Shale Beds Research Articles

Mineralogical and geochemical studies of shales from Kopili Formation, Dima Hasao district Assam, North East India: Insights into diagenesis, deposition and provenance

The Eocene Kopili Formation in the Assam foreland basin records sediment sources, tectonic activity and depositional environments following the India-Eurasia collision. Mineralogical and geochemical analysis of these shales exposed near Garampani, Assam, NE India was conducted to study the diagenesis, palaeoweathering, palaeosalinity, redox conditions, tectonic settings and provenance. The Kopili Formation is composed of mainly shale with thin beds of limestone, black shale and sandstone and these units overlie the Upper Sylhet Limestone. The presence of goethite-rich phosphatic nodules, secondary precipitation within the fissile planes of shale and the occurrence of anatase, talc, smectite and chlorite suggest diagenesis. The prevalence of kaolinite and mean Chemical Index of Alteration (CIA), Chemical Index of Weathering (CIW), Al2O3/MgO and Rb/Sr values of 86.73, 97.26, 16.36 and 1.32, respectively indicates extensive source rock weathering in humid tropical climate. The Index of Compositional Variation (ICV) values ranging between 0.47 and 2.38 also signify high weathering and tectonically active basin. The Sr/Ba ratio 0.34 ± 0.27 (mean±2σ) suggest overall freshwater basin. The Ni/Co (2.84 ± 2.29), V/Cr (1.65 ± 0.45) and Ce/Ce∗ (0.97 ± 0.63) suggest fluctuating redox environment. The samples predominantly cluster in continental island arc domain on the Th-Sc-Zr/10, La-Th-Sc and Th-Co-Zr/10 discriminant diagrams. Elemental ratios of Th/Sc, La/Sc, Cr/Th with average 0.91, 3.18, 10.13 respectively and La/Th-Hf plot suggest a felsic source rock. The Kopili shale was deposited in freshwater, continental island arc basin with fluctuating redox conditions, receiving sediments from weathered Himalayan granites and gneisses under a warm and humid climate. Subsequently, they underwent diagenetic alteration by low-pH fluid(s).

Experimental study on hydraulic fracture propagation behavior in heterogeneous shale formations

The study of fracture propagation in heterogeneous shale is a crucial prerequisite for the investigation of heterogeneous cluster and perforation parameters optimization. In this paper, we conduct a physical simulation fracturing experiment on heterogeneous shale to investigate the effects of various influencing factors, such as shale bedding, near-wellbore fractures, lithological changes, and the presence of fractures surrounding the perforation hole, on fracture propagation law and morphology. Our research demonstrates that during shale fracturing, shear dislocation typically occurs between layers, resulting in the separation of different layer planes. The main fracture primarily propagates through layers in a stepped manner. The presence of sandstone in heterogeneous shale significantly impedes fracturing fractures, causing significant distortion and deviation. As the scale of natural fractures increases, it tends to cause the fracturing fracture to twist and change direction. The natural fractures network can also lead to the distortion of fracturing fractures, albeit to a lesser extent than large-scale natural fractures. The presence of micro fractures parallel to the perforation axis surrounding the perforation hole enhances the ability of the main fracturing fractures to pass through natural fractures.

Geomechanical properties of laminated shale and bedding shale after water absorption: A case study of the Chang 7 shale in Ordos basin, China

There are abundant oil and gas resources in China's continental shale formations, and these formations often contain sandy lamina, tuffaceous lamina and carbonate lamina parallel to the bedding planes, resulting in complex geomechanical properties. During the drilling process, the mechanical weak surface structure inside the shale and the hydration effect of drilling fluid may easily cause wellbore instability, which reduces the safety and benefit of drilling. To explore the geomechanical properties of laminated shale and bedding shale after water absorption, a series of tests were conducted on the Chang 7 laminated shale and bedding shale in the Ordos Basin. The result indicates that the compressive strength and elastic modulus of laminated shale and bedding shale show a trend of decreasing first and then starting to drop as β (the angle between bedding/lamina and the direction of stress) keeps increasing, and laminated shale has stronger anisotropy, lower compressive strength and elastic modulus. The moisture content of laminated shale and bedding shale increases as the soaking time increases, which leads to a decrease in the compressive strength. Compared to bedding shale, laminated shale reaches water saturation faster and has a higher moisture content. Based on the macroscopic and microscopic images before and after shale hydration, it can be concluded that natural microfractures are easily formed at the interface between the lamina and shale matrix, and brittle minerals at the edges of natural microfractures are prone to detachment, thereby increase the hydration area and intensify the hydration process. Compared to bedding shale formations, laminated shale formations have a higher hole-size elongation ratio and are more prone to collapse according to on-site data. This study reveals the geomechanical properties of laminated shale under the dual influence of anisotropy and hydration, provides support for drilling design in such formations.

