Abstract
The IR and Raman powder spectra for the CsHSO 4 in the function of temperature are measured. It is found that the measurements by the KBr pellet method and for the emulsion in Nujol using the KBr windows (in the presence of moisture) give the spectra of the KHSO 4. The spectra for the phases III, II and I are reported. Existence of phase IV is not supported by the vibrational data. Additionally, the reflection polarised spectra for the bc sample of CsHSO 4 single crystal in phase III are measured and discussed.
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