Abstract
The i.r. and Raman spectra of propiolyl chloride HCCCOCl and tetrolyl chloride CH 3CCCOCl were examined in the region 4000-40 cm −1. The i.r. spectra were recorded in the gas phase and solution, whereas the Raman spectra were obtained from the pure liquids. The fundamental frequencies have been assigned and the low frequency vibrations of the COCl group have been discussed. Relatively free rotation of the CH 3 group is evident from the i.r. spectrum. The syntheses of the compounds are reported.
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