Abstract

By X-ray stress analysis technique, a new approach has been applied to determining the yield strength of polycrystalline TiN film with biaxial residual stress adherent to metal substrate. By plasma-assisted chemical vapor deposition (PACVD), TiN film was deposited on a strip of spring steel 60Mn allowing the film to be subjected to tensile stress under loading of the film/substrate. The film thickness is 2.5μm and the steel substrate thickness is 1.1mm. Longitudinal and transverse stresses, σ 1 and σ 2 of the film were measured in situ by X-ray diffraction. On the basis of the experimental results, the effective stress o and the effective uniaxial strain e t were obtained. According to the σ-e t relation, the calculated proof stresses, σ 0.1 , and σ 0.2 , of TiN film are 4.2GPa and 4.4GPa, respectively.

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