Cement Content Research Articles

Incorporating Limestone Powder and Ground Granulated Blast Furnace Slag in Ultra-high Performance Concrete to Enhance Sustainability

Abstract While ultra-high performance concrete (UHPC) offers numerous advantages, it also presents specific challenges, primarily due to its high cost and excessive cement content, which can pose sustainability concerns. To address this challenge, this study aims to develop cost-effective and sustainable UHPC mixtures by incorporating ground granulated blast furnace slag (GGBFS) and limestone powder (LP) as partial replacements for portland cement. Eight fiber-reinforced UHPC mixtures were investigated, with a water-to-cementitious materials (w/cm) ratio of 0.15. In four of the UHPC mixtures, 25% of the cement was replaced with GGBFS, and further, LP was added as a mineral filler, partially substituting up to 20% of the cement. In the remaining four mixtures, cement was replaced with only LP up to 20% (without GGBFS). The 28-day compressive strength of the UHPC mixture with 25% GGBFS and 20% LP was 149 MPa, 3.50% lower than the mixture without GGBFS. Its 28-day flexural strength decreased by 30%. Increasing LP replacement reduced drying and autogenous shrinkage, with a 29% shrinkage reduction at 20% LP replacement. Moreover, UHPC mixtures with GGBFS exhibited lower shrinkage compared to those without GGBFS for all LP replacements up to 20%. For evaluating the sustainability of UHPC mixtures, the cement composition index (CCI) and clinker to cement ratio (CCR) were determined. For 20% LP replacement with 25% GGBFS, CCI was 3.6 and the CCR was 0.5, 38% decrease from the global clinker to cement ratio. Overall, 20% LP replacement UHPC mixtures with and without GGBFS can produce UHPC class performance and reduce the environmental impact.

Assessment of the self-healing capacity of PVA fiber-reinforced composites by chloride permeability and stiffness recovery

This paper investigates the intrinsic ability of PVA fiber-reinforced cementitious composites to re-establish the durability properties of the uncracked state. Comparative chloride penetration tests are used as a direct measure to quantify the effect of self-healing on the chloride penetration resistance after cracking. Two different composites with cement to fly ash ratios of 1:1.5 and 1:2.0 were studied under the influence of healing periods of up to 28 days. After inducing cracks between 100 and 120 μm, samples were exposed to chlorides for 72 h and the resulting chloride penetration depth was compared to the unhealed state. Based on this procedure, a durability recovery index was proposed to quantify the material’s ability to re-establish its function as a protective layer after cracking. Results show that after 14 days of self-healing, chloride penetration through cracks was reduced between 81% and 99%. An extended healing period of 28 days leads to further reduction of the penetration depth to 84%–100%, indicating that most of the reaction takes place within the first 14 days of healing. While the stiffness recovery analysis showed that increasing cement content by 20% correlated with the formation of stronger healing products, no significant difference was found regarding crack closure.

Machine learning prediction of the unconfined compressive strength of controlled low strength material using fly ash and pond ash.

The sustainable use of industrial byproducts in civil engineering is a global priority, especially in reducing the environmental impact of waste materials. Among these, coal ash from thermal power plants poses a significant challenge due to its high production volume and potential for environmental pollution. This study explores the use of controlled low-strength material (CLSM), a flowable fill made from coal ash, cement, aggregates, water, and admixtures, as a solution for large-scale coal ash utilization. CLSM is suitable for both structural and geotechnical applications, balancing waste management with resource conservation. This research focuses on two key CLSM properties: flowability and unconfined compressive strength (UCS) at 28days. Traditional testing methods are resource-intensive, and empirical models often fail to accurately predict UCS due to complex nonlinear relationships among variables. To address these limitations, four machine learning models-minimax probability machine regression (MPMR), multivariate adaptive regression splines (MARS), the group method of data handling (GMDH), and functional networks (FN) were employed to predict UCS. The MARS model performed best, achieving R2 values of 0.9642 in training and 0.9439 in testing, with the lowest comprehensive measure (COM) value of 1.296. Sensitivity analysis revealed that cement content was the most significant factor with obtaining R = 0.88, followed by water (R = 0.82), flowability (R = 0.79), pond ash (R = 0.78), curing period (R = 0.73), and fine content (R = 0.68), with fly ash (R = 0.55) having the least impact. These machine learning models provide superior accuracy compared to traditional methods, particularly in handling complex interactions between mix components. The proposed models offer a practical approach for predicting CLSM performance, supporting sustainable construction practices and the efficient use of industrial byproducts. The novelty of this study lies in the development of precise design equations for evaluating UCS, promoting both practical applicability and environmental sustainability.

