Average Elongation Research Articles

Study on the uniaxial tensile mechanical behavior and constitutive model of advanced high-strength steels for DP1180 and Q&P1180

With the increasing global demand for green and environmentally friendly materials, advanced high-strength steels (AHSS) produced using by cold rolling process are gaining more attention in the construction industry, such as in cold-formed thin-walled structures. To expand their engineering applications, the study of the mechanical behavior and constitutive models of AHSS is particularly important. This paper focuses on DP1180 and Q&P1180, employing experimental research and theoretical analysis to elucidate the patterns at various characteristic points and establish constitutive models for AHSS. The specific conclusions are as follows: 1) For DP1180 and Q&P1180, the average elongation after fracture is 8.9 % and 16.7 %, respectively, with strength-to-yield ratios ranging from 1.24 to 1.34 and 1.14–1.24, respectively. 2) Due to the insignificant nonlinearity exhibited by DP1180 and Q&P1180 near the nominal buckling strength, the modified nominal yield strength and equivalent ultimate strength was defined and adopted as the boundaries to divide the stress-strain curve into three segments. The mathematical expressions and relevant parameter models for each segment are established. Finally, the three-stage AHSS uniaxial tensile constitutive model was established. Compared to existing models, the proposed model demonstrates higher accuracy.

Relationship between grain structure evolution and tensile anisotropy in Al-Zn-Mg-Cu cylindrical part formed by additive friction stir deposition

The thick-walled Al-Zn-Mg-Cu cylindrical part was obtained by additive friction stir deposition, and the relationship between grain structure evolution and tensile anisotropy was investigated in detail. The intra-layer grains are significantly refined due to continuous dynamic recrystallization (CDRX), and the grains at the interface are further refined by 30%-45% due to geometric dynamic recrystallization (GDRX). The early cracking and ductility deterioration under Z direction loading are caused by strain localization due to coarse and fine grain distribution and pre-existing strain at the interface. The grain growth rates for specific orientations (Cube, P, Q, and Rotated Goss) are higher than average, and the mismatch in elastic modulus between these grown grains and the matrix results in ductility differences in the X and Y directions. Texture components and residual stresses affect yield strength in the X and Y directions. Meanwhile, dissolution of η/η' and the coarsening of the particles due to the thermal cycling effect leads to a decrease in the yield strength in the building direction. The average ultimate tensile strength (UTS) and elongation (El) of the part could reach 370 MPa and 20%, respectively. The tensile properties of the as-deposited Al-Zn-Mg-Cu cylindrical part are generally higher than those of melt-based additive manufacturing, but lower than those of the extruded and forged states due to the dissolution and coarsening of the strengthening precipitates during thermal cycling.

Performance Study of Betelvine (Piper betle Linn.) Cultivars under Varying Doses of Phytohormone-Triacontanol

Betel vine (Piper betle Linn.) belongs to the family Piperaceae. The experiment was carried out with two factorial randomized block design combining 3 replications and 18 no. of treatments. Adopted plant spacing was 50 cm x10 cm and plot to plot distance was 60 cm. Treatment Details: Factor 1: Triacontanol – 0.1% (T1), Triacontanol – 0.05% (T2), Triacontanol – 0% (T3), Factor 2: Cultivars: Utkal Sudam, Kali Bangla, Kotki, Simurali Bhabna, Simurali Gol Bhabna, Chalani local. Nutrients were applied as FYM (10 tonnes ha-1) and N:P:K::200:100:100 Kg ha-1year-1. Regarding the interaction effect of cultivar with the effect of Triacontanol, the cultivar Kotki treated with Triacontanol @ 0.1% (T1) recorded highest average vine elongation per month (32.83 cm). Whereas both the cultivar Kotki and Kali Bangla, when treated with Triacontanol @ 0.1% (T1) recorded maximum number of leaves per vine per year (4.60). The highest content of total Chlorophyll (3.89 mg/g) and essential oil (0.82%) was obtained from the cultivar Simurali Gole Bhabna treated with Triacontanol @ 0.1% (T1). The cultivar Utkal Sudam with Triacontanol @ 0.05% (T2) was observed highest Phenol content (142.58 mg GAE /100g). Maximum shelf life (18 days) was obtained from the cultivar Kali Bangla and Kotki treated with Triacontanol 0.1% (T1). From this experiment, highest benefit:cost ratio (3.03) was obtained from the cultivar Kali Bangla treated with Triacontanol @ 0.1%(T1) and lowest benefit:cost ratio (1.75) was recorded in cultivar Chalani local without the use of Triacontanol i.e. in control plot.

