Abstract
AbstractThe compound [VO(dien)]2GeS4 (1, dien = diethylenetriamine) features an ortho‐thiogermanate anion [GeS4]4–, which acts as tetradentate ligand joining [VO(dien)]2– complexes. The compound was obtained under solvothermal conditions crystallizing in thenon‐centrosymmetric orthorhombic space group Pna21 with a =19.8310(11), b = 8.0814(5), c = 12.0889(9) Å, V = 1937.4(2) Å3 and Z = 4. The V4+ cations are in a distorted octahedral environment of a tridentate dien molecule, one oxygen atom and two sulfur atoms from the [GeS4]4– anion. A three‐dimensional network is generated by hydrogen bonding interactions.
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