Change In Deformation Mechanism Research Articles

Strain Rate Sensitivity of Low‐Temperature Superplastic Heterogeneous Medium‐Mn Steel Fabricated by a Novel High‐Ratio Differential Speed Rolling

In the present article, insights into the high‐temperature deformation behavior of medium‐Mn steel (MMS), which is prepared via high‐ratio differential speed rolling (HRDSR), are provided. Moreover, through innovative bidirectional jump experiments, variations in the strain rate sensitivity index m under various conditions are obtained. In the research findings, it is indicated that an increase in strain rate (SR) leads to a hardening of the alloy. During high‐temperature deformation, the value of m decreases with the increase in SR, but the rate of decrease gradually slows down. Furthermore, the higher the temperature (T), the greater the impact of changes in SR on m. In addition, the change in deformation mechanism during deformation leads to microstructural changes, and under the main deformation mechanism of grain‐boundary sliding, m generally increases with strain. Interestingly, at a T of 760 °C, the material exhibits a strong texture with high orientation, resulting in larger m values and superior superplasticity (≈691%). This study not only enriches the research content of HRDSR but also has significant implications for the superplasticity research of MMS. Moreover, a reference is provided for the research of other superplastic materials.

Deformation and melt–rock interaction in the upper mantle: Insights from the layered structure of the Horoman peridotite, Japan

To obtain a better understanding of melt–rock interactions in the upper mantle, microstructural and petrological analyses were conducted on deformed mantle peridotites from the Horoman peridotite complex, Hokkaido, Japan. The Horoman peridotite complex is lithologically heterogeneous and contains various kinds of ultramafic and mafic rocks. We studied an outcrop of 3 × 70 m in size that contains layered spinel harzburgite, plagioclase lherzolite, and mafic rocks. The results indicate that reactive melts migrated preferentially along the foliation in the already deformed peridotite, and that these melt-rich zones became especially prone to further deformation. This inference is supported by (1) the parallelism of the boundaries of rock layers and foliation in the deformed peridotite, and the shape and crystallographic preferred orientations (SPOs and CPOs) of olivine in the peridotites; (2) the diffusive trends of magnesium and modal compositions of pargasite grains near the boundaries between peridotite and mafic layers; (3) variations in the NiO content of olivine crystals; (4) variations in olivine CPOs with orthorhombic (010)[100] slip system patterns and weak fiber-[010] patterns; and (5) the strong pargasite SPOs, the cuspate shapes of the pargasites, and the absence of intercrystallite deformation. The results, combined with previously reported P–T conditions for the Horoman peridotite complex, indicate that the deformed peridotites and mafic rocks with a layered structure represent temperatures of 1050–1150 °C and pressures of 0.7–1.5 GPa. Our results suggest that a decrease in pressure led to the transition from a melt-free to a melt-bearing system with a consequent change in the deformation mechanism, from dislocation creep in the melt-free system to diffusion creep in the melt-bearing system, with strain localization in the fine-grained melt-rich layers. The change in deformation mechanism is likely to have occurred in the uppermost mantle beneath a mid-ocean ridge, where strong rheological contrasts are controlled by spatial variations in the melt fraction.

Size-dependent mechanical responses of twinned Nanocrystalline HfNbZrTi refractory high-entropy alloy

Atomistic simulations are performed to study the size-dependent mechanical responses of HfNbZrTi refractory high-entropy alloy (RHEA) containing ultrafine grains and highly oriented twin boundaries (TBs). The strength and flow stress of nanocrystalline RHEA (NC-RHEA) under tensile loadings are explored versus decreasing grain size d. The transition from classical Hall-Petch (HP) strengthening to inverse HP softening at a critical grain size dc = 5.91 nm is attributed to the change of plastic deformation mechanisms from dislocation emission and phase transformation to grain boundary (GB) activities. Besides, the intragranular TBs considerably enhance the strength of nanotwinned RHEA (NT-RHEA); the enhancing effect reduces with decreasing twin thickness λ. As the volume fraction of GB increases with decreasing d, GB activities dominate the plasticity of NT-RHEA and cause comparable mechanical properties with NC-RHEA. Moreover, the influences of dislocation glide, phase transformation and twinning on the mechanical properties of RHEA are quantified and separately analyzed to further verify our simulation results. Findings of this study not only promote insights into the nanostructure-property relation of HfNbZrTi, but also shed the light on performance enhancement through nanostructural design.

