Change In Electrical Resistance Research Articles

Fractal Circuit Architectures for Spatially Controlled Heating and Multi-Modal Shape Programming of Electro-Active Shape Memory Polymers

Shape memory polymers (SMPs) are commonly activated through external heating or rigid embedded heaters, which lack precise temperature control and restrict programmable shape transformations. This study demonstrates integrating thin films of hard electronic materials patterned in fractal designs into SMPs yields novel thermomechanical responses, enabling flexible implementation of stretchable electronic functionality. Space-filling Hilbert, Moore and Peano fractal curves generate distributed electronic circuitry patterns within the SMP matrices. To investigate the coupled electro-thermal-mechanical behavior, a multi-physics modeling approach is adopted. A nonlinear thermo-visco-hyperelastic constitutive model captures the SMP’s shape memory characteristics. Governing equations for the multi-physics problem are formulated. Experimental data validates the model’s predictions of the SMP’s nonlinear material response under uniaxial loading. This validated framework analyzes SMP composites with integrated fractal circuits. Findings reveal composites with higher-order fractal circuits’ exhibit faster, more uniform resistive heating and smaller electrical resistance changes during stretching, enabling consistent and predictable shape recovery under various deformations. Notably, these advantageous heating and resistance characteristics enhance the force recovery rate during the shape memory cycle. Furthermore, the composites demonstrate excellent shape recovery under bending. Remarkably, uniaxial stretching can induce controlled out-of-plane shape transformations, enabling novel actuation modalities. This work provides insights into leveraging fractal circuit integration to enhance SMP performance and expand capabilities, enabling multi-functional actuators, sensors and programmable soft grippers.

A damage model based on synchronous change of electrical resistance for solder materials–experimental and theoretical analysis

A damage model based on synchronous change of electrical resistance for solder materials–experimental and theoretical analysis

Supercritical CO2-Assisted Electroless Plating of Ultrahigh-Molecular-Weight Polyethylene Filaments for Weavable Device Application

This study reports on the use of supercritical CO2 (scCO2) for the metallization of ultrahigh-molecular-weight polyethylene (UHMW-PE) filaments, which are used as functional components in weavable devices. UHMW-PE is well known for its chemical and impact resistance, making it suitable for use in bulletproof clothing and shields. However, its chemical resistance poses a challenge for metallization. By utilizing scCO2 as the solvent in the catalyzation process, a uniform and defect-free layer of Ni-P is successfully deposited on the UHMW-PE filaments. The deposition rate of Ni-P is enhanced at higher temperatures during the scCO2 catalyzation. Importantly, the durability of the Ni-P-metalized UHMW-PE filaments is improved when the scCO2 catalyzation is carried out at 120 °C, as evidenced by minimal changes in electrical resistivity after a rolling test.

Improving durability and electrical performance of flexible printed e-textile conductors via domestic ironing

The electrical performance of printed conductors often degrades over time due to recurrent or infrequent exposure to practical stresses such as bending and washing. To avoid this, a repair mechanism is required to return the conductor to prime condition, enhancing lifetime and durability during extended stress cycles. In this study, domestic ironing is used to repair and restore the electrical resistance of printed conductors damaged by prolonged bending and washing cycles at standard ironing temperatures. The results of reliability tests on screen-printed conductors on two polyurethane-coated fabrics and six different laminate sheets adhered to the fabrics revealed that ironing significantly enhances the electrical performance of the conductors, limiting the change in electrical resistance to less than 20% after 400 000 bending cycles and to less than 1 Ω after 50 wash cycles. Although laminated conductors are more durable and generally outperformed conductors on the printed primer layer, in both cases, the results showed that the sample could be left for 24 h for ‘self-relaxation’ and would also return to the original value, implying that for future wear, either immediate ironing or leaving the garment for a period between uses could effectively ‘fix’ any bending or washing damage.

