Abstract
A routine gas chromatographic analytical procedure has been developed for the reaction products of a vapor-phase butane nitrator. Replicate samples are used in 3 columns to give satisfactory quantitative separation of the C 1 to C 4 mononitroparaffins, alcohols, aldehydes, C 1 to C 4 paraffins, and NO, NO 2, CO, CO 2, all in the presence of water. Accuracy and precision are at least ±2% of the true value of any component. Carbon and nitrogen material balances of approximately 92% are obtained.
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