Experimental investigations into 3D printed hybrid auxetic structures for load-bearing and energy absorption applications

Auxetic structures possess negative Poisson’s ratio due to their unique geometrical configuration. It also offers enhanced indentation resistance, superior energy absorption capacity, excellent impact resistance, higher compressive strength, and other exceptional mechanical properties. In this study, multiple hybrid auxetic structures of three novel geometries have been designed by considering different sets of geometric parameters to numerically investigate the mechanical behaviors of the structures. The energy absorption properties and Poisson’s ratio of the developed hybrid auxetic structures have been measured under quasi-static compressive and bending loads. The numerically optimized structures from each of the three different geometries have been fabricated of acrylonitrile butadiene styrene using fused deposition modeling. Additionally, the simulated results have been experimentally validated. The validation studies have shown close agreement of their performances with the simulated results. Finally, comparative analyses of energy absorption performances have also been performed to select the most suitable structure for impact-resistant applications. Moreover, it has been observed that structure-2 exhibits superior performance in terms of maximum load-bearing capacity of 3395 N. On the other hand, structure-3 has the maximum energy absorption capacity of 51902 N.mm which is 4.85% higher than structure-1 and structure-2. Similarly, three-point bending test results have revealed that structure-2 performs better in terms of energy absorption capacity (10864 N.mm). Besides this, the effects of loading direction on deformation patterns and mechanical responses of the structures have been observed due to the changes in deformation mechanism. The high-velocity (8 m.s−1) impact test results have also confirmed the suitability of structure-2 for crashworthiness applications. The comparative findings derived from this study contribute significantly in developing lightweight, energy-absorbent, and impact-resistant auxetic core-sandwiched structures for civil, defense, and automobile sectors.

Change in deformation mechanism to change TRIP to TWIP strengthening in the class of 304 austenitic stainless steel sheets by trapezoidal wavy-rolling process

ABSTRACT Strengthening of steels through twinning-induced plasticity (TWIP) has several advantages like high-strength and high-ductility combination over the transformation-induced plasticity (TRIP) mechanism which gives high strength, low ductility and product phase of martensite in the single phase solid solution of austenitic matrix. But, development of TWIP effect will be more difficult unless the steel contains high stacking fault energy (SFE) (>20mJ/M2), fine grain structure and high manganese alloying (15–30 wt.%). These are very expensive processes and susceptible to metallurgical complexity in the austenitic stainless steels. Therefore, new processing technology was developed for strengthening of the austenitic stainless steel sheets by trapezoidal wavy rolling (TWR). Type 304 austenitic stainless steel was selected for this study which is known as martensite transformation, a dominant hardening mechanism due to low SFE and coarse grained structure. Wavy deformation-induced results have been studied through strain hardening behaviour by flow stress-strain curves and microstructural changes by atomic force microscope (AFM), and phase transformations by using X-ray diffractometer (XRD) analysis. It is found that this process introduced changes from TRIP to TWIP mechanism by forming plenty of mechanical twins and shear bands type structure at initial stage of deformations and partial martensite is observed in advanced stage.

Enhanced yield stress and reduced elastic modulus of metastable β Ti–Nb alloys deformed by equal channel angular pressing attributed to the Synergistic effect of deformation mechanisms

This work aims to obtain Ti–Nb alloys with a high yield stress, good plasticity, and low elastic modulus. To this end, metastable β Ti–Nb alloys were subjected to multipass equal channel angular pressing (ECAP) deformation at room temperature, and a thorough investigation of their microstructure evolution, deformation mechanisms, and strengthening/toughening mechanisms was conducted through X-ray diffraction, transmission electron microscopy, electron backscatter diffraction, and tensile tests. In the initial deformation stages, multiple deformation mechanisms are observed, including dislocation slip, {332} <113> twinning, stress-induced martensite (SIM) α″-phase, {112} <111> twinning, and stress-induced ω-phase. However, as the strain accumulates, the ω-phase disappears, the volume fraction of the SIM α″-phase gradually decreases, and the dominant deformation mechanism changes to dislocation slip and {332} <113> twinning. The ECAP deformation results in a complex-network microstructure and the precipitation of the nanoscale SIM α″-phase, which leads to the twinning-induced plasticity (TWIP) and transformation-induced plasticity (TRIP) effects. As a consequence, the Ti–Nb alloy simultaneously exhibits a high yield stress and a good plasticity. Furthermore, the high-density dislocations and interfaces generated by the ECAP deformation reduce the stability of the β-phase, and the introduced nanopores cause a decrease in density, resulting in a decrease in the elastic modulus of the alloy.

