Carbon Fiber Reinforced Polymer Laminates Research Articles

In situ analysis of three-dimensional microcrack propagation in cross-ply laminates using synchrotron radiation X-ray computed tomography

This study utilized synchrotron radiation X-ray computed tomography to investigate the initiation and propagation of microcracks in cross-ply carbon fiber-reinforced polymer (CFRP) laminates under mechanical loading. Initially, static tensile loads were applied to detect microcracks within a ply thickness of 160 μm. The crack propagation was subsequently characterized, extending across adjacent carbon fibers and along the interfaces of individual fibers into the material's interior. The experiment was repeated with cyclic loading, where the laminates were imaged periodically. Analysis of the images revealed the presence of microcracks and provided insights into their progression from the point of initiation. Notably, microcracks exhibited the initiation toward the interior of the material rather than across the neighboring carbon fibers, whereas their propagation is more significant across the adjacent carbon fibers particularly under the static loading. Under cyclic loading, however, the crack propagation toward the interior of the material was more pronounced, implying different propagation behavior than when under static loading. These findings were also validated through the distribution of energy release rate and stress triaxiality along the crack tip calculated by finite element analysis.

Effect of fiber orientation of adjacent plies on the mode I delamination fracture of carbon fiber reinforced polymer multidirectional laminates

AbstractThe extensive use of multidirectional composite laminates requires to understand the delamination behavior at interfaces between plies with different fiber orientations. In this study, double cantilever beam testing was performed to investigate the mode I interlaminar fracture of carbon fiber reinforced polymer laminates with different central interfaces (0//0, 0//+45 and +45//−45). X‐ray microtomography revealed the curved crack front shape that was incorporated to calculate fracture toughness. The fracture toughness varies with the crack length in a typical delamination resistance curve, which can be quantified by an empirical equation. Incorporation of variable fracture toughness into a cohesive zone model can better predict the delamination fracture of the laminate, compared to constant toughness. It was found that the delamination mechanism is independent of central interfaces. However, compared to unidirectional laminates, multidirectional laminates are less resistant to crack initiation, but more resistant to propagation with higher toughness and shorter fiber bridging zone.Highlights Mode I interlaminar fracture of CFRP laminates with different central interfaces was investigated experimentally and numerically. Curved crack front shape was incorporated to calculate fracture toughness. Incorporation of variable fracture toughness into a cohesive zone model can better predict the delamination fracture of the laminate. Multidirectional laminates are less resistant to crack initiation but more resistant to propagation with higher toughness and shorter fiber bridging zone.

Coupled thermal-electrical–mechanical characteristics of lightning damage in woven composite honeycomb sandwich structures

In this study, lightning strike damage of woven carbon fibre-reinforced polymer laminates (W-CFRPs) and woven composite honeycomb sandwich panels (W-CHSPs) are simulated using the proposed sequential thermal-electrical–mechanical finite element (FE) coupling model incorporating dielectric breakdown of materials. Surface current with an amplitude of 200 kA and corresponding lightning shockwave overpressure were applied on each composite. The FE model coupled with LaRC05 criterion was used to study the failure behaviours of intralaminar damage and interlaminar delamination of the W-CFRPs and W-CHSPs. A series of lightning strike tests were performed to validate the FE model. Detailed lightning damage assessments and mechanisms were characterized by a combination of visual inspection, image processing, ultrasonic scanning and micro computed tomography (Micro-CT) and showed good agreements with the FE-predicted results. It can be concluded that shockwave overpressure significantly impacts lightning-induced damages, thereby supporting the effectiveness of the newly proposed sequential thermal-electrical–mechanical coupling model, which demonstrates improved predictive accuracy.

