Abstract
The structure of (η 5-C 5H 5)Fe(CO) 2Si(Ph)(SiMe 3) 2, 1 has been studied by X-ray diffraction; 1 crystallizes in the P 1 space group with a 8.767(1), b 15.782(3), c 16.543(3) Å, α 87.84(1), β 86.28(1), and γ 85.47(1)°. There are two independent molecules in the asymmetric unit. Both conformers are staggered and related by a 120° rotation. The FeSi bond lengths are 2.366(1) and 2.355(1) Å. A steric argument is used to discuss the discrepancy in the FeSi distances.
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