Plastic deformation delocalization at cryogenic temperatures in a nickel-based superalloy

A nickel-based superalloy is examined during monotonic deformation from ambient to cryogenic temperatures, reaching as low as liquid helium temperature. A detailed multimodal analysis of the microstructure and plasticity is conducted to discern changes in deformation mechanisms and plastic deformation localization under cryogenic conditions. This study employs high-resolution digital image correlation and transmission electron microscopy to identify the deformation mechanisms and understand their influence on plastic deformation localization as the temperature varies. At cryogenic temperatures, unusual plastic deformation localization processes are observed, attributed to the competing activation of a range of deformation processes. Furthermore, a mechanism of slip delocalization, i.e., local plastic deformation homogenization through closely spaced slip, is noted at these extreme temperatures. Ultimately, the impact of the microstructure is identified across the temperature range, from room to cryogenic temperatures.

Deformation mechanisms and fluid conditions of mélange shear zones associated with seamount subduction

Lithologic heterogeneity and the presence of fluids have been linked to seamount subduction and collocated with slow earthquakes. However, the deformation mechanisms and fluid conditions associated with seamount subduction remain poorly understood. The exhumed Chichibu accretionary complex on Amami-Oshima Island preserves mélange shear zones composed of mudstone-dominated mélange and basalt–limestone mélange deformed under sub-greenschist facies metamorphism. The mudstone-dominated mélange contains sandstone, siliceous mudstone, and basalt lenses in an illitic matrix. The basalt–limestone mélange contains micritic limestone and basalt lenses in a chloritic matrix derived from the mixing of limestone and basalt at the foot of a seamount. The basalt–limestone mélange overlies the mudstone-dominated mélange, possibly representing a submarine landslide from the seamount onto trench-fill terrigenous sediments. The asymmetric S–C fabrics in both mélanges show top-to-SE shear consistent with megathrust-related shear. Quartz-filled shear and extension veins in the mudstone-dominated mélange indicate brittle failure at near-lithostatic fluid pressure and low differential stress. Microstructural observations show that deformation in the mudstone-dominated mélange was accommodated by dislocation creep of quartz and combined quartz pressure solution with frictional sliding of illite, whereas the basalt-limestone mélange was accommodated by frictional sliding of chlorite and dislocation creep of coarse-grained calcite, with possible pressure solution creep and diffusion creep of fine-grained calcite. The mélange shear zones formed in association with seamount subduction record temporal changes in deformation mechanisms, fluid pressure, and stress state during megathrust shear with brittle failure under elevated fluid pressure, potentially linking tremor generation near subducting seamounts.

Microstructural evolution and cryogenic and ambient temperature deformation behavior of the near-α titanium alloy TA15 fabricated by laser powder bed fusion

Titanium alloys produced by additive manufacturing show excellent mechanical properties at room temperature. However, their deformation behavior at low temperature is still not fully understood. In this study, the microstructural evolution and tensile behavior of the near-α titanium alloy Ti-6.5Al-2Zr-Mo-V (TA15), fabricated via laser powder bed fusion (LPBF), were determined at both 25 °C and −196 °C. The LPBFed TA15 alloy shows the microstructure of α laths and acicular α′ martensite due to the rapid cooling rate during LPBF processing. Pyramidal <c+a> slip and numerous twins, including nano-twins and triple twins, were activated at cryogenic temperature, leading to the high ultimate tensile strength (UTS) up to 1750±8 MPa and yield strength (YS) up to 1548±25 MPa, which is higher than the strength at room temperature (YS∼1103 MPa, UTS∼1281 MPa). The dominant deformation mechanism changes from dislocation slip to twinning with decreasing temperature, leading to uniform deformation with an elongation of 5.2±0.1 %. The results can guide the control of the microstructure of LPBFed near-α titanium alloys at cryogenic temperature.

