Abstract
By examining the diffraction data, the microstructure of the ball-milled synthesized powder sample ([Formula: see text][Formula: see text]TiO3) was characterized. Through the application of Rietveld’s powder structure refinement approach to analyze X-ray powder diffraction data of ball-milled powder mixes, structural and microstructural alterations in terms of lattice defects have been assessed in the formation of single-phase praseodymium-modified BaTiO3. Bond lengths, bond angles, and generated locations of the [Formula: see text]Pr0[Formula: see text]TiO3 ceramic have been discussed about its generated structure. X-ray diffraction with respect to the first sharp diffraction peak (FSDP) is used to study the nanostructure of void species. General equations were utilized to determine various FSDP characteristics such as interlayer separation, correlation length, nanovoid diameter and scattering vector magnitude. Although the literature reports on many properties of Pr-modified barium titanate ceramic, this sample’s quantitative analysis and nanovoid determination are presented for the first time.
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