Advancing infrastructure resilience: A polymeric composite reinforcement grid with self-sensing and self-heating capabilities

In this study, a novel multifunctional grid-shaped polymeric composite (MGPC) with reinforcing, autonomous strain, stress, and damage sensing and localizing in addition to targeted heating capabilities, has been developed. Distinct from preceding composites, this grid synthesizes these features collectively for the first time and concurrently addresses current challenges in multifunctional composites, such as environmental impact, data reliability, complexity, and production costs. The fabrication process entails 3D printing an electrical circuit with conductive filaments within a polylactic acid (PLA) host polymer. The conductive filament was composed of a thermoplastic polymer (TPU) infused with carbon nanotubes (CNT)-grafted carbon fibres (CFs) produced via chemical vapour deposition. The mechanical, microstructural, and electrical properties of the grid elements and cementitious slabs reinforced with MGPC were comprehensively examined. The MGPC's performance in traffic flow monitoring, mechanical behaviour prediction, and damage localization was assessed through wheel tracking, asymmetric punch tests, piezoresistivity response evaluation, and digital image correlation techniques. Furthermore, the self-warming ability of the MGPC in cementitious composites was investigated using different voltages. The extruded TPU containing CNT-grafted CFs exhibited an electrical percolation threshold of approximately 5.0 wt%, resulting in a conductivity of around 70 S/m for the filaments. Incorporating MGPC as reinforcement within cementitious composite slabs led to notable enhancements, with flexural strength increasing by approximately 15 % and failure strain by up to 350 %. Wheel tracking tests revealed changes in the electrical: 5.8 % for 520 N and 7.8 % for 700 N wheel loads, with roughly 5.0 % average error in velocity detection. Transverse elements precisely detected wheel locations demonstrating the MGPC capabilities in accurately detecting wheel speed weight, and location. The study established strong correlations between electrical resistance changes, mechanical behaviour, and damage detection, affirming the MGPC's reliability and efficacy for damage monitoring and localization. The cementitious slab reinforced with MGPC reached around 52°C through a 20 V direct current, with a heating rate of 0.25°C/s and a power density of 142 W/m², showing its potential for practical applications such as self-healing and de-icing. However, design parameters such as mesh and conductive circuit configuration, long-term performance, as well as Life Cycle Assessment need further investigation.

Sensing mechanisms of nanomodified Portland cement composites

Mortar sensors were fabricated as beams incorporating different amounts of carbon nanofibers (CNFs) synthesized in-situ on cement particles. Changes in electrical resistivity were measured and compared to recorded changes in compressive stress, temperature, and humidity. Sensing mechanisms and corresponding models were developed. The findings of the study indicate that the piezoresistive effect is influenced by the critical concentration of CNFs inside the composite matrix and the tunneling effect. In addition, water absorption and desorption, as well as the amount of chemically bound water played an important role in humidity sensing. Thermal fluctuation-induced tunneling conduction was dominant for the temperature sensitivity.

Conductive polymer composites-enable self-sensing twisted string actuators

Twisted string actuators (TSAs) are innovative linear soft actuators that can mimic natural muscle contraction. However, obtaining feedback on their stroke requires cumbersome external sensors that compromise their compliance. We addressed this by developing self-sensing strings using conductive polymer composites (CPCs). The CPC strings exhibit electrical resistance changes in response to strain, enabling stroke sensing by the strings themselves. We fabricated CPCs strings with varying concentrations of multi-walled carbon nanotubes (MWCNTs). Characterization revealed excellent conductivity, tensile strength exceeding 30 N, tunable strain sensitivity via MWCNTs concentration variation, as well as stable and repeatable strain-dependent resistance changes. Optimization via a high-strength core fiber enabled the CPCs strings to withstand over 6[Formula: see text]kg loading with enhanced stroke and minimal resistance variation. We achieved at least a 97.8% linear correlation between resistance change rate and contraction rate in twisting experiments. This research provides a self-contained stroke sensor compatible with high-load soft TSAs, overcoming limitations of external sensors. The simple yet effective sensing mechanism could spur adoption of TSA in robotics.

