Abstract
Except in a two-phase system and contrary to expectation, ethoxycarbonylnitrene when generated from Lwowski's reagent by α-elimination does not add to the unsaturated cyclic sulphones (1)–(10) owing to the presence of orbital interactions (through bonds and through space)between the SO2 group and the double bond, as evidenced by u.v.–photoelectron spectrosocopy.
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