Occurrence and Flow Behavior for Oil Transport in Mixed Wetting Nanoscale Shale Bedding Fractures.

Shale reservoirs are characterized by an abundance of nanoscale porosities and microfractures. The states of fluid occurrence and flow behaviors within nanoconfined spaces necessitate novel research approaches, as traditional percolation mathematical models are inadequate for accurately depicting these phenomena. This study takes the Gulong shale reservoir in China as the subject of its research. Initially, the unique mixed wetting characteristics of the Gulong shale reservoir are examined and characterized using actual micropore images. Subsequently, the occurrence and flow behavior of oil within the nanoscale bedding fractures under various wettability scenarios are described through a combination of microscopic pore image and molecular dynamics simulations. Ultimately, a mathematical model is established that depicts the velocity distribution of oil and its apparent permeability. This study findings indicate that when the scale of the shale bedding fractures is less than 100 nm, the impact of the nanoconfinement effect is significant and cannot be overlooked. In this scenario, the state of oil occurrence and its flow behavior are influenced by the initial oil-wet surface area on the mixed wetting walls. The study quantifies the velocity and density distribution of oil in mixed wetting nanoscale shale bedding fractures through a mathematical model, providing a crucial theoretical basis for upscaling from the nanoscale to the macroscale.

Palaeogeography and tectono‐stratigraphic evolution of the Aptian Ezanga‐Loémé evaporites along the proximal domain of the south Gabon‐Congo‐Cabinda margin

AbstractDuring the Early Cretaceous, massive evaporite accumulations formed in the opening South Atlantic. However, the depositional model of these salts is still poorly constrained at the scale of the West African margin. The present study focuses along the proximal domain of the south Gabon‐Congo‐Cabinda margin and is based on (i) log interpretations of 246 wells crossing undeformed to weakly deformed evaporite intervals and (ii) a structural characterization of the basement. The evaporites show 11 regional evaporite depositional cycles (CI–CXI) bounded by meter‐thick shale beds. The cycles display alternating meter‐scale carnallite‐halite beds that can be correlated over several hundred kilometres, and CVI, CVII, CVIIIa and CX culminate in localized tachyhydrite accumulations. Cross section correlations and isopach maps help to understand the palaeogeographical evolution of each cycle and depositional environments that evolved from relatively deep at the base of cycles, to very shallow at their top. CI formed a mosaic of halite‐prone depocenters deposited in pre‐salt topographic relief. CII and CIII were deposited uniformly over a flattened basin in a highly extended brine pond. From CIV to CVIIIa, the stratigraphic architecture of the salts was shaped by freshwater inflow sourced from the north and possible basement movements. This setting, together with an increased confinement of the proximal domain from the distal one with basin drawdown, favoured the development of depocenters with perennial subaqueous conditions and extreme salinities, in which more than 70 m of tachyhydrite accumulation could locally be preserved. From CVIIIb to CXI, the basin returned to a flat depositional setting without well‐developed depocenters and with increasing subsidence westwards. Marine influx increased starting from CX, allowing the deposition of sulphate beds. The salt section is capped by anhydrite deposits interbedded with clastic and dolomite, before the final marine invasion of the basin. For the first time, this study provides a large‐scale depositional tectonostratigraphic setting of the Aptian salts in the proximal domain of the West African margin. The results are of interest for K‐Mg salts exploration resources in the Aptian and pave the way for further investigation of the salt depositional environment in the distal domain of the margin.