Experimental Study On Self-Compacting Concrete Mix Design By Using Yucca Zeolite

This report aims to present the experimental investigation on mix proportioning of normal concrete and self-compacting concrete with yucca zeolite. The study area comprises of ordinary portland cement of grade 53,mix proportioning of normal concrete for grade of concrete M40, M30 and M20 whereas mix proportioning for self-compacting concrete for grade of concrete M40, M30 ,M20.The parameters considered are cement content, Water cement ratio i.e. for normal concrete 0.4, 0.42, 0.45 and for self-compacting concrete 0.62, 0.44, 0.43 respectively. To reduce the risk of shrinkage, frost attack and corrosion of concrete, yucca zeolite as a mineral admixture and to increase the bond strength techno plast S 300 as a super plasticizer is added. The responses of material testing, normal concrete tests that includes slump flow test and compressive strength test recorded. Also, tests on self-compacting concrete recorded from slump flow test, J ring test, V funnel test, L box test, U box test, Rheological parameters, Compressive strength at 7 and 28 days. The various properties of SCC are ascertained with the IS code 1199:2018 [part 6] IS code 456:2000, IS code 10262:2019.

Role of zeolite and palm fiber in modifying the strength of cement-treated soil.

This paper aimed to research the role of zeolite and palm fiber in changing strength of cement-treated soil. The unconfined compressive strength (UCS) testwas mainly used to study the changes of strength of cement-treated soil by varied content of cement, zeolite, palm fiber under different curing period. The optimum substitution rate of zeolite for cement was researched for the purpose of increasing of strength of cement-treated soil and low carbon and environment protection, while the optimum content of palm fiber was explored for improving of strength and ductility of cement-treated soil by means of analytic software. Finally, the multiple regression technology was used to try to capture the relationship between strength of cement-treated soil and content of zeolite and palm fiber. The results show that the cement, zeolite, palm fiber and curing age have strong effect on the UCS of cement-treated soil.

Preparation and properties of phosphogypsum-based calcined coal gangue composite cementitious materials

Phosphogypsum (PG) and coal gangue (CG), as the largest solid waste today, the effective utilization of this part of the resource can help to alleviate environmental pollution and resource waste. The aim of this study was to utilize the excellent thermal insulation properties of original PG and the regulation of hydration products by calcined coal gangue (CCG) to produce phosphogypsum-based calcined coal gangue composite cementitious materials (PBCM). The optimal ratio of PBCM was studied through a combination of mechanical properties and thermal insulation properties. Finally, the effect of the foam factor is further investigated. The results show that: CCG can be used as a silicon-rich material with gelling properties to regulate the hydration products generated. The test block with a foam content of 8% has the best performance, with a compressive strength of 2.53MPa and a thermal conductivity of 0.1427W/(m·K). The optimal experimental scheme obtained from the orthogonal test was as follows: The optimal experimental design obtained from orthogonal experiments was as follows: PG, quicklime (QL), sulfoaluminate cement (SAC) and foam contents were 45%, 8%, 8% and 8%, respectively. The CCG: cement and water-solid ratios (W/S) were 3:7 and 0.275, respectively. The development of high-performance composites presented in this study is conducive to enhancing waste utilization and provides a novel approach as well as a theoretical foundation for insulating building materials in practical engineering applications.

Enhancement behaviours of carbon nanotubes reinforced cement based grouting materials under dynamic loading

Carbon nanotubes (CNTs) reinforced cement based grouting material is an important part of green manufacturing industry. Our previous research showed that this material can effectively enhance the impact resistance of rock matrix. In this study, We conducted a comprehensive study and quantitative analysis of the changes in pore structure of this material under impact conditions. Dynamic impact testing and computed tomography (CT) revealed that CNTs significantly increased the cement content in the sample by 79.11%. The CNTs group exhibited higher internal pore density and uniformity, effectively suppressing the formation of dynamic cracks in the sample. Compared to Non-carbon nanotubes (Non-CNTs) cement-based materials, the peak dynamic stress of the CNTs group increased by 4.76% to 21.54%, while the porosity decreased by 57.26%.This study further refined the enhancement behaviors of carbon nanotubes reinforced cement based, and making outstanding contributions to engineering practice.