Strength and Plasticity Synergistic Enhancement Mechanism for AZ31B Magnesium Alloy Using Electrically Assisted Electromagnetic Forming

Few independent slip system causes poor formability of magnetic alloys at room temperature. Electromagnetic forming (EMF) is a high‐rate forming method, which improves formability of magnetic alloy. However, conventional EMF weakens energy utilization, and reduces strength and plasticity of formed parts. In this work, a novel electrical assisted electromagnetic forming (EAEMF) is proposed to improve energy utiization and properties of AZ31B alloy. nergy utilization of EAEMF is 100% higher than that of EMF under same height limit, which is due to the greater temperature and electromagnetic force acting on the sheet during EAEMF. Moreover, average tensile strength, yield strength, and elongation of the EAEMF specimen are 7.5%, 6.7%, and 50% higher than those of the EMF‐produced sample, respectively. This is because EAEMF promotes grain refinement, induces more twins and dislocations, which is beneficial for enhancing strength and plasticity. Particularly, twin density of EAEMF sample increased by 70%, grain size decreased by 26.6% owing to dynamic recrystallization. In addition, EAEMF weakened basal texture, increased deformation region and more uniform plastic deformation, provided more interfaces to accommodate disocations, which ensured the increase of plasticity. Therefore, this study proves the feasibility and superiority of EAEMF, providing new prospect for improving property of magnesium alloy parts.

Mechanical properties improvement of titanium alloy and its grain boundary dislocation evolution mechanism by novel electroshock treatment

Titanium alloys are extensively utilized in the aerospace industry due to their exceptional strength and resistance to corrosion. However, litmited performance and high dispersion has always existed for the traditional manufacturing process. A novel Electroshock Treatment (EST) procedure proposed by author's team can synergistically improve the mechanical properties and its consistency of titanium alloys under limited temperature rise, but the relevant mechanism is not yet clear. In present work, the effects of various EST conditions on the mechanical characteristics were investigated by uniaxial tensile testing, and the effect mechanism was revealed using multi-scale microstructure characterization of titanium alloys, such as SEM, EBSD and TEM. The uniaxial tensile test results show that, compared with the sample without EST, the average elongation after fracture improved by 12.5%, the strength-plastic product improved by 16.1%, and the consistency of UTS and elongation after fracture improved by 63.4% and 57.1%, respectively, with a slight increase of tensile strength (30 MPa) after appropriate treatment (current density of 0.93 × 108A/m2, and pulse duration of 300 ms). The multi-scale microscopic characterization reveals a more uniform distribution of stress concentration in TC11 titanium alloy following the appropriate EST process. Besides, the entanglement of dislocations is reduced with some dislocations being annihilated. Especially, the remaining dislocations undergoing orderly rearrangement at grain boundaries after EST. The homogenization of local lattice distortion distribution and orderly rearrangement of dislocations at grain boundaries are the primary factors contributing to the comprehensive improvement in the mechanical properties and consistency of TC11 Titanium alloy.

A new Ti–Al–Cr–Mo–Zr titanium alloy welding wire: Stability, microstructure and mechanical properties

In order to improve the plasticity of titanium alloy welded joints, relevant scholars currently focus primarily on studying the mechanism of action of alloying elements Mo and V, such as reducing the phase transition temperature of the welded seam and ensuring a certain amount of β phase residue in the welded seam. In addition to improving the stability and strengthening ability of titanium alloy welded joint, it can also maintain a certain degree of plasticity of the welded joint. However, the poor impact toughness is still the key problem that restricts its long-term stable service in the harsh environment. Our work designed and developed a new Ti–Al–Cr–Mo–Zr solid welding wire, with the synergistic effect of Al, Cr, Mo and Zr, the welded seam microstructure and grain can be refined while ensuring the enough stiffness of the welding wire and its flatness during wire feeding into the designated working area. It ensures good wetting and spreading flow performance of the liquid molten pool metal in the welding process, so better welded seam formation can be obtained. The relative contents of α′ martensite and β phase in the welded seam are 76.79% and 23.21%, respectively. The residual β phase is interspersed between the α′ martensite of the slats. The β phase provides a path for the plastic deformation of the welded joint, making it easier for dislocation slip to pass the β/α′ interface. At the same time, more dislocation slip channels and a small number of fine twins can be found in the interior of α′ martensite, which can ensure the strength while taking into account the toughness. After testing, it is found that the average tensile strength of welded joints is 901 MPa, which is close to 95% of the base metal (BM), the average post-fracture elongation of welded joints is 21%, and the impact toughness value at room temperature is distributed between 25 J and 33 J, which meets the requirements of the synergistic effect of welded joint strength and plastic toughness. It is suitable for long-term stable service of Ti64 titanium alloy welding structure under harsh working conditions.