Modeling the Hydraulic Fracturing Processes in Shale Formations Using a Meshless Method

Complex bedding properties and in situ stress conditions of shale formation lead to complex hydraulic fracturing morphologies. However, due to the limitations of traditional numerical methods, the simulation of hydraulic fracturing in shale formation still needs further development. Based on this, the liquid–solid interaction modes and the SPH governing equations considering liquid–solid interaction force have been introduced. The smoothing kernel function in the traditional SPH method is improved by introducing the fracture mark ξ, which can realize the simulation of rock hydraulic fracturing processes. The stress boundary of the SPH method is applied by stress mapping of “stress particles”, and the feasibility and correctness of the method are verified by two numerical examples. Then, the simulation of hydraulic fracturing processes of bedding shale formations are carried out. With the increase of horizontal stress ratio, the total number of damaged particles decreases, but the initiation and extension pressure increase gradually. The initiation stress of small bedding dip angles (θ < 45°) is larger than that of big bedding dip angles (θ > 45°). The hydraulic fracture propagation range at low horizontal stress ratio is wider and the fracture is along the direction of maximum principal stress, while the hydraulic fracture propagation range at high horizontal stress ratio is limited to the perforation. The hydraulic fracture will propagate through the bedding with small dip angles. However, when the bedding dip angle is larger, the hydraulic fracture will propagate along the bedding direction.

Assessment of secondary metabolites in Pennisetum purpureum planted into constructed wetlands using shale and laterite as substrate for wastewater treatment

Constructed wetlands (CWs) are systems designed to maximize pollutants removal by various mechanisms, most of which are associated with the presence of plants. However, the substances secreted by plants to defend themselves against external aggressions during their growth are very little studied in these systems. This study aimed to characterize the chemical constituents of Pennisetum purpureum extracts used in an experimental mesocosm filled with shale and laterite treating domestic wastewater. Above-ground biomass, strain diameter and secondary metabolites of P. purpureum plants grown on the different substrates (shale and laterite) were monitored, as were those grown on the experimental site (control). In addition, the removal performance of chemical oxygen demand (COD), biochemical oxygen demand (BOD5), total Kjedahl nitrogen (TKN) and Total Phosphorus (TP) was determined at the outlet of CWs. Plant biomass measured on the shale bed (13.7 ± 0.5 kg m−2) was higher than on the laterite bed (12.5 ± 0.1 kg m−2), both lower than the biomass obtained in the natural environment (14.9 ± 0.6 kg m−2). Performances ranged from 83 ± 5.4 to 76.9 ± 7 % (COD), 84.7 ± 6.8 to 78 ± 8.1 % (BOD5), 72.2 ± 10.7 to 55.5 ± 16.4 % (NTK) and 72.4 ± 4.9 to 58.4 ± 3.4 % (TP), with higher efficiencies in the shale-filled bed. Plant extracts from the experimental site were richer in secondary metabolites (total polyphenol [73.5 mgEAG/gMS], total flavonoids [18.1 mgEQ/gMS] and condensed tannin [13.3 mgEC/gMS]) than those from plants grown in CWs. However, plants in the shale-filled bed secreted more total polyphenol (57.7 mgEAG/gMS), total flavonoids (12.1 mgEQ/gMS) and condensed tannin (12 mgEC/gMS) than those in the laterite-filled bed. In short, wastewater and filtration materials have an influence on the secretion of secondary plant metabolites. However, of the two materials, shale seems to be better suited to CWs, as it promotes an environment close to the natural environment.

Accentuating the Reservoir Potentials of Balkassar Field by Delineating the Fracture Trends and Hydrocarbon Prospects with the Aid of Seismic Attributes.

