Abstract

AbstractTwo‐ and Threefold Intramolecular Brigdging p‐tert‐Butylcalix[8]arene Triphosphates – Synthesis, Structure and Stereochemistry [1]The phosphorylation of p‐tert‐butylcalix[8]arene (1) with phosphorus pentachloride and hydrolysis gives intramolecular bridging tert‐butylcalix[8]arene triphosphates. The reactivity (esterification, dehydratisation, complexation), the structure (nmr and x‐ray), and the stereochemical behaviour of the phosphates will be discussed.

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