Grain size gradient effect on grain boundary mediated deformation of nano-grained metals

The extraordinary mechanical performance of gradient nano-grained (GNG) structures is characterized by the heterogeneity of dislocation-based and grain boundary (GB)-based plasticity, where the grain size gradient effect on these deformation mechanisms even fracture process still remains unclear. Herein, molecular dynamics simulation is conducted on the GNG α-Fe structures to investigate the grain size gradient effect on the GB-mediated hetero-deformation mechanisms. The plastic deformation mechanism changes from GB motion (grain coarsening and merging) to GB-dislocation interaction when the grain size distribution extends from the Hall-Petch softening region to the strengthening region. With increasing grain size gradient, the ultimate tensile stress and flow stress increase in the GB motion-controlled samples, and strain partitioning between hard and soft zones is found to increase in the dislocation-GB interaction- controlled samples from an atomistic perspective. The increased strain partitioning and its accommodation process further contribute to the fracture resistance enhancement, which is demonstrated by the uniform hetero-deformation between coarse and fine grains of the GNG structure, and further avoids localized plastic deformation.

The relationship between deformation mechanisms and mechanical properties in nanocrystalline Cu/Ag-bilayer alloy

The nanocrystalline metallic bilayer structure can effectively enhance the strength of Cu alloy while maintaining excellent electrical conductivity. Based on the microstructure evolution of Cu/Ag alloy observed by transmission electron microscope (TEM), molecular dynamics (MD) simulations of Cu/Ag alloy with nanocrystalline metallic bilayer structure were established. The mechanical properties and deformation mechanisms of nanocrystalline Cu/Ag-bilayer alloys were investigated at different temperatures. A mixed Hall-Petch (H-P) relationship was observed between the ultimate stress and the increased layer thickness. In this paper, the deformation mechanism changes from dislocation accumulation at the Cu-Ag interface to dislocation through the Cu-Ag interface. In addition, the data analysis results of elastic modulus showed an approximately linear decrease trend with increasing temperature, and the deformation mechanism shifted from dislocation motion to a combination of dislocation motion and grain boundaries (GBs) diffusion. These findings provide guidance for the design of high magnetic field facility (HMFF) water-cooled magnets and very large-scale integration (VLSI) lead frames.

Internal pressure testing of open-ended filament-wound cylinders using radial expansion of elastomeric inserts

A novel approach for generating internal pressure in filament-wound cylinders using the compressed elastomer method is investigated. Pressure is exerted on the inner surface of the cylinder by radially expanding elastomeric discs inside the composite cylindrical shell. This is accomplished by applying a uniaxial compressive load to the discs with the aid of rigs placed between compression platens in an ordinary universal testing machine. The digital image correlation (DIC) technique is employed to assist the tests in mapping both strain and displacement fields during the entire testing process. Cylinders with six different winding angles (±35°, ±45°, ±55°, ±65°, ±75°, and ±90°) are prepared and analysed. Their load-carrying capacity increases up to an angle of ±75°, accompanied by systematic changes in deformation and failure mechanisms. The suggested testing setup offers benefits in evaluating the impact of processing parameters on the internal pressure strength of filament-wound cylinders. It serves as a secure and cost-efficient laboratory-scale alternative to conventional hydrostatic pressure testing.

Strength vs temperature for refractory complex concentrated alloys (RCCAs): A critical comparison with refractory BCC elements and dilute alloys

To support the development of refractory complex, concentrated alloys (RCCAs), a clear understanding of the effect of temperature on strength is needed. Body-centered cubic (BCC) refractory metals and dilute refractory alloys show a strong temperature dependence of yield stress (σy) at low and high temperatures, with a relatively temperature-independent regime in between. RCCAs may introduce important changes in deformation and strengthening mechanisms, so it is not clear if RCCAs will show the same thermal dependencies. The objective of this work is to answer the question, “Is the temperature dependence of strength similar or different for RCCAs compared to BCC refractory elements and dilute refractory alloys ?” We evaluate σyvs. temperature for 61 RCCAs by analyzing data curated from the literature. We find that σy increases progressively from refractory BCC elements, to dilute alloys, to single- and multi-phase RCCAs. Single-phase RCCAs show the same three thermal regimes, but the stresses are higher and the intermediate plateau is shorter and is sometimes steeper. The thermal dependence of σy in multi-phase RCCAs shows more substantial differences. Six factors that contribute to the higher σy of RCCAs are discussed: (i) higher solute concentration; (ii) dispersion in atomic sizes; (iii) the shear modulus magnitude; (iv) the type of principal elements; (v) the solvus temperature of predicted secondary phases; and (vi) microstructure. Based on the present observations and analyses, suggestions for future research are made, especially regarding improved models for the effect of temperature on strength.