Carbonates constitute a significant proportion of the world's hydrocarbon reserves, accounting for approximately 43%. Despite their substantial potential, accurately characterizing these reserves is a challenging task due to their complex and anisotropic nature. In the upper Indus basin of Pakistan, Eocene carbonates exhibit strong production capabilities. However, the Eocene reservoir (comprising the Chorgali and Sakesar formations) and the deeper Lockhart formation of the Paleocene age present a considerable challenge. The Chorgali formation is dolomitic in composition, featuring both primary and secondary porosity, while the Sakesar formation has only secondary porosity resulting from tectonic activity. The delineation of tectonically induced porosities is a highly demanding task that requires exceptional quality seismic and well data for reliable results. To address the complex heterogeneities present in the Eocene reservoir of the upper Indus basin, a variety of seismic attributes, such as sweetness, instantaneous frequency, amplitude, curvature, similarity variance, lateral continuity, and fault likelihood, have been employed in conjunction with fundamental interpreting techniques. These advanced seismic attributes greatly contribute to delineating fracture zones and identifying sweet spots with remarkable precision. They also enable a focus on high-frequency data content and differentiate between shale beds and reservoir zones based on frequency and amplitude. This helps in the concise marking of fractured zones to enhance our understanding of secondary porosity. Moreover, these attributes help delineate the continuity of reflectors and pinpoint disruptions caused by compression forces and tectonic activities. This study aims to capture the heterogeneity and complexity of reservoir zones to address a critical question regarding the Balkassar structure. The Western lobe of the field, which demonstrates promising oil production, outperforms the structurally higher Eastern part, which lags behind in production. This research seeks to recognize the geological elements contributing to the superior performance of the Western lobe and provide guidance for maximizing the potential of the Eastern lobe through advanced characterization techniques.

Biomarker characteristics of organic shale beds of Alam El Bueib Formation in Tut Oil Field, Shushan Basin, North western Desert, Egypt: Insights from oil/source rock correlation

Biomarker characteristics of organic shale beds of Alam El Bueib Formation in Tut Oil Field, Shushan Basin, North western Desert, Egypt: Insights from oil/source rock correlation

Study on failure characteristics and evaluation index of aquifer shale based on energy evolution

AbstractThe presence of abundant clay components and microporous structure in shale results in its high hydrophilicity, making a water-rich environment inevitable in petroleum exploration projects. Therefore, it is crucial to consider the influence of bedding structure, moisture content, confining pressure, and their combined effects on the geomechanical properties of shale. This article aims to investigate the mechanical properties of deep shale under varying water content conditions, elucidate the failure mode and failure mechanism of shale in actual engineering scenarios, and explores the interplay between stress, structure, moisture content, and other factors on its mechanical properties. The evaluation of wellbore stability and fracture propagation effects is proposed based on laboratory experiments using triaxial stress and strain data, along with the application of energy evolution theory. The experimental procedures encompass an analysis of shale's microscopic components and structure, as well as anisotropic shale triaxial compression tests conducted under different moisture contents and confining pressures. The results demonstrate that shale exhibits dense pores in its microstructure and displays pronounced anisotropic characteristics in its macrostructure. The presence of water within these pores, combined with the in situ stress within the formation, significantly influences the mechanical properties of shale. This anisotropy decreases with increasing moisture content, but the mechanical performance still decreases. Under triaxial compression conditions, the increase in confining pressure to some extent enhances the anisotropy of shale's deformation characteristics, which is related to the failure modes of shale. However, the detrimental effect of moisture content on shale's mechanical properties still persists. In order to quantify the impact of these factors, this study utilizes the elastic modulus as an indicator of the coupling effect. It combines the triaxial strain curve obtained from laboratory tests and proposes an evaluation index for shale mechanical properties based on the energy evolution theory. This index is suitable for assessing wellbore stability (the stability index called SIr) and crack expansion (the brittleness index called BIr). The calculation results reveal that, during the wellbore drilling process, excavating parallel to the direction of shale bedding while maintaining low moisture content and high confining pressure yields a higher SIr value, indicating better wellbore stability. On the other hand, during reservoir fracturing, fracturing perpendicular to the shale bedding direction and maintaining low confining pressure and moisture content result in a smaller BIr value. This approach is more beneficial for the expansion of shale fracture network in engineering.

