Abstract
A full-sandwich high-valent zirconacarborane containing the unusual B-B-linked bis(carboranyl) ligand [o-C6H4(CH2)(2)C2B10H9](2)(4-) was unprecedentedly isolated from the reaction of ZrCl4(THF)(2) with the carbons-adjacent carborane salt [{mu-1,2-[o-C6H4(CH2)(2)]-1,2-C2B10H10}(2)Na-4(THF)(6)](n). This reaction also generated a divalent zirconacarborane.
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