Short-term mechanical properties and microstructure of coastal cement soil modified by sugarcane bagasse ash

Sugarcane bagasse ash is a kind of agricultural waste with a large quantity and good volcanic ash reactivity, it is necessary to find a way to reasonably utilize it to prevent environmental pollution caused by long-term accumulation. In this paper, the effect of sugarcane bagasse ash on the short-term mechanical properties of coastal cement soil were studied, and unconfined compressive tests and triaxial shear tests were carried out. The sugarcane bagasse ash content was set to 0 %, 1 %, 2 %, 3 %, 4 % and 5 %, respectively, the cement content was set to 5 %, and the curing age was set at 7d. The test results show that sugarcane bagasse ash can effectively improve the unconfined compressive strength and triaxial shear strength of cement soil, exhibiting a trend of increasing first and then decreasing with the increase of its content. When the sugarcane bagasse ash content is 1 %, the unconfined compressive strength reaches the maximum value of 2040 kPa, which is 56 % and 8 % higher than that of cement soil with 5 % and 7 % cement content, respectively. Compared with cement soil with 5 % cement content, the triaxial shear strength increases by 12 %∼17 %, the internal friction angle φ and cohesion c increases by 3 %∼8 % and 2 %∼11 %, respectively. The SEM test results show that the addition of bagasse ash can promote the hydration of cement to produce hydrated calcium silicate and other hydration products, fill the internal pores of the sample, and make the microstructure of the modified cement soil tend to be dense. The research results provide a reference for the application of sugarcane bagasse ash modified cement soil in practical engineering.

Improvement of vibration response of a foundation resting on Salt-Encrusted Flat Soil by cement addition: a numerical investigation

ABSTRACT Excessive vibrations can negatively impact machinery performance by causing misalignment, decreased accuracy, increased wear and tear, and reduced overall operational efficiency. By conducting a numerical investigation on improving vibration response through cement addition to salt-encrusted flat soil, the study aims to enhance the performance and reliability of machine foundations, thereby optimizing machinery operation. The properties of untreated sabkha and cement-sabkha were calibrated to use in the Finite Element Method (FEM) model. The variables investigated have the thickness of cemented sabkha ratio, operation frequency, three types of subsoils (Sabkha and cemented sabkha of 5% and 10%), and vertical amplitude loading. The main findings revealed that the maximum shear modulus (Gmax) increases by 47% with a 5% to 10% increase in cement content. In addition, as the vibration’s frequency increases, the amplitude displacement is observed because the reflected waves become smaller for the foundation resting on cemented sabkha. The natural frequency rises as the thickness ratio and cement amount of cemented sabkha increase. The influence of the thickness ratio on displacement amplitude is considerable when the operation frequency is less than 20 hz. The study implies that engineers can optimize the design of machine foundations to achieve better performance and stability.

Research on the Mechanical Properties of Composite Grouting Materials Based on Ordinary Portland–Sulphoaluminate Cement

This study aimed to enhance the mechanical properties of calcium sulfoaluminate cement grouting materials (HCSA) by investigating the effects of ordinary Portland cement (OPC) content, the ratio of quicklime to gypsum, and the dosage of sodium aluminate on the compressive strength of the OPC-CSA composite system. The results indicate that as the OPC content increases, the compressive strength of the blended cement initially increases and then decreases, reaching a maximum at a 60% OPC replacement ratio within the experimental group. The addition of an appropriate amount of OPC to the CSA composite system effectively prevents the regression of compressive strength. With an increase in quicklime content, the compressive strength of the samples at various ages first increases and then decreases, with the optimal ratio of quicklime to gypsum found to be 2:8. Furthermore, sodium aluminate, used as an activator, when increased in dosage, leads to an initial increase followed by a decrease in the compressive strength of OPC-CSA samples, with an optimal incorporation rate of 0.75%, significantly enhancing the strength of the blended cement. In the orthogonal experiments, the dosage of sodium aluminate was identified as the most influential factor affecting the compressive strength of the composite grouting materials.