Reservoir characteristics of the middle Eocene Avanah Formation in Erbil governorate, northern Iraq: Integration of outcrop and subsurface data

The current work investigate the petrophysical characteristics of the Middle Eocene Avanah Formation in the Erbil Governorate using IP software to analyze the well data, integrated with the 
 petrographic investigation of the formation in the nearest outcrop in the Gomaspan section. Well logging data revealed that the main lithology of the formation is limestone and dolostone while the lithology in the Gomaspan section is composed of limestone, dolomitic limestone, marly dolomitic limestone, and thin beds of shale. The lower dolomitic unit in the subsurface section of the formation is believed to be the most suitable reservoir unit due to good petrophysical characteristics including, low water saturation, high porous medium, and the presence of movable hydrocarbon. To measure porosities, a variety of well logging techniques were used in this study. The investigated formation was divided into Avanah dense (limestone unit) and Avanah porous (dolostone unit) based on their porous components. The petrographic study shows that most pore types of the formation are secondary and represented mainly by vuggy, moldic, intercrystalline, and fracture types. Most of the fractures in the upper limestone units are filled by calcite cement. The study claimed that the lower part of the formation (dolostone unit) in both sections is considered a good reservoir.

Microfacies analysis and depositional environment of Shiranish Formation in Selected Sections, Kurdistan Region, NE Iraq

Shiranish Formation in both Smaquli and Rawanduz sections is composed of an alternation of marly limestones, limestone and marl beds with fissile shale beds. Depend on color, lithology and other sedimentological criteria during field observations of the studied sections, the Shiranish Formation is divided lithologically into lower, middle and upper units. Planktonic Foraminiferal Lime Mudstone Microfacies (Shf1), Lime Wackestone (Shf2) and Planktonic Foraminiferal Lime Packstone Microfacies (Shf3) have been defined as three distinct microfacies with four submicrofacies ((Keeled Planktonic Foraminiferal Lime Wackestone submicrofacies (Shf2b), Globular Chamber Planktonic Foraminiferal Lime Wackestone submicrofacies (Shf2a), Bioclastic Lime Wackestone submicrofacies (Shf2c), Planktonic Foraminiferal Lime Wackestone submicrofacies (Shf2d)). The major microfacies in both sections was lime wackestone which is dominated in middle and upper units in both sections. Sedimentological and paleontological evidences suggest that the Formation was deposited in the outer shelf setting and progressed to the upper bathyal setting, in addition to that the microfacies changed from packstone to mudstone meaning deeping upward sequence.

Application of nano-scratch technology to identify continental shale mineral composition and distribution length of bedding interfacial transition zone - A case study of Cretaceous Qingshankou formation in Gulong Depression, Songliao Basin, NE China

Bedding is the smallest macroscopic layer in a sedimentary sequence, usually containing different mineral compositions and ranging in thickness from a few tens of micrometers to a few millimeters. The microscale mineral composition and mechanical properties of the bedding interfacial transition zone (BITZ) have a significant influence on the crack propagation mode, which further leads to changes in hydraulic fracturing efficiency. At present, most of the identification of the shale mineral composition and the distribution length of the bedding interface transition zone relies on scanning electron microscope, but this method can only obtain the surface morphology and cannot further evaluate the mechanical properties. In this paper, the mechanical parameters such as friction coefficient and fracture toughness of shale samples from Songliao Basin were measured by nano-scratching technique. The damaged shapes and mineral composition in the scratched area were analyzed by scanning electron microscope. Indentation depth and fracture toughness data obtained from scratch tests were fitted with a Gaussian function to determine mineral composition. The slope of the d2-L curve is closely related to the mechanical behavior of minerals and is considered an effective parameter for identifying mineral composition. Based on the fluctuation characteristics of friction coefficient and fracture toughness curve, a quantitative method of shale BITZ distribution length based on linear regression is proposed, and the upgrade from single-parameter to multi-parameter combination is realized by using the method of dimensional analysis. The results of the study show that plastic minerals can effectively absorb energy and convert it into volume deformation and the rapid release of strain energy from brittle minerals results in the collapse of rock debris. The identification of mineral composition based on fracture toughness is a more accurate and effective method compared to the scratch depth and the slope of the d2-L curve. As the influence of mechanical performance was not considered, the length of BITZ distribution determined by SEM was significantly smaller than the analysis results of mechanical parameters. Compared with the friction coefficient method and the fracture toughness method, the dimensionless parameter method integrates several mechanical parameters and has high accuracy and applicability in identifying the distribution length of the interfacial transition zone of shale bedding. The results will help study the mechanical properties of different mineral interfaces of shale at the microscopic scale using the nano-scratch technique.