Heat partition evaluation during dry drilling of thick CFRP laminates with polycrystalline diamond drills

Since various material properties of carbon fiber-reinforced polymer (CFRP) are temperature dependent, dry drilling of CFRP is a delicate process. Thermal damage can be caused by a rise in temperature during drilling due to a large portion of heat being transferred into the material. Heat partition is used to quantify this, which represents the percentage of total heat being dissipated into the constituent objects during a machining operation. Drill margin and contact conditions at the tool-workpiece interface significantly affect the drilling of CFRP material. Drilling experiments were performed to measure thrust force, torque, and temperatures for five different sets of feed rates and rotational speeds. This study proposes a method for calculating heat partition values during CFRP drilling by developing a finite element-based thermal model. The FE model employs a Gaussian distributed ring-type heat flux that is a function of the equivalent contact length at the interface between the drill and the material surface and the geometry of the workpiece which operates as a moving heat source, emulating the progress of the drill through the CFRP laminate. The tool implements heat fluxes that use characteristic time-point-based step functions to represent the temperature on the drill as it advances through the workpiece during machining. The temperature profiles obtained from the FE analysis and the experiments for the workpiece and tool were subsequently matched iteratively to determine the corresponding heat partition value.

Normalization and Processing of Rotational Eddy Current Scans for Layup Characterization of CFRP Laminates

ABSTRACT The verification of fiber orientation and layup in carbon fiber-reinforced polymer (CFRP) composite laminates is essential to guarantee the performance of the material. This work reports the background, methodology, and results of a rotational eddy current testing (ECT) system for determining fiber orientation and ply layup of unidirectional CFRP components. The system presented mechanically rotates a 15 MHz directional transmit-receive ECT probe, which poses several speed and consistency advantages. The paper presents a theoretical discussion of how these scans are produced, a unique preprocessing normalization method, and an optimization process for determining the layup from the captured datasets. Results show a high level of accuracy for identifying the unique directions present in a laminate, and the theory-supported model enables the extraction of layup order information of multilayer parts, even where repeated lamina are present within the laminate.

Monitoring of damage evolution in carbon fiber reinforced polymer composites by electrical impedance tomography

Electrical impedance tomography (EIT) has been widely investigated as a nondestructive testing method for carbon fiber reinforced polymer (CFRP) composites. However, the performance of EIT method on the damage process monitoring of the composites is lack of investigation. Herein, quasi-static indentation tests were utilized to introduce damage on CFRP laminates. The damage evolution process was monitored by EIT, while the potential of distinguishing the elastic deformation stage from the plastic stage was analyzed with the aid of acoustic emission. It was found that the changes in conductivity first appeared in the non-central region. With the accumulation of damage, the conductivity changes gradually extended to the center region. The reconstructed damage images were in the crossover shape, which was consist with the micro-CT results that showed the fracture of fibers in ±45° direction. This work further promotes the application of EIT in damage process monitoring of CFRP components.

An approximation method to determine the travel time in total focusing imaging of carbon fiber-reinforced laminates

Abstract It is critical to accurately determine the propagation time in testing objects for ultrasonic array imaging using the Total Focusing Method (TFM). However, it poses challenges for the calculation of wave propagation time in carbon fiber reinforced polymer (CFRP) laminates because of the material anisotropy and inhomogeneity. This paper introduces a novel approach for computing ultrasonic wave travel time to enhance the TFM image of CFRP laminates. This method, termed the layer-by-layer acoustic travel time approximation (L-L TravelTimeAppro), considers the anisotropy within each monolayer and the heterogeneity of CFRP. It approximates the propagation path as straight throughout the material and computes the wave propagation duration utilizing the group velocity in each ply. The application of this method to TFM imaging is referred to as TravelTimeAppro-TFM. Experiments were conducted in a specially designed CFRP laminate. Subsequently, TFM imaging was processed by using propagation time calculated by isotropic, Dijkstra, and L-L TravelTimeAppro methods, respectively. The results indicate that TravelTimeAppro-TFM outperforms isotropic-TFM in terms of imaging amplitude gain with a maximum gain of 4.67 dB. Furthermore, it offers superior computational efficiency compared to Dijkstra-TFM.

