Abstract
A unique 3D entangling Cu(II)-metal organic framework, namely, {[Cu4(abtc)2(btab)6·3H2O]·2H2O}n (1), has been successfully constructed from CuII and 3,3′,5,5′-azo benzene tetracarboxylate building units with the aid of N-donor bridging spacers [1,4-bis(triazol)butane], and directs a rare self-penetrating structure with polyhelix motifs and presents a new (4,4,8)-connected (4.65)2(64.7.8)2(42.620.72.84) topology. The magnetic investigations demonstrate that complex 1 exhibits antiferromagnetic coupling interaction between the adjacent Cu(II) ions.
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