Piezoresistive and capacitive cement-based stress sensors designed by incorporating carbon nanotubes doped with graphene nanopowder for structural health monitoring

Piezoresistive and capacitive cement-based smart composites are promising candidates for stress monitoring applications in buildings. However, the drawbacks of designing cement-based smart composites with a piezoresistive mechanism sensitive to temperature variations or a capacitive mechanism sensitive to vibration can be solved with sensor designs based on two principles. To address this issue, cement-based smart composites with piezoresistive and capacitive stress sensitivity and significantly improved compressive strength were designed using carbon nanotubes (CNT) doped with graphene nanopowder. A maximum fractional change in electrical resistivity of 90.08% with a high linearity of 98% was obtained with a blend of 0.01 wt%, and the maximum fractional change in capacitance was 163.11% with a high linearity of 97% at 0.05 wt%. Cement-based smart composites have absolute piezoresistive stress sensitivities that vary from 1.38% MPa−1 to 4.16% MPa−1 and 2.54% MPa−1 to 2.57% MPa−1 for blended and impregnated low doses of 0.01 wt% to 0.05 wt% CNT doped with graphene. In addition, capacitive stress sensitivities of 22.74% MPa−1 and 5.1% MPa−1 were achieved by blending and impregnating 0.01 wt% CNT doped with graphene in cementitious composites. Furthermore, the conductive path, overlapping, and tunneling effect created by CNT doped with graphene in cementitious composites and the porous structure in the dielectric layer are responsible for the increased stress sensitivity.

Biodegradable polylactic acid emulsion ink based on carbon nanotubes and silver for printed pressure sensors

Investigating biodegradable and biocompatible materials for electronic applications can lead to tangible outcomes such as developing green-electronic devices and reducing the amount of e-waste. The proposed emulsion-based conducting ink formulation takes into consideration circular economy and green principles throughout the entire process, from the selection of materials to the production process. The ink is formulated using the biopolymer polylactic acid dissolved in a sustainable solvent mixed with water, along with conductive carbon nanotubes (CNTs) and silver flakes as fillers. Hybrid conductive fillers can lower the percolation threshold of the ink and the production costs, while maintaining excellent electrical properties. The coating formed after the deposition of the ink, undergoes isothermal treatment at different temperatures and durations to improve its adhesion and electrical properties. The coating’s performance was evaluated by creating an eight-finger interdigitated sensor using a Voltera PCB printer. The sensor demonstrates exceptional performance when exposed to various loading and unloading pressures within the 0.2–500.0 kPa range. The results show a consistent correlation between the change in electrical resistance and the stress caused by the applied load. The ink is biodegradable in marine environments, which helps avoiding its accumulation in the ecosystem over time.

Facile and eco-friendly room-temperature electrical-enhanced technology for conductive circuits electrohydrodynamic-printed directly on textiles with small usage of conductive fillers

Flexible printed circuits are crucial for efficiently manufacturing electronic textiles. To achieve high conductivity with small usage of conductive fillers and avoid fabric shrinkages caused by high-temperature curing, an eco-friendly and high-temperature-free technology combining UV curing and chemical sintering with electrohydrodynamic (EHD) printing was innovatively proposed. The process integrating sequence was systematically investigated, along with in-depth analysis on surface morphology, electrical performance and enhancement mechanism. Results show that pre-treating fabrics using chemical sintering agent before EHD printing leads to an approximately parabola-like change in electrical resistance, and the “holes” formed by polymer aggregation deteriorates the uniform morphology of printed conductor. In contrast, treating printed lines by optimized integrating process facilitates the uniform and sufficient 3D-sintered structure. Electrical resistance was remarkably reduced by 93 % and successfully lowered to 1.24 ± 0.32 Ω even with 20 wt% Ag. The variation in resistance remained within 20 % after 3000 bending cycles and within 42 % after 10 washing times, exhibiting outstanding flexibility and washability. Additionally, application of as-prepared conductive circuits in electronic textile devices is demonstrated through the performance of ultra-high-frequency radio frequency identification (UHF RFID) antenna. Significant electrical enhancement based on small usage of conductive fillers in this work provides an efficient and green approach towards high-performance flexible circuits and e-textiles.