Influence of stacking sequence on flexural properties of hybrid carbon fibre reinforced polymer laminates

This paper presents a numerical investigation of the influence of the stacking sequence and fibre variation of the plies on the flexural properties of carbon fibre-reinforced polymer laminates. The numerical approach utilised a three-point flexural test to evaluate different quasi-isotropic stacking sequences. It also analysed attempts to reinforce failure-prone plies only using a stronger prepreg material to reduce the cost of the laminate. The results were validated by conducting a cantilever bending test and compared with calculations based on classical lamination theory. The beam deflection, normal stress per ply, and the Puck failure criterion inverse reverse factor per ply were used for evaluation and result comparison. The results showed that the quasi-isotropic stacking sequence [0/90/+45/−45]s is the most suitable for beam applications. Replacement of the outer plies of the composite laminate by a stronger ply material made the hybrid laminate performance almost identical to a pure composite laminate consisting of stronger material only.

A novel layup process for reducing surface thermal distortion of CFRP laminate reflector

This study proposes a novel anti-symmetric folding layup process to reduce the surface thermal distortion of carbon-fiber-reinforced polymer (CFRP) reflector. Firstly, theoretical equations regarding the influencing factors of surface thermal distortion in CFRP reflector are derived, and the concept and advantages of the anti-symmetric folding layup process are introduced. Secondly, free thermal expansion analysis considering the ply angle misalignment is conducted, showing that the novel process can reduce surface thermal distortion by 36.13 % compared to traditional process. Finally, experimental samples with different layup processes are designed and manufactured, and their surface thermal distortion is detected using shear speckle interferometry. The experimental results show that compared with the traditional symmetric layup process, the double anti-symmetric folding layup process can reduce the surface thermal distortion of CFRP reflector by 32.39 %, demonstrating significant advantages in thermal stability and strong potential for practical engineering applications.

Damage characterization and discrimination in laser-shocked carbon fiber reinforced polymer laminates: A mass-spring-damping model approach

Damage characterization and discrimination in laser-shocked carbon fiber reinforced polymer laminates: A mass-spring-damping model approach

Geometry accuracy control in abrasive water jet taper hole machining of ultra‐thick carbon fiber‐reinforced polymer (CFRP) laminates

AbstractThe primary factors affecting the geometric accuracy of abrasive water jet (AWJ) machining of ultra‐thick carbon fiber‐reinforced polymer (CFRP) laminates are the cutting front drag and kerf width deviation caused by energy dissipation. Firstly, this study comprehensively analyzes the influence of the coupling relationship between cutting front drag and kerf width deviation on the geometric accuracy of hole machining. Secondly, a gradient distribution theory for jet traverse speed with cutting depth is proposed for taper hole machining characteristics. Finally, a general geometric error model applicable to both straight and taper hole machining of ultra‐thick CFRP laminates using AWJ is established, along with a geometric error compensation method. A series of experiments validate the accuracy of the proposed geometric error model and compensation method. The novelty of this research lies in unifying the geometric error models for straight and taper hole machining of ultra‐thick CFRP laminates by considering the gradient distribution of jet traverse speed. The proposed error compensation method reduces the high degree of freedom required for machine tools. This study provides a general geometric error model and compensation strategy for AWJ hole machining of ultra‐thick CFRP laminates, which has significant engineering value for achieving 3D controllable AWJ machining of complex ultra‐thick CFRP components.Highlights The high geometric precision taper holes machining technique is a necessary prerequisite for achieving precise machining of complex trajectories in ultra‐thick CFRP with abrasive water jet. The influence of the coupling relationship between cutting front drag and kerf taper on the geometric accuracy of hole processing is comprehensively analyzed. A model considering the gradient distribution of traverse speed during taper holes machining was established, and a geometric error model considering this gradient distribution of traverse speed was developed. A taper holes machining geometric error compensation method with high engineering applicability was proposed. Geometric error prediction experiments and error compensation experiments were conducted, and the results proved the accuracy of the geometric error model and error compensation method.