Indirect estimation of compressive strength of cement-stabilized mine tailings by using ultrasonic pulse velocity for road construction

This study proposes a correlation formula between the compressive strength, ultrasonic pulse velocity UPV, and dynamic elastic modulus of cement-stabilized mine tailings CSMT. Samples were tested in curing times (1, 7, 14, 28, and 90 days) by cement amounts (2%, 4%, 6%). The findings demonstrated that the strength and wave velocities of CSMT were enhanced due to increased cement content and extended curing periods. A regression equation with a high coefficient of determination (R-square >0.95) was developed to establish a relationship between compressive strength and ultrasonic pulse velocity UPV for tailings containing 6% cement content in both treated types. The study uncovered a strong relationship between pulse velocity and compressive strength in different CSMT mixtures. These findings indicate that UPV tests can accurately, rapidly, and without causing damage, and evaluate the compressive strength of CSMT for road paving. The results improve the advancement of environmentally friendly building materials and showcase the efficacy of non-destructive ultrasonic testing in assessing structural characteristics. The investigation has profound consequences in enhancing the quality and management of road construction industry, and the management of mining waste.

Self-compacting concrete using molybdenum mineral tailings: materials and mechanical property

Recycling mineral tailings poses significant challenges, but one effective solution is their incorporation into self-compacting concrete (SCC) mixtures. This research explores the material and mechanical properties of SCC by integrating mineral tailings at three different ratios: 10%, 20%, and 30%. The primary aim is to determine the optimal replacement ratio that preserves key characteristics such as flowability and viscosity. To assess the material properties of fresh SCC, we conduct various tests, including rheological, V-funnel, U-box, and air content tests. These evaluations focus on how the addition of mineral tailings at different levels impacts flowability and viscosity. In terms of mechanical performance, we analyze compressive strength relative to the increasing proportion of mineral tailings. The results indicate that higher proportions of mineral tailings negatively affect flowability and viscosity. As a result, the optimal replacement ratio for mineral tailings is identified as up to 20% of the total cement content. These findings suggest that mineral tailings can effectively replace conventional cement, making them a promising option for producing environmentally friendly self-compacting concrete.

Low-dose cement stabilized large particle size graded crushed stone: Laboratory and field investigations

Compared with traditional graded crushed stone (GCS), the maximum aggregate size of large particle size GCS (LPS-GCS) is larger and the content of large-size aggregates is more, which can form an interlocking skeletal structure with a stronger bearing capacity. Nevertheless, LPS-GCS occasionally exhibits unstable performance, and one effective way to enhance LPS-GCS's mechanical and physical properties is to stabilize it with low-dose cement. In this study, four cement contents (1.5 %, 2.0 %, 2.5 %, and 3.0 %, by mass) were selected to form low-dose cement stabilized LPS-GCS (LCS-LPS-GCS) mixtures with a maximum aggregate particle size of 53 mm. Unconfined compressive strength (UCS) and compressive resilient modulus (CRM) tests were performed on LCS-LPS-GCS samples for different cement contents and curing times. Moreover, prediction models and correlations for the UCS and CRM at different curing times were established. Furthermore, a test road was used to evaluate the LCS-LPS-GCS's field compaction level and deflection. Laboratory test results indicated that while the California bearing ratio was significantly higher than that of conventional GCS, the maximum dry density of LPS-GCS designed in this study was close to that of conventional GCS. With the same cement content, LCS-LPS-GCS outperformed conventional GCS in terms of UCS and CRM. Based on the variation law of the mechanical properties, the ideal cement content should be around 2.5 %. There was a strong positive correlation between UCS and CRM scores from LCS-LPS-GCS. The UCS and CRM were appropriate to be predicted by exponential and growth functions models, respectively. The field investigations indicated that asphalt pavements reconstructed with LCS-LPS-GCS had high compaction and low deflection, resulting in better bearing capacity and durability. The results of this investigation can serve as a reference for the design and application of LCS-LPS-GCS base for long-lasting and resilient pavements.

Research on the factors affecting the compressive strength of rubber powder modified cement-stabilized crushed stone based on orthogonal experiments

Based on an orthogonal experimental design, this study introduces rubber powder particle size alongside rubber powder content, aggregate gradation, and cement content as factors. A total of 16 mix proportions were formulated. For each mixture, compaction tests and unconfined compressive strength (UCS) tests were conducted. Using Statistical Product and Service Solutions (SPSS) software, a multifactor variance analysis was performed to determine the influence levels of the four factors on maximum dry density and compressive strength. The optimal mix proportion was selected based on compressive strength. The results indicate that aggregate gradation and rubber powder content significantly affect the maximum dry density of the mixture, with aggregate gradation having the greatest impact. Rubber powder content has the most substantial effect on compressive strength, while rubber particle size has the least influence. The optimal formulation is 7% cement content, 30-mesh rubber powder, 0.5% rubber powder content, and a skeletal dense gradation close to the median.

