Abstract
This research paper, reports the preparation of palladium impregnated [Zn2(BDC)2(4-bpdh)]3DMF (Pd@TMU-16) with a simple liquid impregnation-reduction method as a novel and efficient catalyst with the high catalytic performance for coupling reactions. To indicate the excellent performance of the presented catalytic system, the catalytic behavior of Pd@TMU-16 was tested in the Sonogashira C‐C coupling reaction of aryl halides with different functional groups with terminal alkynes, and the desired products were produced with good yields. In addition, Pd@TMU-16 was recovered and reused for at least five cycles, and no obvious activity changes was seen. The investigation on the amount of Pd loaded in the catalyst achieved by inductive couple plasma atomic emission spectroscopy (ICP-OES) showed its stability during the coupling reaction.
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