Effect of Ce on microstructure and dynamic compression properties of ZK60 alloy

The Mg–6Zn– xCe–0.6Zr ( x = 1, 2) alloys were subjected to a dynamic compression experiment, and the change in microstructure was noticed and studied. The primary components of two alloys are α-Mg matrix, Mg7Zn3 phase, and (Mg1− xZn x)11Ce phase. The two alloys have grain diameters of 2.8 and 3.2 μm, respectively. The dynamic compressive mechanical characteristics of the two alloys show a positive strain-strengthening effect, with Mg–6Zn–1Ce–0.6Zr alloy having somewhat higher values than Mg–6Zn–2Ce–0.6Zr alloy. At a strain rate of 500 s−1, {10[Formula: see text]2} tensile twin is the dominant deformation mechanism for two alloys, but the Mg–6Zn–2Ce–0.6Zr alloy is more prone to produce {10[Formula: see text]2} tensile twin. With the increase of the strain rate, the dominant deformation mechanism changes from {10[Formula: see text]2} tensile twin to pyramidal slip.

In-situ SEM micropillar compression and nanoindentation testing of SU-8 polymer up to 1000 s−1 strain rate

In situ micropillar compression and nanoindentation were performed on photolithographically fabricated SU-8 polymer inside a scanning electron microscope (SEM), covering seven orders of strain rates from 10-3 to 103 s−1. The extracted mechanical properties – modulus, hardness, yield strength, strain rate sensitivity (SRS) exponent – were systematically compared from both microscale tests and showed excellent agreement. No change in deformation mechanism was observed at high strain rates. We report a novel experimental protocol for high strain rate nanoindentation, comprising of input profile smoothing, that minimizes resonance amplitude during unloading and allows reliable extraction of modulus and hardness using standard Oliver-Pharr analysis. To the best of our knowledge, this is the first report of mechanical properties of SU-8 beyond 1 s−1 strain rate using nanoindentation based tests.

Calcite fabric development in calc-mylonite during progressive shallowing of a shear zone: An example from the South Tibetan Detachment system (Kali Gandaki valley, Central Himalaya)

Calcite-rich lithologies within the Annapurna Detachment zone, a strand of the South Tibetan Detachment System in central Himalaya (Kali Gandaki region, Western Nepal) have been characterized for the superimposition of microstructures to unravel deformation variations during syn-collisional exhumation. Finite-strain, grain size, twinning and crystallographic preferred orientations have been combined to define the contribution of dynamic recrystallization and twinning in calcite in the overall deformation. Dynamic recrystallization and twinning occurred respectively at temperatures of c. 400–550 °C and <250 °C. The comparison of calcite-based paleopiezometers indicates that cooling occurred along with an increase in differential stress from c. 4–19 MPa up to c. 118–154 MPa at decreasing strain rates. Flow estimates with the subsimple shear (30–50% of simple shear) regime for both fabrics support a single progressive deformation where the plastic regime progressively changed. We interpret the changes in intracrystalline deformation mechanisms in calcite and their differences in differential stress records, deformation temperature, and strain rate as linked to the exhumation of the rocks induced by the detachment, from deeper to upper crustal levels. Results for the Annapurna Detachment zone have been compared with the literature database for the regional continuation along the Himalaya, the South Tibetan Detachment System, which is defined by a lower main shear zone and an upper brittle fault. Data comparison led us to link our early stage of ductile shearing to that elsewhere recorded in the main lower branch of the system. Conversely, data for the late shearing are not found for the main branch when affecting quartz-bearing rocks, as strain hardening resulted in an upward partitioning of the deformation and in the localization of a brittle fault. Therefore, this study highlights how variations in lithology in regional-scale shear zones influences the exhumation path and the overall architecture of shear zones.

Length-scale effect on the hardness of metallic/ceramic multilayered composites: A machine learning prediction

The length-scale effect on the hardness of Al/Si3N4 multilayered composites were investigated via combined experimental and machine learning approaches. It was found that the hardness decreases with increase of the individual layer thickness, in agreement with the classic Hall-Petch relation. However, the hardness decrease became moderate when the individual layer thickness was less than 80 nm. The individual critical layer thickness of metallic/ceramic multilayered composites for the change in deformation mechanism was obtained by machine learning methods. The prediction results indicated that the individual critical transition layer thickness was mainly determined by the metal layer, and the corresponding critical transition hardness was positively correlated with the elastic modulus of the ceramic layer. Importantly, it was confirmed that the hardness of other metallic/ceramic multilayered composite systems could be predicted by the machine learning approach, especially the optimized random forest regression (RFR) model.

