Abstract
The X-ray structure of H 10 Si 10 O 15 has been determined at 180 K and at 295 K. It crystallizes in the monoclinic space group I2/a, with a=14.141(8) A, b=8.953(3) A, c=15.022(8) A, β=94.91(3) o , and V=1894.9 A 3 at 180 K, a=14.254(5) A, b=9.053(2) A, c=15.062(5) A, β=94.87(1) o , and V=1936.6 A 3 at 295 K, Z=8, D x =1.86 g cm -3 (180 K), 1.82 g cm -3 (295 K), and fw=530.92. Single-crystal diffraction data were collected with λ(Mo Kα)=0.710 73 A and μ(Mo Kα)=7.45 cm -1 (180 K) and with λ(Ag Kα)=0.560 83 A μ(Ag Kα)=3.78 cm -1 (295 K)
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