Enhancing wearable humidity sensing with conductive PANi-Coated polyurethane nanofibers

This study presents a flexible nanofibrous humidity sensor for wearable applications and smart textiles. The methodology involved fabricating polyurethane (PU) nanofibers via electrospinning, followed by polyaniline (PANi) coating under varied synthesis conditions. Scanning electron microscopy (SEM) analysis revealed consistent diameter uniformity in the prepared PU nanofibers. Moreover, an increase in average nanofiber diameter (305 to 539 nm) was observed with rising polymer solution concentration (7% to 9%). Fourier-transform infrared spectroscopy (FT-IR) confirmed the physical presence of PANi on PU nanofiber surfaces without inducing structural changes. Additionally, the strength of PU nanofibrous samples, with or without PANi coating, increased proportionally with higher PANi and PU polymer concentrations. Electrical conductivity was measured using a four-point device, and surface resistance was assessed across varying humidity levels to study humidity’s impact on samples. Results exhibited a linear relationship between surface electrical resistance and relative humidity changes. Furthermore, the PU and PU/PANi nanofibers exhibit contact angles of 113° and 133°, respectively. The PANi-coated sample is more hydrophobic compared to the uncoated sample. In conclusion, these findings underscore the potential of the developed sensor as a responsive tool for monitoring humidity fluctuations in diverse applications.

Detecting DC Electrical Resistivity Changes in Seismic Active Areas: State-of-the-Art and Future Directions

In this paper, a critical review of the geoelectrical monitoring activities carried out in seismically active areas is presented and discussed. The electrical resistivity of rocks is one of the geophysical parameters of greatest interest in the study of possible seismic precursors, and it is strongly influenced by the presence of highly fractured zones with high permeability and fluid levels. The analysis in the present study was carried out on results obtained over the last 50 years in seismic zones in China, Japan, the USA and Russia. These past works made it possible to classify the different monitoring strategies, analyze the theoretical models for interpreting possible correlations between anomalies in resistivity signals and local seismicity, and identify the main scientific and technological gaps in the literature. In addition, great attention has been paid to some recent works on the study of the correlations between focal mechanisms and the shapes of anomalous patterns in resistivity time series. Finally, some future scenarios for the development of new activities in this field have been identified.

Effects of thermo-oxidative aging on progressive bending damages and electromechanical behaviors of carbon fiber/epoxy 3D woven composites

The effect of thermo-oxidative aging on mechanical properties is important to designing carbon fiber-reinforced composites serviced in long-term atmospheric environments. Here, we report the progressive bending damage behaviors of carbon fiber/epoxy 3D angle-interlock woven composites (3DAWCs) after thermo-oxidative aging. Three-point bending tests were conducted to characterize bending damage behaviors after different aging days. The electrical resistance change of 3DAWCs was also simultaneously measured with the two-probe method during three-point bending tests. Combining side image and digital image correlation (DIC) technology, we found that the bending strength and modulus deteriorated rapidly during thermo-oxidative aging. The strain distribution and progressive bending damage modes also changed significantly, i.e., a symmetrical strain distribution for the unaged specimens, while the existing interface cracks of the aged specimen changed this symmetry. The electrical resistance method (ERM) effectively identified the early-stage damages, and the first derivative of the rate of resistance change (FDC) revealed differences in the progressive damage modes of aged and unaged specimens.

Void geometry analysis and multifaceted characterisation of cementitious mortar reinforced with short carbon and glass fibres – A comparative study

This paper presents comprehensive experimental and numerical studies on void analysis, durability performance, electrical properties, and microstructural behaviour of fibre-reinforced cementitious composites (FRCC) with varying short carbon and glass fibre volume fractions. Durability and electrical properties are evaluated based on the hydrochloric acid effect, water absorption, drying shrinkage and electrical resistivity changes over time. The incorporation of CF and GF remarkably limits drying shrinkage, primarily attributed to the bridging and bonding effects of fibres within the matrix. The addition of 1.0 % carbon fibre significantly decreases the electrical resistivity and improves acid resistance performance. Furthermore, for the first time, the influence of fibre type and quantity on the formation of elongated and eccentric voids is investigated by using X-ray computed tomography (micro-CT). The results demonstrate that higher porosity leads to lower strength and durability performance, while a greater occurrence of elongated voids contributes to increased length change in shrinkage.