Unravelling Cenozoic carbonate platform fluid expulsion: Deciphering pockmark morphologies and genesis in the Tanintharyi shelf of the Andaman Sea as promising hydrocarbon reservoirs

Pockmarks, intriguing seafloor geological and geomorphological features, are commonly observed in marginal basins with hydrocarbon potential. As a Cenozoic marginal sea, the Andaman Sea is known for its significant petroleum reserves, and exploring its back-arc continental margin has revealed favourable conditions for petroleum occurrences. This study focuses on the Tanintharyi passive continental margin in the Andaman Sea, employing extensive stratigraphic and morphological analyses based on 2D and 3D seismic data interpretation techniques. Specifically, sub-seafloor characteristics of the Tanintharyi shelf region were investigated, focusing on comprehensively understanding pockmark morphologies, including their generation, evolution, migration, preservation, and the complete process leading to seabed leakage. This study revealed the potential of the Oligocene/Early Miocene carbonate platform in the Tanintharyi shelf region as a significant hydrocarbon reservoir for the upwelling buoyant fluids from the deep East Andaman Basin. Besides reservoir function, this carbonate platform serves as a passageway for the migration of fluids from the deep-sea area to the shallow-sea area, thereby playing a pivotal role in supporting fluid expulsion mechanisms in shaping a pockmark train adjacent to truncated sedimentary formations surrounding a geomorphological high on the contemporary seafloor. Additionally, the study examines the influence of changes in sedimentary facies and the tectonic setting of the Andaman Sea on pockmark evolutions, with a specific emphasis on the role of the uppermost shallow marine shale beds in developing sub-seafloor overpressure systems due to their impermeable seal rock properties. The article presents substantial evidence for the initiation of pockmark fields during the Middle Miocene period, followed by their transformation into pockmark trains on the present-day seafloor, attributed to the triggering effect of sub-seafloor overpressure systems due to changes in sedimentary dynamics in the Andaman Sea.

Utilizing of aquifer hydraulic parameters to assess the groundwater sustainability in the new reclamation area of Moghra Oasis: Western Desert—Egypt

The sustainability of groundwater aquifers requires evaluating several parameters, the most important of which are hydraulic parameters. Therefore, the essential aim of this research is to develop a management plan for the Moghra aquifer in order to prevent the expanding of water level decline and degradation of groundwater quality due to overexploitation and scarcity of recharge. To achieve this goal, all aquifer hydraulic parameters such as transmissivity, hydraulic conductivity, radius of interference, specific capacity, resulted drawdown, well loss, formation loss, well efficiency, and optimum safe yield had been measured for 40 groundwater wells drilled in the new reclaimed areas of Moghra Oasis. Based on geographic information system (GIS), hydrogeological cross sections and thematic maps for all parameters were created such as aquifer thickness, water table, groundwater flow direction, drawdown and groundwater salinity maps. The results revealed that clay and shale beds separated the three water-bearing formations of the Moghra aquifer. The aquifer-saturated thickness ranged from 30 and 102 m, and the groundwater level was below the mean sea level for all wells (ranges from − 72 to − 26.6 m). The calculated hydraulic parameters based on the analysis of long-duration pumping tests indicated that the studied aquifer has a wide variety of transmissivity (T) between 631 and 3768 m2/day, hydraulic conductivity (K) between 13.4 and 104.6 m/day, radius of influence from 126.3 to 581.3 m and specific capacity between 377.14 and 883.72 m2/day. On the other hand, the evaluation of existing drilled wells performance based on the results of step tests showed that well loss coefficient ranges between 0.0004749 and 0.0676 (h2/m5), formation loss coefficient varies from 3.34 × 10–8 to 4.80 × 10–6 (h/m2), well efficiency (γ) ranged from 50.53 to 98.08%, and optimum safe yield ranged from 40 to 98 (m3/h). Results of aquifer mapping and pumping tests can be more important for solving water scarcity issues, non-polluting water issues, health issues, and source of fresh water on the surface of the earth. The characterization of aquifer parameters in the study area, however, should be a significant component in the scientific planning and sustainability of groundwater.

