Abstract
Oxidation of various olefins into methylketones by a catalytic system constituted of palladium, copper, phosphomolybdovanadic acid and per(2,6-di- O-methyl)-β-cyclodextrin is investigated. The role of each redox catalytic system component is discussed from experiments under argon atmosphere and from vanadium NMR spectroscopic studies. The influence of various parameters, such as the per(2,6-di- O-methyl)-β-cyclodextrin concentration and the nature of the phosphomolybdovanadic acid is also reported. Finally, a catalytic cycle is also proposed.
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