Viscoelastic characterization of coating layers by ultrasonic interference and critical attenuation

Abstract

This study proposes a characterization technique for a viscoelastic coating layer on a metal substrate immersed in water based on ultrasonic interference and critical attenuation phenomena. Theoretical analysis shows that the reflection spectrum for the normal incidence wave has local minima at the resonance frequencies of the coating layer, which provide its elastic property if the layer thickness is given a priori. Furthermore, it is revealed that the lower envelope of the reflection spectrum takes a minimum, whose frequency can be related to the critical attenuation condition. This feature implies a possibility that the viscous property of the coating material can be estimated by similarly measuring a characteristic frequency to the estimation of the elastic property. Two bonded specimens consisting of polycarbonate (PC) sheets and metal substrates were prepared to validate the proposed method. The reflection spectra measured for the normal wave incidence showed multiple local minima and critical attenuation, which are predicted to appear by theoretical predictions. The wave velocities and loss factors of PC estimated from the two specimens are in fair agreement with the properties shown in the previous paper. This result demonstrates that the ultrasonic interference and critical attenuation behavior can be applied to the characterization of the viscoelastic coating layers.