Abstract
Nanocrystalline Alloys In article number 2200354, Jason Trelewicz and co-workers connect nanocrystalline stability regimes with temperature-dependent segregation states through in situ mapping of microstructural evolution in Mo–Au nanometallic multilayers combined with thermodynamic predictions of stable solute configurations. These findings provide a framework for decoupling thermodynamic and kinetic contributions to the stability of nanocrystalline alloys exhibiting a transition from grain-boundary segregation to solute clustering and nanophase separation at elevated temperatures.
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