Combined effects of bedding anisotropy and matrix heterogeneity on hydraulic fracturing of shales from Changning and Lushan, South China: An experimental investigation

Shales are intrinsically anisotropic and heterogeneous due to the existence of bedding planes and natural microfractures. Although the roles of shale bedding anisotropy and inherent heterogeneity have been well studied, their combined effects remain unclear. To fill this knowledge gap, we performed six hydraulic fracturing tests on shales with varying bedding inclinations (0°, 45° and 90°) collected from Changing (Sichuan) and Lushan (Jiangxi), South China. The mineral components and microstructure of shales collected from these two places were compared. The results indicate that the shale from Lushan is more heterogeneous due to its higher content of microfractures and pores than the shale from Changning. Through hydraulic fracturing analysis, we show that the fracture initiation pressure and breakdown pressure first increase and then decrease with increasing bedding inclination, and a strong linear correlation between the two pressures is found to be independent of shale heterogeneity. Second, we find inconsistency between the high breakdown pressure and large hoop deformation, which can be attributed to the anisotropy effect of shale’s bedding strength relative to the maximum principal stress. In addition, the analysis of the amplitudes and frequency of acoustic emission signals suggests that tensile cracks preferentially occur in a short-transverse mode, while deviating the bedding plane from the axial direction suppresses the initiation of tensile cracks. Shale heterogeneity is mainly reflected in reducing the magnitude of critical pressures and deflecting local fracture branch behaviors, which are less significant than the impacts of bedding anisotropy during the hydraulic fracturing process.

Geochemistry and depositional environment of black shale beds of the Belata Formation, Peninsular Malaysia

Shale deposits from Belata Formation outcrops were examined geochemically and mineralogically to establish their paragenesis and, subsequently, to identify factors that govern their depositional environment. Fifty representative samples were examined through SEM/EDX, XRD and XRF. The findings show the mineralogical composition was abundant in quartz, with pyrite and calcite in trace amount. Zr–TiO2 bivariate diagram showed predominantly felsic and intermediate igneous rocks, suggesting that the shales may be coming from the hidden basement rocks of Peninsular Malaysia. The diagenetic controls on the geochemistry are suggested by the changes in compositional trends. The samples exhibit CIA values ranging from 62.2 to 80.2, and PIA values ranging from 65 to 100. According to the V/Ni, Ni/Co, and V/Cr ratios, these black shales were formed in a suboxic environment. Additionally, the high V/Ni ratios (1.47) point to a marine source for the organic content that gives the shales their dark color. The paleoclimate during deposition was interpreted to be semiarid to warm. The black shale samples are inferred to have originated from a passive margin tectonic setting that followed continental collision and rifting stages of the foreland basin development phase of Peninsular Malaysia based on geochemical proxies and associated diagrams.

The influences of perforating phase and bedding planes on the fracture deflection in laminated shale

The perforating phase leads to complex and diverse hydraulic fracture propagation behaviors in laminated shale formations. In this paper, a 2D high-speed imaging scheme which can capture the interaction between perforating phase and natural shale bedding planes was proposed. The phase field method was used to simulate the same conditions as in the experiment for verification and hydraulic fracture propagation mechanism under the competition of perforating phase and bedding planes was discussed. The results indicate that the bedding planes appear to be no influence on fracture propagation while the perforating phase is perpendicular to the bedding planes, and the fracture propagates along the perforating phase without deflection. When the perforating phase algins with the bedding planes, the fracture initiation pressure reserves the lowest value, and no deflection occurs during fracture propagation. When the perforating phase is the angle 45°, 60° and 75° of bedding planes, the bedding planes begin to play a key role on the fracture deflection. The maximum deflection degree is reached at the perforating phase of 75°. Numerical simulation provides evidence that the existence of shale bedding planes is not exactly equivalent to anisotropy for fracture propagation and the difference of mechanical properties between different shale layers is the fundamental reason for fracture deflection. The findings help to understand the intrinsic characteristics of shale and provide a theoretical basis for the optimization design of field perforation parameters.

