Abstract
Photocatalytic C(sp3)-H phosphorylation of xanthenes and 9,10-dihydroacridines with P(O)-H compounds under the irradiation of 18 W blue LEDs at room temperature using fluorescein as the photocatalyst and molecular oxygen (O2) as the sole oxidant has been achieved. The newly developed reaction provides direct access to 9-phosphorylated xanthene derivatives with good functional group compatibility.
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