Functional behaviour of novel multi-layered deposition via twin wire arc additive manufacturing: Microstructure evolution and wear tailoring characteristics

Twin wire arc additive manufacturing offers advantages such as high deposition rates and the ability to use a wide variety of materials, making it suitable for large-scale metal part production with enhanced efficiency and flexibility. Functionally graded deposition (FGD) based structure of dissimilar steels (SS316LSi and ER70S-6) fabricated via twin wire arc additive manufacturing and their detailed performance analysis are accomplished in the current research work. Microstructural, mechanical, and tribological characteristics of the deposited structure were investigated and analysed. Microstructure reveals polygonal ferrite, widmanstatten ferrite, skeletal ferrite, lathy ferrite, ferrite solidification, and ferrite to austenite (F/A) transformation. FGD structure possessed a microhardness of 371 HV. Average ultimate tensile strength, yield strength, and elongation percentage were 675.98 MPa, 414.21 MPa, and 38.37 %, respectively. In wear analysis, the average coefficient of friction value of WAAM-processed FGD samples is 0.44–0.49. 3D profilometer analysis reveals that average values of roughness, maximum height of roughness, and maximum roughness valley depth are significant with increasing applied loads. The findings of the present research focus on the quality and appropriateness of dissimilar steels for structural applications and provide a novel method for creating high-strength components.

Microstructures and mechanical behaviour of bimetallic structures of tungsten alloy (90WNiFe) and nickel alloy (In625) fabricated by wire-arc directed energy deposition

ABSTRACT This study reported the fabrication of bimetallic structures (BS) from tungsten alloy (90WNiFe) and nickel alloy (In625) via wire-arc directed energy deposition (DED)-based additive manufacturing (AM). Its microstructures and mechanical properties were investigated for three different heat input conditions: low (180A), medium (200A), and high (220A). The highest average ultimate tensile strength of 618 MPa was achieved in the low heat input condition, with an average elongation of 49%. Although the ultimate tensile strength of the produced BS is lower than that of 90WNiFe and In625 individually, its yield strength closely resembles that of In625 processed by wire-arc DED. Tensile samples from each heat input condition experienced different fracture locations and exhibited distinct fracture morphologies. It can be concluded that the bonding strength is attributed to the diffusion of chromium, nickel, molybdenum, and niobium from In625 into the γ-(Ni, Fe, W) binding matrix of the 90WNiFe substrate.

Microstructure and mechanical properties of TC4/TA2 honeycomb structure fabricated by Selective Laser Melting(SLM)

A TC4/TA2 honeycomb structure was fabricated using Selective Laser Melting. The study primarily investigates the impact of process parameters on the mechanical properties of as-built TC4 and TA2, as well as the correlation between microstructure and mechanical properties in as-built TC4/TA2. The resulting composite displays a heterogeneous structure of acicular α′ and columnar β grains, and exhibits superior mechanical properties with a maximum tensile strength of 1081 MPa and an average elongation of approximately 14 %. These outstanding mechanical properties are attributed to the strengthening effect of acicular α′ martensite and synergistic effect between dissimilar materials. The anisotropy of the mechanical properties of heat-treated TC4/TA2 decreased, which is attributed to the transformation of the columnar grains to the basket-waving structure and equiaxed structure.

Effects of tendon elongation on plantar pressure and clinical outcomes: A comparative analysis between open repair and minimally invasive surgery.

