Abstract

A completely automated method for the determination of oxygen in organic compounds is described. Parallel operation of two pyrolysis apparatus and two automatic titrators, with inclusion of a print-out desk calculator and an electrobalance, is electronically controlled, so that the total cycle, including the print-out of sample number, volume and sample weight, proceeds automatically. A single analysis requires 14–18 min, and the number of erroneous determinations is kept to a minimum by individual programming of the apparatus according to the pyrolysis properties of the compounds.

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