Abstract
The crystal and molecular structure of the title compound has been determined by X-ray crystallography, 1H NMR and 13C NMR spectroscopy. In the crystals of the chiral carbohydrate the hydroxyl groups are held together by intramolecular H bonding, and there is an intermolecular link between one hydroxyl hydrogen atom and an oxygen of the isopropylidene ring. The tin atom is in a tetrahedral environment and the shortest Sn … O separation is 3.354(5) Å, an interaction that appeats to have no effect on the stereochemistry of the metal. The 1H NMR spectrum shows long-range splitting of a methylene proton by a hydroxyl hydrogen.
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