Comparison of carbon‐reinforced composites manufactured by vacuum assisted resin infusion with traditional and fully recyclable epoxy resins

AbstractThis study presents a comparative analysis of carbon fiber reinforced polymer (CFRP) composites manufactured through vacuum assisted resin infusion (VARI) using a traditional epoxy resin (E), a fully‐recyclable epoxy resin system with (BBR10) and without (BBR) the addition of a reactive diluent (R*Diluent). Various mechanical and thermal tests were conducted to assess their performance. The BBR10 laminate, incorporating 10 wt% R*Diluent, exhibited competitive mechanical performance, comparable to traditional (E) and fully‐recyclable laminates (BBR). Despite a slightly lower ultimate tensile strength (UTS) compared with BBR, BBR10 demonstrated improved flexural strength and modulus. Low‐velocity impact testing confirmed comparable strength between VARI‐produced composites with the recyclable matrix (BBR and BBR10) and the traditional one (E). X‐ray mCT investigations revealed distinct void arrangements in the CFRP laminates. Additionally, a chemical approach was employed for recovering high fractions of fibers from CFRP laminates with a recyclable matrix (BBR and BBR10). Chemical recycling achieved an almost 100% yield for long carbon fibers.Highlights Comparative analysis of CFRP composites manufactured through VARI. Diluent addition allowed to tailor the recyclable epoxy viscosity. Mechanical characterization of traditional and fully recyclable epoxy resins. Investigation by X‐ray mCT of potential flaws and manufacturing defects. Chemical recycling of CFRP laminates with a recyclable matrix.

Flexural behavior of RC beams externally strengthened with side-bonded CFRP laminates with variable internal reinforcement

This study investigates the flexural behavior of reinforced concrete (RC) beams externally strengthened with bottom- and side-bonded carbon fiber-reinforced polymer (CFRP) sheets with variable steel ratio. The choice of applying the CFRP sheets in a bottom- or side-bonded configuration depends on the accessibility of the beam. This experimental investigation is aimed at studying and comparing the efficacy of bottom- and side-bonded CFRP sheets for flexural strengthening of RC beams with variable internal steel ratios. The effect of steel reinforcement ratio, and the number of CFRP plies are examined by testing 10 RC beams under a four-point bending configuration. The results in terms of load-deflection response, ultimate load-carrying capacity, failure modes, and ductility are studied and compared with control unstrengthened beams. The study revealed that side-bonded beams provided flexural capacity comparable to the bottom-bonded beams for both ratios of internal reinforcement used in the study. The study also showed that both strengthening configurations were more effective when the internal steel ratio was low. In terms of ductility, the side-bonded scheme provided ductility indices comparable to the bottom-bonded beams. The findings of this study confirm the feasibility of using side-bonded fiber-reinforced polymer (FRP) sheets as a strengthening technique for RC beams when the soffit of the beam is inaccessible.

Study of synergistic and competitive mechanisms on toughening CFRP composites with intrinsic and extrinsic multiscale interleaves

Delamination damage is a common failure mode of carbon fiber reinforced polymer (CFRP) laminates, which severely limits their application. This paper proposes a novel interlaminar toughening structure based on intrinsic and extrinsic multiscale toughening mechanisms using nanoscale multi-walled carbon nanotubes (MWCNTs) and microscale core-shell rubber (CSR). The resin sample M-0.5/C-8, containing 0.5 wt% MWCNTs and 8 wt% CSR, exhibited significant improvements in fracture toughness, with increases of 183.3 % in the mode-I critical stress intensity factor (KIC, Resin) and 412.0 % in the critical energy release rate of resin (GIC, Resin). However, its flexural strength and modulus decreased by 3.1 % and 3.3 %, respectively. Introducing MWCNTs and CSR into the interlayers of the CFRP, the interleaved toughened CFRP laminate exhibited a 123.3 % improvement in the mode-I critical energy release rate (GIC, Comp) and a 79.6 % increase in the mode-II critical energy release rate (GIIC, Comp) during the crack propagation stage, without sacrificing flexural performance. This remarkable enhancement in interlaminar fracture toughness results from the simultaneous triggering of nanoscale extrinsic toughening and microscale intrinsic toughening during crack growth. The flexural properties and fracture toughness of Epoxy/MWCNTs/CSR composites were also investigated to understand the properties transformation from resin matrix to CFRP. Morphological characterization and numerical analysis were used to analyze the synergies and constraints between two energy dissipation behaviors.