The aim of this study was to assess whether variances in Achilles tendon elongation are linked to dissimilarities in the plantar pressure distribution following two different surgical approaches for an Achilles tendon rupture (ATR). All patients who were treated with open or minimally invasive surgical repair (MIS) and were over 2 years post their ATR were eligible for inclusion. A total of 65 patients with an average age of 43 ± 11 years were included in the study. Thirty-five patients were treated with open repair, and 30 patients were treated with MIS. Clinical outcomes were evaluated using the American Orthopedic Foot and Ankle Society (AOFAS) and ATR Score (ATRS). Achilles tendon elongation was measured using axial and sagittal magnetic resonance imaging scans. Plantar pressure measurements for the forefoot, midfootand hindfoot during gait were divided into percentages based on total pressure, measured in g/cm2 for each area. The average AOFAS score was found 'excellent' (93 ± 2.8) in the MIS group, while it was found 'good' (87.4 ± 5.6) in the open repair group. In addition, the MIS group showed significantly superior ATRS scores (78.8 ± 7.4) compared to the open repair group (56.4 ± 15.4) (p < 0.001). The average tendon elongation in the MIS group was 11.3 ± 2 mm, while it was 17.3 ± 4.3 mm(p < 0.001) in the open repair group. While the open repair group showed significantly higher plantar pressure distribution in the initial contact and preswing phases compared to uninjured extremities, there was no significant difference between the uninjured extremities and the MIS group. In conclusion, the findings of this study demonstrated that minimally invasive surgery was associated with less tendon elongation, more proximity to the plantar pressure distributions of the uninjured extremity and superior clinical outcomes compared to open surgical repair. Therefore, minimally invasive surgery may be considered a more suitable option for acute Achilles tendon repair to achieve overall better outcomes. Level III.

Microstructure and properties of metal inert gas welded joints in a novel Al–Mg–Zn–Er–Zr alloy

Metal inert gas (MIG) welding of a novel Al-5.82Mg-0.61Zn-0.14Er-0.11Zr alloy was performed using ER5E61 and ER5B71 filler wires. The effect of the two filler wires on microstructures and mechanical properties of MIG welded joints was investigated. The study shows that fully penetrated joints are obtained by MIG welding process filled with ER5E61 and ER5B71 wires. Compared with ER5B71, the weld metal (WM) with ER5E61 exhibits a coarse structure and high solid solution of Mg and Mn elements. After the tensile test, the WM with ER5E61 and ER5B71 wires is composed of elongated coarse grains with a higher proportion of low angle grain boundaries (LAGBs). In addition, the lattice rotation occurring within the grains, indicating that single grain has an unevenly plastic deformation after the tensile test. The average microhardness of the WM is 83.4 HV and 82.9 HV for ER5E61 and ER5B71 wire, which is the lowest microhardness in the MIG welded joint. The average ultimate tensile strength (UTS) and elongation index (EI) of the MIG joints are 327.7 MPa and 8.5% for ER5E61 wire, and 314.3 MPa and 8.2% for ER5B71 wire, suggesting the MIG welded joint with ER5E61 wire achieves a good combination of strength and ductility. Quantitative assessments of the effects of different strengthening mechanisms on the strength reveal that dislocation strengthening and solid solute strengthening are the main factors to obtain a higher strength of welded joints with ER5E61.

Pelayanan pengujian kekuatan pipa HDPE di Laboratorium Kimia Material Departemen Teknik Material dan Metalurgi FTIRS-ITS

HDPE pipes are widely used in various industries, such as drinking water and sewage infrastructure, petroleum, agriculture, and construction. The advantages of HDPE pipes include corrosion resistance, light weight, easy installation, and low maintenance costs. Checking the quality of HDPE pipes, spesifically from industry that we tested, is important to ensure infrastructure safety, prevent system failure, improve operational efficiency, obtain user satisfaction, and conserve resources. We evaluated HDPE pipes with type PN 12.5 SDR 13.6 from industry in terms of resistance to hydrostatic pressure, tensile strength, and expansion capability. The evaluation was carried out at the Material Chemistry Laboratory of the Department of Material Engineering and Metallurgy FTIRS-ITS ITS in accordance with the standards of SNI 4829.2: 2015, ASTM D 638 M, and SNI 2553: 1999. The results show that HDPE pipes can withstand hydrostatic pressure up to 12 bar without leakage. The average tensile strength is 43.34 MPa with an average elongation of 354%, indicating ductile pipe properties with necking. Pipe expansion was observed to be 0.195%, indicating a good ability of the pipe to undergo expansion.

