30 days of storage, no significant difference was found between tea and coffee in either resin composite cured with QTH or LED. The effect of the staining solutions (tea, coffee) on color changes in composites was immersion time and resin-material dependent.

Color Stability of Resin Composites after Immersion in Different Drinks

The purpose of this study was to evaluate the discoloration of two nanohybrids, two microhybrids, and a posterior composite resin restorative material upon exposure to different drinks--namely tea, cola, coffee, red wine, and water. The colors of all specimens before and after storage in the solutions were measured by a colorimeter based on CIE Lab system, and the color differences thereby calculated. Data were analyzed by two-way analysis of variance (ANOVA) and Tukey's HSD test. According to ANOVA, the restorative material, staining agent, and their interaction were found to play a statistically significant role (P = 0.0001) in color change. Among the staining agents, water consistently showed the lowest deltaE* value for all materials, whereas red wine showed the highest deltaE* value. In other words, for all the materials tested, their color change in staining agents ranked in this increasing order: water < cola < tea < coffee < red wine. In terms of comparison among the five restorative materials, Filtek P60 and Z250 were observed to manifest less color change than the nanohybrids and Quadrant LC.