Predictive modeling of compressive strength in silica fume‐modified self‐compacted concrete: A soft computing approach

AbstractSelf‐compacting concrete (SCC) is a specialized type of concrete that features excellent fresh properties, enabling it to flow uniformly and compact under its weight without vibration. SCC has been one of the most significant advancements in concrete technology over the past two decades. In efforts to reduce the environmental impact of cement production, a major source of CO2 emissions, silica fume (SF) is often used as a partial replacement for cement. SF‐modified SCC has become a common choice in construction. This study explores the effectiveness of soft computing models in predicting the compressive strength (CS) of SCC modified with varying amounts of silica fume. To achieve this, a comprehensive database was compiled from previous experimental studies, containing 240 data points related to CS. The compressive strength values in the database range from 21.1 to 106.6 MPa. The database includes seven independent variables: cement content (359.0–600.0 kg/m3), water‐to‐binder ratio (0.22–0.51), silica fume content (0.0–150.0 kg/m3), fine aggregate content (680.0–1166.0 kg/m3), coarse aggregate content (595.0–1000.0 kg/m3), superplasticizer content (1.5–15.0 kg/m3), and curing time (1–180 days). Four predictive models were developed based on this database: linear regression (LR), multi‐linear regression (MLR), full‐quadratic (FQ), and M5P‐tree models. The data were split, with two‐thirds used for training (160 data points) and one‐third for testing (80 data points). The performance of each model was evaluated using various statistical metrics, including the coefficient of determination (R2), root mean square error (RMSE), mean absolute error (MAE), objective value (OBJ), scatter index (SI), and a‐20 index. The results revealed that the M5P‐tree model was the most accurate and reliable in predicting the compressive strength of SF‐based SCC across a wide range of strength values. Additionally, sensitivity analysis indicated that curing time had the most significant impact on the mixture's properties.

Effect of Grain Size and Porosity/Binder Index on the Unconfined Compressive Strength, Stiffness and Microstructure of Cemented Colombian Sands.

Artificial cementation of granular soils results in improved stabilization, increased stiffness, and greater mechanical strength. The porosity index and volumetric cement content η/Civa is presented as a key measure to study the evolution of different soil stabilization types. However, this index had not been previously studied or adjusted for sands in Colombia. Therefore, this study evaluates the applicability of the η/Civa index on unconfined compressive strength (qu) and stiffness (Go), complemented by microstructural analysis, in four sandy soils from Luruaco (Atlántico), Lorica (Córdoba), Medellín (Antioquia), and Bogotá D.C. The soils were stabilized with Type III Portland cement in dosages of 3%, 5%, 7%, and 9%, and subjected to UCS, ultrasound, and SEM-EDS tests after a curing period of 7 days. It was found that increasing cement content results in higher qu values for the samples, and higher molding density also leads to higher qu values. Additionally, the grain size distribution influenced the adjustment of parameter "a". In the sands from Bogotá and Lorica, with high uniformity, the value of "a" was 1.00. In contrast, mineralogy and particle shape played a predominant role in the sands from Medellín and Luruaco, where the coefficient of uniformity is higher, suggesting a possible inverse relationship between particle angularity and the value of "a".

Research on the Preparation of Dry Mixed Mortar Using Waste Incineration Fly Ash

This study investigated the effect of water-washed municipal solid waste incineration fly ash (MSWI FA) as an admixture on the performance of dry mixed mortar and used X-ray diffraction (XRD) and scanning electron microscope (SEM) detection methods to conduct microscopic analysis. The experiment investigated the effects of the amount and water content of washed municipal solid waste incineration fly ash, cement, additives, sand and gravel, and curing time on the compressive flexural strength of dry mixed mortar at 28 days. The results show that when the content of water-washed MSWI FA is 9.80%, the content of sand and gravel is 73.50%, the content of ordinary Portland cement (PO42.5) is 16.66%, the content of water-reducing agent is 1.47‰, the content of cellulose is 0.03‰, the content of the expansion agent is 0.49‰, the addition of water is 130–160 mL/kg, the consistency of the sample can reach 91.8 mm, and the water retention rate can reach 93.6%. The flexural strength of the sample at 28 days can reach 7.5 MPa, and the compressive strength at 28 days can reach 28.30 MPa. Metal ions, such as Pb2+ and Gd2+ in MSWI FA, under the combined action of silicate cement in dry mixed mortar and fibers in cellulose, crisscross and form a solidified material, which will not be leached out. This quality meets the requirements of dry mixed mortar for ordinary plastering and masonry mortar (GB-T 25181-2019), and the leaching toxicity of the sample meets the “Identification Standard for Hazardous Waste” (GB5085.3-2007). This work provides a meaningful exploration of the resource utilization of water-washed MSWI FA.