Technological properties of aromatic Basmati rice accessions

The objective of this study was to characterize the paste profile of basmati-style aromatic rice accessions. The evaluation of the 56 rice accessions by the Mean of Distances Method yielded seven groups of rice accessions based on the evaluated parameters (elongation, apparent amylose content (AAC), aroma, and paste properties). Group 1 was represented by the control sample IRGA417, a non-aromatic cultivar with the highest AAC (22.5%). The aromatic cultivars Jasmine, Empasc 104, IAC500, and Jasmine85 constituted the third group. Group 4 consisted of 41 Basmati accessions and exhibited the highest average elongation ratio (greater than 2.0). Groups 3 and 4 exhibited comparable aroma scores (2.9 and 2.8, respectively) and retrogradation processes (final viscosity: 285.37 and 291.26 RVU, and setback: 136.84 and 166.01 RVU, respectively). Group 5 was constituted with seven Basmati accessions, while groups 6 and 7 were formed with one and two Basmati accessions, respectively. Groups 5 and 6 exhibited comparable paste properties, with peak viscosities of 186.06 and 153.1 RVU, respectively, and final viscosities of 210.27 and 236.7 RVU, respectively, which were lower than those observed in the other groups. In contrast, group 7 exhibited intermediate parameters between the control IRGA417 and groups 3 and 4. Groups 3, 4, 5, 6, and 7 were classified as low amylose grains, with an AAC of 12-20%. The Basmati accession (group 4) exhibited a comparable paste profile, with a notable distinction in its high elongation, aroma, and low AAC. Consequently, these cultivars may be well accepted by consumers of aromatic rice.

Structure refinement and performance balance of high-strength aluminum alloys using an improved thermomechanical treatment process

The microstructure of 7A85 aluminum alloy forgings often contains coarse second-phase particles and grains. To improve the microstructures and balance the properties, we used an enhanced thermomechanical treatment process that included multiaxial hot forging, multiaxial cryoforging (MACF), and three-step aging treatment. We thoroughly investigated the effects of MACF with 1–3 passes on the evolution of microstructure, three-dimensional (3D) mechanical properties at the center and edge, fracture toughness, and corrosion resistance of the alloy. Our findings revealed that multiaxial hot forging had a limited ability to crush the coarse second-phase particles. However, the higher flow stress and compound brittleness of MACF resulted in a significant increase in particle fragmentation and driving force for precipitation. Additionally, under MACF, massive dislocations proliferated due to the inhibition of dynamic recovery, forming large orientation gradient regions, which promote static recrystallization and grain refinement during solution treatment. As the number of MACF passes increased from one to three, the effect of particle crushing initially increased and then plateaued, the 3D grain sizes first decreased and then slightly increased, and the spacing of grain boundary precipitates (GBPs) increased. The dense and uniform precipitates, finest equiaxed grains, a low fraction of coarse particles, and large GBP spacing in MACF2 resulted in the higher strength, highest elongation with minimal anisotropy, superior fracture toughness, and enhanced corrosion resistance. Ultimately, MACF2 demonstrated the best overall performance and good homogeneity, with an average 3D ultimate tensile strength, average 3D yield strength, average 3D elongation, and fracture toughness at the center of 548 MPa, 476 MPa, 13.4%, and 42.5 MPa m1/2, respectively. These values were respectively 4.2%, 1.9%, 50.6%, and 13.9% higher than those of the uncompressed sample.

AZ91 Magnesium Alloy CMT Cladding Layer Processed Using Friction Stir Processing: Effect of Traverse Speed on Microstructure and Mechanical Properties.

