Abstract
Minor amounts of rare earth elements (0.01 to 1.0%) in high-purity rare earth oxides may be determined by a fluorescent x-ray procedure. Basic to the method is accurate determination of spectral line intensity above background. Sample and standard preparation, choice of analytical lines, and utilization of a helium path to increase x-ray intensities are discussed. Precision and accuracy were evaluated by analyzing samples of known composition. The average of fiye separate determinations showed an average error of about 10%. (auth)
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