Comprehensive evaluation of CFRP laminates using NDT methods for aircraft applications

The evaluation of carbon fiber reinforced polymers (CFRP) laminates during and after the Mode I test was successfully conducted, integrating non-destructive testing of acoustic emission (AE) and ultrasound scanning. Two different specimens [+45°/-45°/0°]2S and [0°/+45°/-45°]2S were used to detect the effects of stacking sequences of the laminates. Results indicated that applying AE sensors to the specimens slightly affect to the laminate performance. Thus, the laminates are validated and showed that for [+45°/-45°/0°]2S laminates, the system can withstand load and increase the displacement at break more than twice of [0°/+45°/-45°]2S laminates. Moreover, the ultrasound scanning showed that the crack trace is visible. [+45°/-45°/0°]2S laminates have smaller crack around 24 mm compared to [0°/+45°/-45°]2S laminates with 30 mm. Image analysis revealed that after specimen are forced to open, the [+45°/-45°/0°]2S laminates can prevent long crack compared to [0°/+45°/-45°]2S laminates. The double cantilever beam (DCB) test, employing various stacking sequences, demonstrated excellent examination results using non-destructive testing. Theoretical calculations regarding residual thermal expansion due to different coefficients of thermal expansion also revealed a slight impact of varying manufacturing temperatures on the laminates. These findings offer valuable insights for detecting, predicting, and preventing specimen failures in aircraft and aerospace structures without resorting to destructive examinations, facilitating appropriate preventive maintenance.

FBG Sensing Data Motivated Dynamic Feature Assessment of the Complicated CFRP Antenna Beam under Various Vibration Modes

Carbon fiber-reinforced polymer (CFRP) components were extensively used and current studies mainly refer to CFRP laminates. The dynamic performance of the complicated CFRP antenna beams is yet to be explored. Therefore, a sensor layout based on fiber Bragg gratings (FBGs) in series was designed to measure the dynamic response of the CFRP antenna beam, and various vibration tests (sweep frequency test, simulated long-life vibration test, shock vibration test, functional vibration test, and constant frequency vibration test) were conducted. The time and frequency domain analysis on FBG sensing signals was performed to check the vibration performance and assess the health condition of this novel CFRP structure. The results indicate that strain values reach a maximum of only 300 µε under different test conditions. The antenna beam exhibited clear vibration patterns, with the first four intrinsic frequencies identified at 44, 94.87, 107.1, and 193.45 Hz. It shows that strain distribution and vibration modes of the antenna beam can be characterized from the sensing data, and the dynamic feature can be much more accurately assessed. The FBG sensors attached on the surface of CFRP antenna beam can accurately and stably measure the dynamic response, which validates that the interfaces between optical fiber sensing elements and CFRP material have excellent interfacial bonding characteristics. The novel CFRP antenna beam exhibits the excellent dynamic performance and stability, offering the replacement of traditional steel antenna beams. The study can finally instruct the development of self-sensing CFRP antenna beams assembled with FBGs in series.

Effect of the level of anisotropy on the macroscopic failure of notched thin-ply laminates

This work presents a detailed experimental study conducted for a range of different lay-ups using thin-ply carbon fiber reinforced polymer (CFRP) laminates. The selection of the laminates was performed relying on their level of anisotropy. The laminates vary from a quasi-isotropic (QI) laminate, which is weakly anisotropic, to a cross-ply (CP) laminate, which is strongly anisotropic. The laminates were tested in on-axis and off-axis open hole tension (OHT). The main objective was to observe the effect of the level of anisotropy of the laminate on the macroscopic failure and observed failure patterns. It is shown that, contrary to most existing observations so far, depending on the lay-up and consequently its level of anisotropy, open-hole, quasi-homogeneous thin-ply laminates do not necessarily exhibit a fiber dominated failure mode, but could develop sub-critical damage mechanisms in a large extent prior to ultimate failure, reminiscent of what is observed for standard-ply CFRP laminates.

