This research aims to study two gilded hollow bronze statues from pharaonic Egypt excavated in a karnak temple. The two objects had an unusual casting core and one of them was gelded on the ground. Various parts and layers, including the casting core, gold layer, gilding ground, corrosion products, and metallic structures, were characterized via scanning electron microscopy (SEM), polarized light microscopy (PLM), and USB digital microscopy. X-ray diffraction, Fourier transform infrared spectroscopy (FTIR), and SEM coupled with energy-dispersive spectroscopy (EDS) were employed for the analysis. The features related to manufacturing and gilding technologies of the two statues are presented. Specifically, the casting core consisted of an external lime layer on the clay-based internal core, contrarily to the typical casting cores in ancient Egypt and other ancient civilizations consisting of a clay-based mixture. The study proposed a specific method of hollow casting to obtain the casting core, reasonably adopted by the ancient Egyptians to replicate analogous hollow objects from a master mold, whereas the mold of usual hollow casting methods was destroyed after casting. Moreover, the gilding of one of the statues is a unique example of gilded bronze with ground calcite as filler material and beeswax as blinding medium. Finally, the chemistry and structure of the corrosion layers were characterized to gain insights into the morphology and corrosion mechanisms in the presence of calcite ground and gold layers.
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