Friction stir processing (FSP) is a solid-state treating method to enhance the mechanical properties of materials by altering their microstructure. In this study, FSP was applied to the AZ91 magnesium alloy cladding layer prepared using cold metal transition (CMT) technology, and the purpose was to investigate the effect of the traverse speed of the H13 steel stirring head under a constant rotation speed on the microstructure and mechanical properties of the cladding layer. The results demonstrated that FSP could effectively decrease the grain size of the cladding layer and lead to the dispersion and dissolution of the coarse β-Mg17Al12 second phase into the α-Mg matrix. The mechanical characteristics of the processed cladding layer were significantly enhanced compared to the unprocessed cladding layer due to the grain refinement and second-phase strengthening induced by FSP. When the stirring head rotation speed was set at 300 r/min, the average microhardness and tensile properties of the specimens showed a tendency of initially increasing and then dropping as the traverse speed increased. The cladding layer, obtained at a traverse speed of 60 mm/min, displayed optimal mechanical properties with an average microhardness, tensile strength, and elongation of 85.6 HV0.1, 278.5 MPa, and 13.4%, respectively.

Hybrid interlayer hot rolling and wire arc additive manufacturing of Al-Mg alloy: Microstructure, mechanical properties and strengthening mechanism

Considering the deformation-strengthening benefits of Al-Mg alloy and the high forming efficiency offered by wire and arc additive manufacturing (WAAM), the microstructure evolution and strengthening mechanism of hybrid interlayer hot rolling and wire arc additive manufacturing (HR-WAAM) samples have been systematically investigated in this study. The results indicate that interlayer hot rolling can effectively reduce the size and number of pores, which diminishes the stress concentration areas. Additionally, rolling deformation significantly enhances the effect of dislocation strengthening. Furthermore, a high density of dislocations can promote recrystallization to refine grain size, while also improving grain orientation, all of which contribute to better stress distribution. Due to these reasons, the strength and toughness of the alloy are notably improved. The average ultimate tensile strength (UTS), yield strength (YS), and elongation (EL) values achieved by HR-WAAM samples were 338 MPa, 276 MPa, and 20.9%, respectively. These values represent increases of 28.5%, 41.5%, and 38.4% compared to conventional WAAM samples. These findings are expected to provide an efficient and cost-effective method for additive manufacturing (AM) of deformation-strengthened aluminum alloys.

Particle fracture regimes from impact simulations.

We introduce an approach to particle breakage, wherein the particle is modeled as an aggregate of polyhedral cells with their common surfaces governed by the Griffith criterion of fracture. This model is implemented within a discrete element code to simulate and analyze the breakage behavior of a single particle impacting a rigid plane. We find that fracture dynamics involves three distinct regimes as a function of the normalized impact energy ω. At low values of ω, the particle undergoes elastic rebound and no cracks occur inside the particle. In the intermediate range, the particle is damaged by nucleation and propagation of cracks, and the effective restitution coefficient declines without breakup of the particle. Finally, for values of ω beyond a well-defined threshold, the particle breaks into fragments and the restitution coefficient increases with ω due to kinetic energy carried away by the fragments. We show that particle damage, restitution coefficient, and fracture efficiency (the amount of energy input consumed for particle fracture) collapse well as a function of dimensionless scaling parameters. Our data are also sufficiently accurate to scale fragment size and shape distributions. It is found that fragment masses (volumes) follow a power-law distribution with an exponent decreasing with fracture energy. Interestingly, the average elongation and flatness of fragments are very close to those observed in experiments and lunar samples at the optimal fracture efficiency.

Sustainable highly stretchable and tough gelatin-alkali lignin hydrogels for scaffolding and 3D printing applications

Hydrogels and bioinks obtained from gelatin (Gel) generally present poor mechanical properties and require a series of time-consuming and stepwise chemical processes to exhibit improved elasticity and resistance to fatigue. Alkali lignin (AL) is an underutilized by-product of the paper and pulp industry. It is a widely available and inexpensive biomaterial that presents enormous potential for high-value applications owing to its ease of chemical modification and unique naturally occurring polyaromatic structure. This work aims to develop different GelAL hydrogel formulations with a single-step method that are innovative and sustainable. The results obtained from the mechanical, rheological, and degradation studies of the developed GelAL hydrogels demonstrated that their properties can be easily modified and tuned using straightforward processing techniques, allowing these stretchable and tough hydrogels to be used as bioinks in 3D printing. The modulation of mechanical properties through hydrogel formulations is a result of interactions between the Gel and AL which can be associated with the interplay of anionic sulfonates in AL and the arginine and lysine residues from Gel. The tensile stress at the break for the Gel20AL10 formulation was 32% higher than the value for Gel20AL5 and 157% higher than that of Gel10AL10. The elongation at break also decreased as it averaged 659 ± 149% for the Gel20AL10 formulation, which is 20% more than that of Gel20AL5 and 55% more than the average elongation at break of Gel10AL10. Further zeta potential measurements and quartz crystal microbalance with energy dissipation studies demonstrated that Gel and AL seem to form neutral complexes when mixed. These assays support the idea that AL and Gel are readily bound through weak interactions, and chemical crosslinking strategies need to be considered when degradability and mechanical properties tuning are envisioned. Altogether, these high-performance GelAL hydrogels display mechanical properties similar to soft tissues with high elasticity beyond that of natural hydrogels and fulfill the requirements of a broad range of biomedical and tissue engineering scaffolding applications.

