Abstract

A novel zeolite-coated fiber sensors for detection of volatile organic compounds (VOCs) based on the Fabry-Perot interferometer was proposed and demonstrated. The sensor comprised a polycrystalline silicalite thin film grown up on the cleaved end face of a standard single-mode fiber. The inline Fabry-Perot cavity was composed by the end face of the single-mode fiber and the thin film. The sensor device operated by measuring the interference signal, which was a function of the amount of chemical vapor adsorption in its crystalline micro porous structure. Experimental results showed that the proposed VOC sensor worked well and the sensitivities were 2.78×10−3 dB/ppm when the concentration ranged from 350 ppm to 2100 ppm and 1.23×10−3 dB/ppm when the concentration ranged from 2100 ppm to 5250 ppm.

Highlights

  • The detection of volatile organic compounds (VOCs) has been found useful in many areas including environmental pollutant monitoring, food quality assurance, and emission control [1]

  • Experimental results showed that the proposed sensor for chemical vapor measurement worked well and the sensitivities of the isopropanol concentration were 2.78×10–3 dB/ppm when the concentration ranged from 350 ppm to 2100 ppm and 1.23×10–3 dB/ppm when the concentration ranged from 2100 ppm to 5250 ppm

  • The sensor was made by growing the thin silicalite film on the cleaved end face of a standard single-mode fiber by in situ crystallization from an aluminum-free precursor solution using tetrapropylammonium ion (TPA+) as the structure directing agent (SDA)

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Summary

Introduction

The detection of volatile organic compounds (VOCs) has been found useful in many areas including environmental pollutant monitoring, food quality assurance, and emission control [1]. The sensors based on optical fibers have been attracting increasing interest due to their advantages such as the small size, remote measurement, and immunity to electromagnetic interference. The F-P cavity can be constituted by a section of the fiber between two dielectric mirrors [2] or a gap between two dielectric end surfaces [3]. An interferometer signal which is formed by two reflections at two end surfaces is a function of the length and refractive index of the cavity. A fiber F-P sensor is capable of measuring various parameters which are resulted from environmental changes. Because of the high sensitivity and quick response time, the fiber F-P sensors are attractive for applications involving pressure and temperature measurement [4]

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