Hierarchical enhancement of carbon fiber reinforced polymer laminate with randomly hybridized carbon nanotubes and aramid‐pulp micro/nano‐fibers

AbstractIn this study, inspired by human teeth, random hybrid carbon nanotubes (CNTs) and aramid‐pulp micro/nano‐fibers (AP) with different mixing ratios were experimentally interleaved into carbon fiber reinforced polymer (CFRP) panels to form a gradient interface for hierarchical enhancement and synthetic effects. Due to different out‐of‐plane movability or penetrability of the CNTs, AP, and resin, 3rd and 4th order bio‐inspired gradient interfaces between the carbon‐fiber plies were formed in situ. According to flexural testing, hybrid CNT/AP‐interleaved CFRP with a CNT of 3.6 gsm and an AP of 2.4 gsm showed an improvement of 47.35% in flexural strength. Furthermore, the synthetic effects of hybrid CNT/AP‐interleaving were investigated by analyzing the mer3its and demerits of the CNT‐ or AP‐interleaving methods. It was identified that the hybridization of multiple length‐scale fibers as interleaves can be used to produce more hierarchical enhancements and synthetic effects. The new insights into multi‐scale strengthening mechanisms were systematically revealed from the models of hierarchical fiber‐bridging. And the graded penetration mechanisms of multi‐scale fiber‐reinforced CFRP laminates were analyzed.Highlights The in situ gradient interfaces form by Z‐direction penetration of CNT/AP. CNT/AP‐interleaving can form hierarchical enhancements and synthetic effects. Multi‐scale strengthening via fiber‐bridging and graded penetrations achieved. More fiber‐bridging occur at sub‐surface regions of the carbon‐fiber plies.

Partition five-axis surface machining of CFRP laminate structures considering fiber orientation

ABSTRACT Carbon Fiber Reinforced Polymer (CFRP) is commonly employed in advanced industries, acclaimed for their outstanding mechanical properties. The inherent anisotropy of CFRP necessitates careful consideration of the Fiber Cutting Angle (FCA) to achieve optimal surface quality during machining, a challenge that intensifies with curved surface components due to the continuous variability of FCA. In the machining of CFRP curved surfaces, the presence of local singularity precipitates abrupt changes in tool orientation, adversely affecting surface integrity and machining efficiency. To solve this problem, this study proposed a toolpath partitioning method specifically designed for the machining of CFRP curved surfaces, aiming to mitigate the effects of local singularity. Additionally, a novel tool positioning strategy accounting for dual fiber orientations in the machining of bidirectional CFRP curved surfaces was developed. The practical applicability of these methodologies was assessed through the manufacturing of an internal fixation plate via 5-axis machining of bidirectional CFRP laminates. Comparative microscopic observations and surface profile assessments demonstrate a marked improvement in surface quality relative to traditional 3-axis machining, alongside a 25% reduction in machining time compared to 5-axis machining processes absent the partitioning method.

Permeability and barrier layer properties of a woven carbon fibre polymer composite as battery packaging

Carbon fibre reinforced polymer (CFRP) laminates are used in various studies as Li-ion polymer (LiPo) battery packaging. However, their suitability as a packaging material is not well understood. The present study investigates the liquid absorption (water and lithium bis(trifluoromethanesulfonic)imide (LiTFSI) electrolyte immersion tests) and barrier layer properties (water vapour transmission rate (WVTR) and oxygen transmission rate (OTR) tests) of a 200 gsm woven CFRP laminate to assess its suitability as a battery packaging material. This is the first study to show that prolonged immersion in battery electrolyte does not change the mechanical properties of a woven CFRP laminate. Hence, the CFRP laminate may be suitable for structural battery components, such as current collectors and electrodes. However, CFRP should not be used as battery packaging, as OTR and WVTR values of the CFRP laminate were found to be five and one order of magnitudes higher than typical battery pouch materials (i.e. aluminium foil), respectively.