Application of recycled concrete aggregates in continuous-graded cement stabilized macadam

This study investigates the potential of using recycled concrete aggregate (RCA) derived from construction and demolition waste as a replacement for natural aggregate in cement-stabilized macadam (CSM). Various substitution rates of RCA, ranging from 0 % to 100 %, were examined with a focus on mechanical properties and durability, including unconfined compressive strength (UCS), indirect tensile strength (ITS), compressive elastic modulus, drying shrinkage, frost resistance, scour resistance, and water damage resistance. Nanoindentation was used to analyze the interfacial transition zones (ITZs) within the CSM. The results show that with a fixed cement content, the UCS, ITS, and compressive elastic modulus decrease as the RCA content increases. Higher RCA content also leads to reduced drying shrinkage, frost resistance, scour resistance, and water damage resistance. Nanoindentation revealed that ITZ1 and ITZ2 have similar thicknesses (∼50 μm), while ITZ3 is about 80 μm thick, highlighting the intricate physical composition of ITZs, including pores, low-density C-S-H, high-density C-S-H, and Ca(OH)2. These findings provide critical insights for optimizing sustainable CSM design using RCA, thereby promoting environmental sustainability in road construction.

Sustainable and mechanical properties of Engineered Cementitious Composites with biochar: Integrating micro- and macro-mechanical insight

Engineered Cementitious Composites (ECC) are ductile, strain-hardening cementitious composites with a tightly controlled crack opening profile. A significant concern in the development and application of ECC is its high carbon emissions associated with high cement content consumption. As an emerging green additive, biochar can significantly cut down on the carbon emission of concrete products. However, research that integrates micro- and macro-mechanical insights with biochar incorporation is limited. In this study, micro-mechanical tools indicated that a certain amount of substitution biochar could enhance the tensile properties of ECC. The study assessed various properties including compressive strength, porosity, density, tensile performance, crack pattern, sustainability and cost of ECC with different biochar proportions. The findings showed that incorporating 10 %–20 % biochar effectively increased the tensile strain capacity and decreased the crack opening width in ECC materials. This improvement can be attributed to the introduction of finer biochar particles (≤75 μm) at the fiber/matrix interfacial transition zone, which alters the fiber-bridging force by reducing the chemical and frictional bond strength between the fiber and matrix, as revealed by micro-mechanical tests and microstructural inspection. Moreover, the utilization of biochar contributes to reducing the carbon emission of ECC, enhancing sustainability while maintaining a ∼10 % minimal reduction in compressive strength. Overall, this study introduces a novel approach for reusing low-carbon biomass waste in the production of building materials, offering potential advantages in micro- and macro-mechanical performance, cost-effectiveness, and environmental sustainability.

From loose sand to sandstone: An experimental approach on early calcite precipitation in sands of siliciclastic and mixed carbonate-siliciclastic composition.

Artificially cemented sandstones were produced to assess the impact of detrital texture and composition on the precipitation and distribution of early calcite cement, and cement-related degradation in porosity. To simulate early-calcite cementation, loose sediment of variable composition (siliciclastic and calcareous) and grain size was exposed to a calcite supersaturated solution for 35 to 58 days at 23°C. Identification and distribution of the newly precipitated crystals was performed with high resolution 2D optical and scanning electron microscopy. The experimental results show the precipitation of grain-coating, pore-bridging and pore-filling granular calcite cement with up to 100 μm crystal size. Despite a positive correlation between the amount of detrital carbonate grains and calcite crystals, calcite cement does not preferentially nucleate on bioclast surfaces, irrespectively of their favourable mineralogy. Siliciclastic grains show high calcite cement coverage with altered feldspar, particularly plagioclase, displaying coverage of 94.3%. Grain size variations within the sand packs have influence on the precipitation pattern of calcite with coarse-grained layers (500-710 μm) showing minor calcite cementation (6.3%), while medium- (250-500 μm) to fine-grained layers (125-250 μm) comprise average calcite cement contents of 16.3% and 28.2%, respectively. The findings of this study enhance our knowledge regarding the precipitation processes of calcite in porous material with heterogeneous reacting mineral phases, shapes and pore connectivity.