Experimental study on flow heterogeneity of shale bedding fractures based on full-diameter cores

A self-designed full-diameter core experimental facility was used to evaluate the flow heterogeneity of bedding fractures at four radial directions under different closure pressures and injection rates, using full-diameter cores retaining original natural bedding fractures. The distribution morphology of bedding surface affects the conductivity of bedding fractures, and the flow capacity of bedding fractures in four radial directions varies greatly with the closure pressure and injection rate. The rougher the fracture surface, the greater the flow capacity varies with the closure pressure. For unsupported bedding fractures, the mean percentage error (MPE) of the conductivity in four radial directions increase gradually with the increase of the closure pressure. This phenomenon is especially prominent in deep rock samples. It is indicated that the flow heterogeneity of bedding fractures tends to increase with the closure pressure. When proppant is placed in the fracture, at a low closure pressure, due to the combined effects of self-support of rough fracture surface, proppant instability and uneven proppant placement, the flow heterogeneity is greater than that when proppant is not placed at the same closure pressure; however, with the increase of the closure pressure, the proppant becomes compact and stable, and the flow heterogeneity is mitigated gradually.

Significance of organo-mineralogical constituents on pore distribution, fractals and gas sorption mechanism of Permian shale beds in Korba sub-basin of the Son-Mahanadi Valley, India

In this study, shale samples obtained from the Korbasub-basin of Central India have been evaluated for the significance of organo-inorganic constituents in terms of their source potential of gas genesis, pore-matrix setup, and gas adsorption and desorption. The samples were analysed for various properties, such as megascopic features, lithological variations, depositional facies, and sources of organic and inorganic sediments. Also, maceral content, mineralogical constituents, kerogen type, pore distribution, pore structure, fractal characteristics and gas storage capacity were examined. The analysis revealed a trend of alternating bands of carbonaceous matter, silts, intercalations, and fluvial bedding lithofacies patterns indicating that the sediments were deposited under fluvio-terrestrial-lacustrine depositional conditions. Ternary facies analysis of maceral composition and van Krevelen diagram suggested the evolutionary path of type IV kerogen and are thermally matured source material located within the dry hydrocarbon generation window. Evaluation of pore types and pore structures using BET sorption plots (hysteresis H3 and isotherm type IV) revealed the presence of cylindrical, slit and combined cylindrical-slit pores with two distinct fractal characteristics. The discrete macerals underwent partial decomposition during transportation and mixing with inorganic components (clay and minerals), which influenced organic matter preservation, gas genesis, pore fractals and storage mechanism. The chemical index of alteration (CIA – 88.36 to 91.97), weathering (CIW – 96.60 to 98.80) and compositional variation (ICV – 0.31 to 0.70) demonstrated the influence of partial decomposition and strong weathering patterns on the organo-inorganic matter. A significant correlation was observed between pore fractals and elemental composition, particularly related to the resistance of weathering elements such as MgO, Al2O3, Fe2O3, SiO2, P2O5, TiO2, etc., which partially contributed to the formation of pore rugged surfaces. Microscopic and XRD analyses were employed to determine the mineral type, grain shape and size, and their amount leading to the development of the shales brittleness index (MBI). The importance of brittle characteristics, governed by minerals and clays within the shale, is discussed in relation to the hydro-fracturing technique for permeability enhancement. The results of high-pressure methane sorption indicated a moderate gas storage potential. The variation in sorption capacity (VL – 6.65 to 8.25 cc/g) is described through relationships with the ICV, pore diameter, pore volume, liptinite and total maceral content. Fractal dimensions D1 (2.4571–2.5611) and D2 (2.5804–2.7529) exhibited a direct relationship with adsorption properties, indicating the presence of rugged surfaces associated with meso- and macro-scale pores, which primarily control gas storage in shale. This research offers detailed insights into shale gas, providing valuable information for CBM and petroleum operators engaged in methane gas exploration and production. While commercial CBM production has been ongoing in India for over a decade, the exploration and understanding of shale gas reservoir characteristics are still in progress. This investigation adds significant value and highlights the extensive opportunities for research and potentially commercially recovering shale gas in the Korba sub-basin.