Abstract
AbstractA visible light‐induced direct decarboxylative peroxidation of carboxylic acids under mild conditions has been disclosed. With this protocol, a variety of readily available carboxylic acids were converted to the peroxidation products in moderate to good yields via decarboxylative radical C−OO bond coupling. Tert‐butyl hydroperoxide acts as both the oxidant and peroxyl source, avoiding the use of transition metals or extra oxidants.
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