A steady-state irradiation creep and thermal creep model for zirconium alloys

In this work, a mechanistic steady-state creep model is developed to characterize the macroscopic strain rate of metallic materials affected by irradiation flux, testing temperature and applied stress. Thereinto, the steady-state strain rate is obtained by considering the density evolution of mobile dislocations, which involve the mechanisms of dislocation multiplication, dynamic annihilation and time-dependent dislocation annihilation. In order to effectively analyze the irradiation creep behavior in the low and high stress region, main attentions are focused on the influence of dislocation mobility on the process of time-dependent dislocation annihilation. At low stress, dislocation mobility is affected by dislocation climb and thermally activated glide. For the former, the absorption of irradiation-induced point defects can promote dislocation climb; whereas, thermally activated dislocation glide might be inhibited by the existing defect clusters. At high stress, the dominant deformation mechanism changes from dislocation climb to displacement cascade unpinning. For the latter, an explicit formula for dislocation mobility is deduced to address the influence of dislocation unpinning from the barriers on irradiation creep. To further verify the established model, thermal creep and irradiation creep data of zirconium alloys are considered to compare with the theoretical results. A good agreement is achieved over a wide range of temperature and stress indicating that the model can well describe the deformation behavior of steady-state creep. In addition, contribution of the dominant dislocation mobility components and dislocation density evolution components is compared under both thermal and irradiation creep, which can facilitate the comprehension of fundamental creep mechanisms of metallic materials.

Hydration State and Rheologic Stratification of the Lithospheric Mantle Beneath the North Anatolian Fault, Turkey

AbstractWe present constraints on the hydration state and rheology of the lithospheric mantle beneath the North Anatolian fault zone (NAFZ). Peridotite xenoliths from the Biyikali and Çorlu volcanic centers record deformational microstructures consistent with shearing in a lithosphere‐scale transcurrent fault system. Analysis by Fourier transform infrared spectroscopy indicates that nominally anhydrous phases retain some OH−, but bulk rock concentrations are generally restricted to &lt;50 ppm H2O by weight. From the rock microstructure, we determined differential stress magnitude and active deformation mechanism(s); combined with estimates of hydration state, we constrained the rheology. Recrystallized grain size piezometry shows that the mantle beneath the NAFZ sustained differential stresses of 10–20 MPa, largely independent of depth. The dominant deformation mechanism(s) change with depth; xenoliths extracted from shallower depths record evidence for grain size‐sensitive creep possibly in the presence of melt. At intermediate depths, both dislocation creep and grain size‐sensitive mechanisms were active, and we did not observe evidence for deformation in the presence of melt. The deepest samples were dominated by dislocation creep. The strong temperature sensitivity of creep mechanisms, combined with the low variability in differential stress, contributes to a stratified viscosity profile ranging from 1018 Pa s for the deepest samples to &gt;1022 Pa s at shallower depths (assuming a melt‐free rheology). Although difficult to quantify from the rock record, melt likely reduced the viscosity of the shallow lithospheric mantle. Vertical stratification in viscosity beneath the NAFZ, the result of melt‐present deformation and/or transitions in the dominant deformation mechanism, has important consequences for the seismic cycle of strike‐slip fault systems.

Microstructural evolution and yield strength of a novel precipitate-strengthened Fe-based superalloy during thermal aging at 700 °C

Microstructures and compressive yield strength of a novel γ′-strengthened Fe-based superalloy with about 55 wt% iron are investigated after aging at 700 °C for various durations. We found that the γ′ particle always displays a spherical shape and its size increases only from 9 ± 1.6 to 51 ± 14.0 nm with increasing the aging time up to 10,000 h. Meanwhile, the distribution of carbides at grain boundaries is always discontinuously, and no topologically close-packed phases are visible in the alloy during aging. Compressive deformation tests disclose that the yield strength of the experimental alloy at 700 °C increases firstly and then decreases with particle size. Microstructural observations uncover that the predominant deformation mechanism changes from shearing of γ′ particles by weekly-coupled dislocations to shearing by strongly-coupled dislocations and then to Orowan looping with enlarging particle size at the beginning of plastic deformation. Based on these results, it is deemed that the evolution of microstructure and deformation mechanism with aging time leads to the changes in the yield strength during thermal aging.