A novel magnetic field assisted powder arc additive manufacturing for Ti60 titanium alloy: Method, microstructure and mechanical properties

Due to the rapid heating-cooling process and unstable keyhole, pore defects are easily formed during the high energy beam-powder additive manufacturing (AM) process, posing great challenges to the high-performance manufacturing of aerospace components. Using an arc with lower energy density as a heat source can effectively avoid these defects, but its matching raw materials are limited to wire. In this paper, a novel magnetic field assisted powder arc additive manufacturing (MFA-PAAM) method has been proposed, which combines arc heat source and powder raw material to achieve dense metal parts. A transverse magnetic field (TMF) was introduced to solve the powder spattering problem which impacts the stability of the PAAM process, by regulating the direction of the arc plasma flow and the arc pressure. The unique melting behavior of the powder under arc heating was captured by a high-speed camera, which can be summarized into two steps: balling and adsorption by the molten pool. And the well-formed and fully dense Ti60 high-temperature titanium alloy wall components were successfully manufactured using the self-developed equipment. The microstructure of the thin-wall component is dominated by basket-weave distributed α laths and few β sheets remaining at their boundaries. A layered periodic distribution along the building direction was observed, which is mainly distinguished from the content and morphology of the β phase. The average ultimate tensile strength (UTS) and elongation to failure in the travelling direction are 1003.2 MPa and 15.1%, while the average UTS and elongation along the building direction are 1009.3 MPa and 16.6%, respectively. The fracture morphologies in both directions are characterized by ductile fracture. The MFA-PAAM technique shows great potential for fabricating materials that are difficult to be drawn into wires with high efficiency and performance.

Study on the Forming Process and Properties of AlSi60 Alloy by Selective Laser Melting

Hypereutectic Al-Si alloys, which have a silicon content ranging from 12% to 70%, are a new generation of casing materials for chip packaging. They have broad applications in aerospace, weaponry, and civilian communications. Selective Laser Melting (SLM) offers significant advantages in achieving near-net shaping of complex casings. This paper presents a study on the formation defects, microstructure, and room temperature tensile properties of AlSi60 alloy prepared by SLM. The results indicate that the primary forming defects in the SLM AlSi60 alloy are balling, lack of fusion, and porosity. These defects are mainly influenced by the volumetric energy density. Samples of good quality can be produced within the range of 150 J/mm3 to 250 J/mm3. However, the same volumetric energy density can result in differences in sample quality due to various combinations of process parameters. Therefore, it has been determined that a well-formed AlSi60 alloy can be obtained within a laser power range of 300 W–350 W, scanning speed of 400 mm/s–800 mm/s, and hatch spacing of 0.09 mm–0.13 mm, with a density close to 98%. The microstructure of the SLM AlSi60 alloy consists of primary Si phases with irregular shapes and sharp edges measuring 5–10 μm, eutectic Si particles of 0.5 μm, and α-Al phases, with eutectic Si dispersed within the α-Al. The SLM AlSi60 alloy exhibits fine and evenly distributed primary Si phases with an average hardness of 203 HV. No significant anisotropy in hardness values was observed in the X and Y directions. The tensile strength of the alloy reached an average of 219 MPa, with an average elongation of 2.99%. During the tensile process, cracks initiated by the primary Si phases rapidly expanded, exhibiting minor ductile fracture characteristics in the Al phases. Due to the high volume fraction of Si phases, the tensile test was dominated by brittle fracture. The tensile curve only exhibited the elastic stage.