Visualization and investigation of healing mechanism in carbon fiber reinforced Elium® composites

Abstract

In this study, carbon fiber/Elium® composites are manufactured using the resin infusion manufacturing technique. Artificial cracks representing impact-induced delamination are incorporated during layup. The laminates are subsequently healed using several healing parameters. The bonding mechanisms are investigated through microscopic analyses and X-ray Computed Tomography (XCT). The mechanical performance of the healed composites is investigated through four-point bending tests. It is found that as the healing temperature is increased, the cracks are gradually healed by interdiffusion and macroscopic resin flow across each crack interface. The 3D models generated from XCT images show an increase in solid volume fraction from 48% to 70% at the optimum healing parameters. The flexural strength and flexural modulus of the undamaged composites subjected to optimized healing condition are significantly increased relative to the room temperature cured pristine samples. The residual flexural strength of the damaged samples healed at the optimum parameters is 96% of the reference condition. The SEM images confirm that delamination from the previously-healed crack interfaces is the most dominant failure mode in the healed samples, in contrast to fiber fracture and brittle failure in the undamaged reference composite samples. The results show that the damaged composite laminates can be effectively healed and repaired to as good as undamaged laminates using the interdiffusion mechanism.