Annealing hardening of the pre-deformed Cu-56at.%Au alloy due to retardation of recrystallization by L1o-type ordering

The evolution of the microstructure, physical and mechanical properties of pre-deformed samples of the non-stoichiometric alloy Cu-56at.%Au in the process of the L1o-type atomic ordering was studied. The duration of annealing at 250 °C ranged from 1 h to 2 months. Changes in microhardness and electrical resistivity at various stages of the disorder→order transition were found out, the microstructure was examined using a transmission electron microscope, XRD-scans and tensile tests were performed. Based on the resistometric results and XRD-analysis, the dependence of the fraction of the ordered phase vs. the annealing time was plotted. Consecutive changes in structural states observed during long-term annealing were considered through the competition between the energy of the elastic stresses, the surface energy and the energy of the dislocation structure. An abnormal increase in the strength properties of the alloy during annealing was found: the yield strength and microhardness of the initially deformed samples significantly increase (at 15 % and 30 %, respectively), at the same time there is a drop in electrical resistivity and an increase in plasticity. An attempt was made to describe the observed phenomena considering mutual effect of ordering and recrystallization. Discovered annealing hardening was explained in terms of the suppression of recrystallization by ordering, which is confirmed by the preservation of a high density of inherited dislocations in an ordered matrix and low plasticity of the annealed samples. The retardation in the recrystallization rate with an increase in the preliminary deformation strain of the alloy was discovered.

Smart ultra-high-performance concrete under cyclic high compressive stress

The self-stress sensing response of smart ultra-high-performance concrete (S-UHPC) under high cyclic compressive stress was investigated at different temperatures between 15 °C and 35 °C as a basic study for understanding the effects of temperature on the self-stress sensing response of S-UHPC. The S-UHPC has maintained the quasi-linear relationship between stress and fractional change in electrical resistivity (FCR) even under cyclic stress. The stress-sensing coefficient (SSC) of S-UHPC almost linearly decreased from 0.2450 %/MPa to 0.1722%/MPa with increasing the temperature from 15 °C to 35 °C. The lower SSC at higher temperature is based on the decreased electrical resistivity (∆ρ) of S-UHPCs owing to more activated ion movements in S-UHPCs.

Predicting soil parameters in Maroua 1st, Cameroon, using correlations of geophysical and geotechnical data

This study aims to predict specific soil parameters based on quantitative and qualitative correlations between electrical and geotechnical data. A total of 21 geotechnical boreholes followed by sampling, 21 light dynamic penetrometer tests, and 76 vertical electrical sounding surveys were carried out in Maroua 1st. The electrical resistivity data of the soil layers were obtained through 1D and 2D inversions of the ERT surveys. The geotechnical data were obtained from field tests and laboratory experiments. The statistical analysis of the entire dataset indicates that most of the samples are clay formations, as demonstrated by the means of variables and low variance coefficients, enabling qualitative identification. The distribution analysis of the parameters confirms the complexity of the physical characteristics of soils and the measurement procedures for each parameter. The Spearman's rank correlation matrix indicates that these observations can be used to propose predictive models for free swelling, allowable stress, natural water content, and electrical resistivity. Correlations between free swelling (εg) and other variables are not significant, as the degree of significance is lower than the fixed limit, except for models εg - W (R2 = 0.94), εg - ρ (Ώ.m) (R2 = 0.803), and εg - σ adm (R2 = 0.757). Grouping variables in multiple linear regression enables the development of a mathematical model. The predicted values of εg from this model demonstrate good agreement with the measured values for a validity domain of 0–16 %. The soil's natural water content has a strong correlation (R2 = 0.80 and rs = – 0.87) with electrical resistivity, meaning that an increase in water content results in a decrease in electrical resistivity. The permissible stress σadm has a strong correlation (R2 = 0.89 and rs = 0.85) with electrical resistivity. This indicates that changes in soil electrical resistivity are associated with soil stiffness.

