Abstract
Highly resolved CKα spectra of the compounds K3C60 and K6C60 synthesized by thermal decomposition of potassium azide in a vacuum chamber of an X-ray tube were obtained. The possibility of monitoring the extent of intercalation of fullerenes by the CKα spectra is demonstrated. The results are compared with the MNDO calculations for K6C60. The data are used to construct a diagram of the structure of the highest occupied and C1s levels in the series C60−K3C60−K6C60.
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