A new winding homogenization method based on thermal resistance concept

PurposeThe aim of this paper is to provide a simple yet accurate and efficient geometric method for thermal homogenization of impregnated and non-impregnated coil winding technologies based on the concept of thermal resistance.Design/methodology/approachFor regular windings, the periodic microscopic cell in the winding space is identified. Also, for irregular windings, the average microscopic cell of the winding is determined. An approximation is used to calculate the thermal resistance of the winding cell. Based on this approximation, the winding insulation is considered as a circular ring around the wire. Mathematical equations are obtained to calculate the equivalent thermal resistance of the cell. The equivalent thermal conductivity of the winding is calculated using equivalent thermal resistance of the cell. Winding thermal homogenization is completed by determining the equivalent thermal properties of the cell.FindingsThe thermal pattern of different windings is simulated and compared with the results of different homogenization methods. The results show that the proposed method is applicable for a wide range of windings in terms of winding scheme, packing factor and winding insulation. Also, the results show that the proposed method is more accurate than other winding homogenization methods in calculating the equivalent thermal conductivity of the winding.Research limitations/implicationsIn this paper, the change of electrical resistance of the winding with temperature and thermal contact between the sub-components are ignored. Also, liquid insulators, such as oils, and rectangular wires were not investigated. Research in these topics is considered as future work.Originality/valueUnlike other homogenization methods, the proposed method can be applied to non-impregnated and irregular windings. Also, compared to other homogenization methods, the proposed method has a simpler formulation that makes it easier to program and implement. All of these indicate the efficiency of the proposed method in the thermal analysis of the winding.

Electrical Resistivity Behavior of Saline Soil under Low-Temperature Conditions

Freeze-thaw cycling of frozen soils is known to be the cause of various engineering failures of infrastructure in cold regions. Researchers found that electrical resistivity methods outperform traditional ground surveying methods in frozen soils for their greater convenience and cost-effectiveness. However, detailed investigation into the relationship between the electrical resistivity of soil and a variety of soil properties is still needed. In this study, a series of laboratory experiments using the Wenner method were conducted to determine the relationship between soil electrical resistivity and soil geotechnical properties such as initial water content and pore fluid concentration under freeze-thaw conditions. Cylindrical soil samples undergo artificial freeze-thaw cycles to a temperature as low as −70°C, and electrical resistivity and temperature values are recorded simultaneously. Measurement results are summarized for curve fitting, and a statistical model showing relationship between electrical resistivity and temperature during freezing and thawing was given. Above freezing point, the log of electrical resistivity had a linear relationship with temperature. Below freezing point and above −15°C, the log of electrical resistivity had a square root relationship with temperature. Different trends in electrical resistivity change in extremely low-temperature regions (from −15°C to −70°C) are also discussed. In extremely low-temperature regions, the electrical resistivity of frozen soils did not monotonously increase with lower temperature, which may be because of increasing salt concentration in the unfrozen water phase. The findings of this study are expected to bring more insights to frozen soil structure, and assist in geophysical surveying in cold regions and construction methods utilizing ground freezing.

Characterization of a Deglaciated Sediment Chronosequence in the High Arctic Using Near‐Surface Geoelectrical Monitoring Methods

ABSTRACTAccelerated climate warming is causing significant reductions in the volume of Arctic glaciers, such that previously ice‐capped bare ground is uncovered, harboring soil development. Monitoring the thermal and hydrologic characteristics of soils, which strongly affect microbial activity, is important to understand the evolution of emerging terrestrial landscapes. We instrumented two sites on the forefield of a retreating Svalbard glacier, representing sediment ages of approximately 5 and 60 years since exposure. Our instrumentation included an ERT array complemented by adjacent point sensor measurements of subsurface temperature and water content. Sediments were sampled at each location and at two more additional sites (120 and 2000 years old) along a chronosequence aligned with the direction of glacial retreat. Analysis suggests older sediments have a lower bulk density and contain fewer large minerals, which we interpret to be indicative of sediment reworking over time. Two months of monitoring data recorded during summer 2021 indicate that the 60‐year‐old sediments are stratified showing more spatially consistent changes in electrical resistivity, whereas the younger sediments show a more irregular structure, with consequences on heat and moisture conductibility. Furthermore, our sensors reveal that young sediments have a higher moisture content, but a lower moisture content variability.